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2021 年度 実施状況報告書

Real-time quantitatively assessing the corrosion-induced hydrogen trapping in metals

研究課題

研究課題/領域番号 21K14435
研究機関東京大学

研究代表者

ウ ガイカ  東京大学, 大学院工学系研究科(工学部), 特任研究員 (70887984)

研究期間 (年度) 2021-04-01 – 2023-03-31
キーワードpitting corrosion / stress corrosion / acoustic emission / X-ray CT / steel / magensium alloy / alunimum alloy
研究実績の概要

1.A micro-experimental jig was designed and prepared to facilitate the micro-droplet corrosion testing, acoustic emission (AE) monitoring, in-situ video microscope (VM), and X-ray computed tomography (CT) scanning;
2.A visualization of a single pit-to-crack transition on SUS420J2 steel was revealed with specific AE signal evolution and X-ray CT observation; AE signals of hydrogen-bubble evolution and cracking were specifically separated owing to the k-means clustering method;
3.Evolution of pitting corrosion on AZX912 Mg alloy and AA5083 Al alloy was well monitored by AE signals and real-time microscopic in-situ observation; Passive-film rupture and hydrogen bubble evolution were well recognized by AE signals.

現在までの達成度 (区分)
現在までの達成度 (区分)

2: おおむね順調に進展している

理由

Each of the studies of interest was carried out as scheduled.

今後の研究の推進方策

In the second fiscal year, all studies will focus on experimental investigation on the hydrogen trapping during corrosion, which will be correlated the hydrogen-AE signals.
1.Regarding the droplet corrosion testing of high-strength alloys of SUS420J2, AX41, AA5083 alloys, a series of experiments interrupted at different points will be performed by integrated with TDS analysis to investigate the contents of corrosion-induced hydrogen trapping;
2.Corrosion-induced hydrogen entry into alloys will be correlatively analyzed with the various AE signals parameters and corrosion morphological aspect ratio.
3.Extra attention will also be placed on the AE signals during cathodic charging and the H-charging induced hydrogen trapping in metals.

次年度使用額が生じた理由

1. Regarding the travel expenses, no travel for academic activity was done because of the covid-19 pandemic last year; The relevant budget will be planned for participating in an international conference and several domestic conferences this fiscal year.
2. Article costs: it was planned to purchase a small environmental testing device for my experimental studies, but the price exceeds the budget amount of the previous fiscal year. So the budget from the previous fiscal year and the next fiscal year will be used together for the purchase of the environmental testing device.

  • 研究成果

    (5件)

すべて 2022 2021

すべて 学会発表 (5件) (うち国際学会 1件)

  • [学会発表] Analysis of pitting corrosion initiation in AZX912 alloy by in-situ 4D imaging and AE monitoring2022

    • 著者名/発表者名
      Kaige Wu, Manabu Enoki
    • 学会等名
      日本金属学会2022年春期(第170回)講演大会
  • [学会発表] Corrosion monitoring of Mg-Zn-Y alloy containing LPSO phase by acoustic emission method2021

    • 著者名/発表者名
      Kaige Wu, Nobu Yatagai, Fabien Briffod, Takayuki Shiraiwa, Manabu Enoki
    • 学会等名
      日本金属学会2021年秋期(第169回)講演大会
  • [学会発表] Transition of corrosion mode under a NaCl droplet in pure Mg and an extruded Mg-Al-Ca-Mn alloy studied by acoustic emission2021

    • 著者名/発表者名
      Kaige Wu, Manabu Enoki
    • 学会等名
      2021年度欧州腐食会議 (EUROCORR2021)
    • 国際学会
  • [学会発表] Characterizing anodic and cathodic pitting corrosion of AA5083 alloy during potentiodynamic polarization using AE method2021

    • 著者名/発表者名
      Kaige Wu, Manabu Enoki
    • 学会等名
      第23回アコースティック・エミッション総合コンファレンス
  • [学会発表] Analysis of acoustic emission (AE) characteristics of atmospheric and electrochemical corrosion of AZ31 Mg alloy2021

    • 著者名/発表者名
      Kaige Wu, Manabu Enoki
    • 学会等名
      日本非破壊検査協会2021年度秋季講演大会

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公開日: 2022-12-28  

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