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Temperature dependent deformation mechanisms in magnesium alloys: insights from a combination of in-situ neutron diffraction and acoustic emission techniques

研究課題

研究課題/領域番号 23K04429
研究種目

基盤研究(C)

配分区分基金
応募区分一般
審査区分 小区分26040:構造材料および機能材料関連
研究機関国立研究開発法人日本原子力研究開発機構

研究代表者

Gong Wu  国立研究開発法人日本原子力研究開発機構, 原子力科学研究部門 J-PARCセンター, 研究副主幹 (30780770)

研究期間 (年度) 2023-04-01 – 2026-03-31
研究課題ステータス 交付 (2023年度)
配分額 *注記
4,550千円 (直接経費: 3,500千円、間接経費: 1,050千円)
2025年度: 910千円 (直接経費: 700千円、間接経費: 210千円)
2024年度: 1,300千円 (直接経費: 1,000千円、間接経費: 300千円)
2023年度: 2,340千円 (直接経費: 1,800千円、間接経費: 540千円)
キーワードMagnesium / Neutron diffraction / Acoustic emission / Deformation / Microstructure
研究開始時の研究の概要

Nowadays, there is a rising emphasis on the development of Mg and its alloys due to their significant potential for various applications. In present study, the deformation behavior and microstructure evolution of Mg alloys at temperature from 20K to 773K will be investigated by a combination of in-situ neutron diffraction and AE techniques. By conducting well-designed experiments and meticulous data analysis, valuable insights into Mg alloys can be gained to improve their performance in cryogenic and elevated temperature environments, as well as optimize hot forming processes.

研究実績の概要

The present study is to establish an experimental system that combines in-situ neutron diffraction and AE techniques to investigate the deformation behavior and microstructure evolution of Mg alloys at temperatures ranging from 20K to 723K. In FY2023, the applicant conducted the following experiments and presented the corresponding results at various conferences to achieve this aim:
(1) In-situ neutron diffraction experiments during deformation at cryogenic temperatures were successfully performed on AZ31 alloy and LZ91 alloy using the engineering diffractometer TAKUMI at J-PARC.
(2) The results of the AZ31 alloy showing the detwinning behavior at 20K were presented at the "2023 JIM Fall Meeting" and "PRICM 11".
(3) The results for the LZ91 alloy showing the deformation mechanisms at 20K and 77K were presented at "TMS 2024".

現在までの達成度 (区分)
現在までの達成度 (区分)

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理由

In FY 2023, the in-situ neutron diffraction during cryogenic deformation experiments were performed successfully. The temperature dependent deformation behavior of AZ31 alloy and dual-phase LZ91 alloy were investigated. The results were presented at one domestic conference and two international conferences.

今後の研究の推進方策

In FY 2024, the applicant will utilize the newly purchased AE sensor and pre-amplifier, combined with in-situ neutron diffraction, to track the deformation behavior of Mg alloys at cryogenic and elevated temperatures. Microstructure observation experiments will be conducted. The obtained results will be presented in conferences.
In FY 2025, the applicant will conduct additional experiments, data analysis. The results of these experiments will be presented in conferences. Additionally, the applicant intends to summarize all the findings for submission to academic journals.

報告書

(1件)
  • 2023 実施状況報告書
  • 研究成果

    (5件)

すべて 2024 2023

すべて 雑誌論文 (1件) 学会発表 (4件) (うち国際学会 3件)

  • [雑誌論文] Cryogenic Deformation Behavior of a Dual-Phase Mg-Li Alloy Investigated by In-Situ Neutron Diffraction2024

    • 著者名/発表者名
      Gong Wu, Gholizadeh Reza, Kawasaki Takuro, Aizawa Kazuya, Harjo Stefanus
    • 雑誌名

      TMS 2024: Magnesium Technology 2024

      巻: - ページ: 89-90

    • DOI

      10.1007/978-3-031-50240-8_19

    • ISBN
      9783031502392, 9783031502408
    • 関連する報告書
      2023 実施状況報告書
  • [学会発表] Cryogenic Deformation Behavior of a Dual-phase Mg-Li Alloy Investigated by In-situ Neutron Diffraction2024

    • 著者名/発表者名
      Wu Gong, Reza Gholizadeh, Takuro Kawasaki, Kazuya Aizawa, Stefanus Harjo
    • 学会等名
      TMS 2024 Annual Meeting & Exhibition
    • 関連する報告書
      2023 実施状況報告書
    • 国際学会
  • [学会発表] Deformation Mechanisms of AZ31 Magnesium Alloy at 21K Revealed by In-situ Neutron Diffraction2024

    • 著者名/発表者名
      Wu Gong, Takuro Kawasaki, Ruixiao Zheng, Tsuyoshi Mayama, Kazuya Aizawa, Stefanus Harjo, Nobuhiro Tsuji
    • 学会等名
      TMS 2024 Annual Meeting & Exhibition
    • 関連する報告書
      2023 実施状況報告書
    • 国際学会
  • [学会発表] その場中性子回折による20KにおけるAZ31合金の双晶形成と双晶消滅の調査2023

    • 著者名/発表者名
      ゴン ウー、ハルヨ ステファヌス、川崎 卓郎、相澤 一也、辻 伸泰
    • 学会等名
      日本金属学会 2023年秋期(第173回)講演大会
    • 関連する報告書
      2023 実施状況報告書
  • [学会発表] Twinning and detwinning in AZ31 alloy at 20K studied by in-situ neutron diffraction2023

    • 著者名/発表者名
      Wu Gong, Stefanus Harjo, Takuro Kawasaki, Kazuya Aizawa, Nobuhiro Tsuji
    • 学会等名
      The 11th Pacific Rim International Conference on Advanced Materials and Processing (PRICM11)
    • 関連する報告書
      2023 実施状況報告書
    • 国際学会

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公開日: 2023-04-13   更新日: 2024-12-25  

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