1990 Fiscal Year Annual Research Report

放射光の応用による微小粒子と微結晶及びその成長過程に関する学際的共同研究

Research Project

Project/Area Number	01045006
Research Institution	University of Tsukuba
Principal Investigator	若槻雅男筑波大学, 物質工学系, 教授 (50114153)
Co-Investigator(Kenkyū-buntansha)	PARISE John State University of New York―SB, Dept. Ear, Assistan P WEIDNER Dona State University of New York―SB, Dept. Ear, Professor CHU Benjamin State University of New York―SB, Dept. Che, Professor 栗田敬筑波大学, 地球科学系, 助教授 (00111451) 浜谷望筑波大学, 物質工学系, 講師 (70156420) 中井泉筑波大学, 化学系, 講師 (90155648) 福谷博仁筑波大学, 物理学系, 助教授 (40011580) 大嶋建一筑波大学, 物理工学系, 助教授 (70109271) 青木貞雄筑波大学, 物理工学系, 助教授 (50016804) 藤井保彦筑波大学, 物質工学系, 教授 (00013524) 末野重穂筑波大学, 地球科学系, 教授 (30110513)
Keywords	微細粒子 / 結晶成長 / 放射光 / 高圧力 / 地球深部 / 物質合成
Research Abstract	本研究の目的は、微細粒子及びその集合体からの結晶生成の過程を広い視野から、かつ双方の大学が得意とする見地から、学際的に研究することである。平成2年度における両大学間の研究交流の経過は次の通りである。 1.7月18〜8月1日:末野がSB校を訪問。地球深部鉱物中の水素の存在について討論し、それについて双方で合成実験をすることになった。 2.7月19〜23日:B.Chu教授が本学を訪問。研究代表者らと交流研究の進め方について懇談の後、各研究室を視察。2回にわたり最近のレ-ザ-光散乱を応用した研究を紹介(講演会)。 3.9月23〜29日:研究代表者(若槻)がSB校を訪問。高圧合成についてLiebermann教授らと討論ならびに実験、また本学で開発した新しい光学用超高圧セルの紹介と討論を行った。 4.12月:福谷がSB校を訪問:Kirtz教授と軟X線領域の多層膜反射について共同研究を行った。 5.1月19日〜26日:Weidner及びLiebermann両教授が本学を訪問。高圧下における結晶成長について若槻、末野らと討論。また栗田との高圧合成実験についての打ち合せ、及び予備実験を行った。 6.3月11〜29日:栗田がSB校を訪問。地球深部物質の合成と高圧合成物質における水素の存在形態に関する実験を行った。以上の相互交流による研究成果は両大学における将来の研究の進展を大いに促すものである。また次年度は従来よりも一層若手研究者間の交流に注力することが双方によって了解された。

Research Products

(26 results)

All Other

All Publications (26 results)

[Publications] Masao Wakatsuki: "Detection of impurities in diamond grown in the metallic solvent by xーray fluorescence method using SR." Proc.2nd International Conf.on New Diamond Science and Technology,Washington,1990(Special issue of J.Materials Research). (1991)
[Publications] Kaoru J.Takano: "An optical high pressure cell with spherical sapphire anvils." Rev.Sci.Instrum.62. (1991)
[Publications] Kaoru J.Takano: "New high pressure phases of carbon." Japan.J.Appl.Phys.30. (1991)
[Publications] H.Yurimoto: "Quantitative SIMS analysis of GSJ rock reference samples." Geochem.Cosmochem.J.23. 215-235 (1990)
[Publications] C.K.Shearer: "Ion microprobe studies of trace elements in Apollo 14 volcanic glass beads:Comparison to Apoll 14 mare basalts and petrogenesis of picritic magas." Geochimica et Cosmochimica Acta. 54. 851-867 (1990)
[Publications] S.Sueno: "A SIMS study on lattice and dislocation diffusion in MgO." Proc.2nd Eurasia Conf.on on Chemistry,Seoul.171-172 (1990)
[Publications] H.Yurimoto: "Quantitative nickel analysis in GSJ standard rock using ionmass spectrometry." Geostandards Newsletter. (1990)
[Publications] 末野重穂: "SIMSによるセラミックスの微量分析ー最近の進歩ー" 工業と製品. 72. 147-152 (1990)
[Publications] N.Metoki: "Timeーresolved xーray diffraction study of oneーdimensional nucleation and growth in the firstーorder transition." Phys.Rev.Letters. 64. 657-660 (1990)
[Publications] Y.Ohishi: "Structural instability of PbSe/SnSe superlattices under pressure." High Pressure Research. 4. 300-302 (1990)
[Publications] H.Fujihisa: "Pressureーinduced molecular dissociation in iodine at low temperatures." High Pressure Research. 4. 330-332 (1990)
[Publications] S.Hayakawa: "Xーray microanalysis with energy tunable synchrotron xーrays." Nuclear Instruments and Methods in Physics Research. B49. 555-560 (1990)
[Publications] K.Ninomiya: "Xーray photoelectron spectroscopy using a focused 300μmーdiameter xーray beam." Jpn.J.Appl.Phys.29. 974-979 (1990)
[Publications] K.Ninomiya: "Xーray photoelectron spectroscopy of micrometerーsize surface area using synchrotron radiation." Jpn.J.Appl.Phys.29. L1026-L1028 (1990)
[Publications] Y.Kuroiwa: "Xーrayーdiffraction study of inーplane and interlayer correlations in layered compounds Ag_xTiS_2." Phys.Rev.B. B42. 11591-11597 (1990)
[Publications] 黒岩芳弘: "層間化合物Ag_xTis_2の次元間相転移" 日本結晶学会誌. 33. 1-6 (1991)
[Publications] N.Toyoshima: "A simple device for mounting a vacuum chamber on a fourーcircle diffractometer with central chiーcircle." to be published in J.Appl.Cryst.
[Publications] K.Yagi: "Angle resolved photoemission study of Pd(110)surface." Surf.Sci.231. 397-403 (1990)
[Publications] H.Fukutani: "Reflection and photoemission study of neutron irradiated graphite." J.Phys.Soc.Jpn.59. 3089-3093 (1990)
[Publications] T.Koide: "Optical study of stoichiometry dependent electronic structure of TiC_x,VC_x,and NbC_x." Phys.Rev.B42. 4979-4995 (1990)
[Publications] Izumi Nakai: "Synchrotron xーray Rietvert analysis of αーhafnium phosphate." Analytical Sci.6. 689-693 (1990)
[Publications] Izumi Nakai: "Singleーcrystal xーray structure analysis of new oxideーsuperconductor Bi_2(Sr_<1ーx>Ln_x)_2(Gd_<1ーy>Ce_y)_2Cu_2O_<10> _<+z>." Jpn.J.Appl.Phys.29. L572-L575 (1990)
[Publications] R.Miyawaki: "Crystal structure of rare earth minerals.3rd Supplement." 希土類. 17. 1-10 (1990)
[Publications] J.B.Parise: "Crystal structure and thermal expansion of(Mg,Fe)SiO_3 perovskite." Geophys.Res.Letters.17. (1990)
[Publications] N.Hamaya: "High Pressure Research" Search for polytypic structures of gadolinium., 375-377 (1990)
[Publications] 丁立業: "成都科学技術大学学報" 金鋼石合成用介質的伝圧効果研究, 41-46 (1990)

1990 Fiscal Year Annual Research Report

放射光の応用による微小粒子と微結晶及びその成長過程に関する学際的共同研究

Principal Investigator

若槻 雅男 筑波大学, 物質工学系, 教授 (50114153)

Research Products

[Publications] Masao Wakatsuki: "Detection of impurities in diamond grown in the metallic solvent by xーray fluorescence method using SR." Proc.2nd International Conf.on New Diamond Science and Technology,Washington,1990(Special issue of J.Materials Research). (1991)

[Publications] Kaoru J.Takano: "An optical high pressure cell with spherical sapphire anvils." Rev.Sci.Instrum.62. (1991)

[Publications] Kaoru J.Takano: "New high pressure phases of carbon." Japan.J.Appl.Phys.30. (1991)

[Publications] H.Yurimoto: "Quantitative SIMS analysis of GSJ rock reference samples." Geochem.Cosmochem.J.23. 215-235 (1990)

[Publications] C.K.Shearer: "Ion microprobe studies of trace elements in Apollo 14 volcanic glass beads:Comparison to Apoll 14 mare basalts and petrogenesis of picritic magas." Geochimica et Cosmochimica Acta. 54. 851-867 (1990)

[Publications] S.Sueno: "A SIMS study on lattice and dislocation diffusion in MgO." Proc.2nd Eurasia Conf.on on Chemistry,Seoul.171-172 (1990)

[Publications] H.Yurimoto: "Quantitative nickel analysis in GSJ standard rock using ionmass spectrometry." Geostandards Newsletter. (1990)

[Publications] 末野 重穂: "SIMSによるセラミックスの微量分析ー最近の進歩ー" 工業と製品. 72. 147-152 (1990)

[Publications] N.Metoki: "Timeーresolved xーray diffraction study of oneーdimensional nucleation and growth in the firstーorder transition." Phys.Rev.Letters. 64. 657-660 (1990)

[Publications] Y.Ohishi: "Structural instability of PbSe/SnSe superlattices under pressure." High Pressure Research. 4. 300-302 (1990)

[Publications] H.Fujihisa: "Pressureーinduced molecular dissociation in iodine at low temperatures." High Pressure Research. 4. 330-332 (1990)

[Publications] S.Hayakawa: "Xーray microanalysis with energy tunable synchrotron xーrays." Nuclear Instruments and Methods in Physics Research. B49. 555-560 (1990)

[Publications] K.Ninomiya: "Xーray photoelectron spectroscopy using a focused 300μmーdiameter xーray beam." Jpn.J.Appl.Phys.29. 974-979 (1990)

[Publications] K.Ninomiya: "Xーray photoelectron spectroscopy of micrometerーsize surface area using synchrotron radiation." Jpn.J.Appl.Phys.29. L1026-L1028 (1990)

[Publications] Y.Kuroiwa: "Xーrayーdiffraction study of inーplane and interlayer correlations in layered compounds Ag_xTiS_2." Phys.Rev.B. B42. 11591-11597 (1990)

[Publications] 黒岩 芳弘: "層間化合物Ag_xTis_2の次元間相転移" 日本結晶学会誌. 33. 1-6 (1991)

[Publications] N.Toyoshima: "A simple device for mounting a vacuum chamber on a fourーcircle diffractometer with central chiーcircle." to be published in J.Appl.Cryst.

[Publications] K.Yagi: "Angle resolved photoemission study of Pd(110)surface." Surf.Sci.231. 397-403 (1990)

[Publications] H.Fukutani: "Reflection and photoemission study of neutron irradiated graphite." J.Phys.Soc.Jpn.59. 3089-3093 (1990)

[Publications] T.Koide: "Optical study of stoichiometry dependent electronic structure of TiC_x,VC_x,and NbC_x." Phys.Rev.B42. 4979-4995 (1990)

[Publications] Izumi Nakai: "Synchrotron xーray Rietvert analysis of αーhafnium phosphate." Analytical Sci.6. 689-693 (1990)

[Publications] Izumi Nakai: "Singleーcrystal xーray structure analysis of new oxideーsuperconductor Bi_2(Sr_<1ーx>Ln_x)_2(Gd_<1ーy>Ce_y)_2Cu_2O_<10> _<+z>." Jpn.J.Appl.Phys.29. L572-L575 (1990)

[Publications] R.Miyawaki: "Crystal structure of rare earth minerals.3rd Supplement." 希土類. 17. 1-10 (1990)

[Publications] J.B.Parise: "Crystal structure and thermal expansion of(Mg,Fe)SiO_3 perovskite." Geophys.Res.Letters.17. (1990)

[Publications] N.Hamaya: "High Pressure Research" Search for polytypic structures of gadolinium., 375-377 (1990)

[Publications] 丁 立業: "成都科学技術大学学報" 金鋼石合成用介質的伝圧効果研究, 41-46 (1990)

若槻雅男筑波大学, 物質工学系, 教授 (50114153)

[Publications] 末野重穂: "SIMSによるセラミックスの微量分析ー最近の進歩ー" 工業と製品. 72. 147-152 (1990)

[Publications] 黒岩芳弘: "層間化合物Ag_xTis_2の次元間相転移" 日本結晶学会誌. 33. 1-6 (1991)

[Publications] 丁立業: "成都科学技術大学学報" 金鋼石合成用介質的伝圧効果研究, 41-46 (1990)