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2006 Fiscal Year Final Research Report Summary

Selective Synthesis of Luminescent Metal Complexes by Microwave Thermo-Catalytic Method and Development of Environment Friendly Reaction Processes.

Research Project

Project/Area Number 16350084
Research Category

Grant-in-Aid for Scientific Research (B)

Allocation TypeSingle-year Grants
Section一般
Research Field Environmental chemistry
Research InstitutionMinerva Light Laboratory L.C.C.

Principal Investigator

MATSUMURA Takeko  Minerva Light Laboratory, L.L.C., Microwave Chemistry Department, Chief Researcher, マイクロ波化学部, 主任研究員 (60031556)

Co-Investigator(Kenkyū-buntansha) MATSUMURA Kiiro  Minerva Light Laboratory, L.L.C., Microwave Chemistry Department, Researcher, マイクロ波化学部, 研究員 (50426649)
IIDA Masayasu  Nara Women's University, Faculty of Science, Professor (00107343)
NAKAJIMA Riichiro  Doshisha University, Faculty of Science and Industry, Professor (20066286)
YAMAUCHI Jun  Minerva Light Laboratory, L.L.C., Microwave Measurement Department, Researcher (10027071)
MIKATA Yuji  Nara Women's University, Kyousei Science Center, Associate Professor (10252826)
Project Period (FY) 2004 – 2006
KeywordsMicrowave thermo-catalysis / Luminescent complexes / Polypyridine Complexes / Rear earth metal complexes. / Precise microwave reactor
Research Abstract

Selective synthesis of luminescent metal complexes by microwave thermo-catalytic method is studied.Luminescent Ir(III)-polypyridine complexes, Tb(III) and Eu (III) complexes with β-diketone and polypyridine ligand have been synthesized under microwave irradiation with various microwave reaction equipments. High Intense luminescent complexes with various emission colors were obtained rapidly with high yields. The photochemical properties of these luminescent complexes were investigated. Semiconductor HPA precise microwave chemical reactor has been newly developed for environment friendly reaction processes. With this equipment, microwave synthesis of metal complexes and nano gold particles has been efficiently carried out.
As related study, liquid crystal metal complexes and organic compounds have been synthesized and their physicochemical properties have been studied. Luminescent metal complexes with novel ligands were also studied.

  • Research Products

    (16 results)

All 2007 2006 2005 2004 Other

All Journal Article (16 results)

  • [Journal Article] マイクロ波化学の原理と実際2007

    • Author(s)
      松村竹子
    • Journal Title

      分離技術 37

      Pages: 6-11

    • Description
      「研究成果報告書概要(和文)」より
  • [Journal Article] Facile synthesis of 2-(b- C glucopyranosyl)-b-amino acid : A new class of glycopeptide building block2007

    • Author(s)
      Y.Mikata, T.Fujimoto, Y.Sugai, S.Yano
    • Journal Title

      Tetrahedron Lett. 48

      Pages: 993-997

    • Description
      「研究成果報告書概要(和文)」より
  • [Journal Article] 金ナノ粒子のマイクロ波合成と表面増強ラマン散乱2007

    • Author(s)
      福岡隆夫, 松村竹子, 森康維
    • Journal Title

      0 70

      Pages: 14

    • Description
      「研究成果報告書概要(和文)」より
  • [Journal Article] Microwave synthesis of gold nano particles and their surface enhanced Raman spectra2007

    • Author(s)
      T.Fukuoka, T.Matsumura, Y.Mori
    • Journal Title

      J.Photo.Soc.Japan 70

      Pages: 14

    • Description
      「研究成果報告書概要(欧文)」より
  • [Journal Article] Principle and practical view of Microwave Chemistry2007

    • Author(s)
      T.Matsumura
    • Journal Title

      Bunrigijutu 37

      Pages: 2

    • Description
      「研究成果報告書概要(欧文)」より
  • [Journal Article] Efficient microwave synthesis of luminescent europium(III) complexes with polypyridine and the study of electrospectrochemistry2006

    • Author(s)
      Y.Masuda, S.Wada, T.Nakamura, T.Matsumura-Inoue
    • Journal Title

      Journal of Alloys and Compounds 1017-102

      Pages: 408-412

    • Description
      「研究成果報告書概要(和文)」より
  • [Journal Article] 半導体マイクロ波反応装置の開発2006

    • Author(s)
      松村竹子, 藤井 知, 福岡隆夫, 栗原英紀, 矢嶋龍彦
    • Journal Title

      ケミカルエンジニヤリング 51

      Pages: 590-596

    • Description
      「研究成果報告書概要(和文)」より
  • [Journal Article] 講座マイクロ波化学への招待1、マイクロ波化学の原理-マイクロ波の電界と物質の誘電特性-2006

    • Author(s)
      松村竹子
    • Journal Title

      化学と教育 54

      Pages: 402-405

    • Description
      「研究成果報告書概要(和文)」より
  • [Journal Article] Principle of microwave chemistry2006

    • Author(s)
      T.Matsumura
    • Journal Title

      Chemistry and Education 54

      Pages: 402-405

    • Description
      「研究成果報告書概要(欧文)」より
  • [Journal Article] Efficient microwave synthesis of luminescent europium(III) complexes with polypyridine and the study of electrospectrochemistry2006

    • Author(s)
      Y.Masuda, S.Wada, T.Nakamura, T.Matsumura-Inoue
    • Journal Title

      Journal of Alloys and Compounds 408-412

      Pages: 1017-1021

    • Description
      「研究成果報告書概要(欧文)」より
  • [Journal Article] Development of semiconductor HPA precise microwave chemical reactor2006

    • Author(s)
      T.Matsumura, T.Fujii, et al.
    • Journal Title

      Chemical Engineering 51

      Pages: 590-596

    • Description
      「研究成果報告書概要(欧文)」より
  • [Journal Article] 蛍光錯体のマイクロ波合成の新展開2005

    • Author(s)
      松村竹子
    • Journal Title

      ケミカルエンジニヤリング 50

      Pages: 26-31

    • Description
      「研究成果報告書概要(和文)」より
  • [Journal Article] Microwave synthesis of Luminescent Complexes, New Development2005

    • Author(s)
      T.Matsumura
    • Journal Title

      Chemical Engineering 50

      Pages: 26-31

    • Description
      「研究成果報告書概要(欧文)」より
  • [Journal Article] Microwave synthesis of novel Ir(III) complexes and their application to electroluminescence device2004

    • Author(s)
      T.Matsumura-Inoue, Y.Yamamot, N.Yoshikawa, M.Terashima, Y.Yoshida, A.Fujii, K.Yoshino
    • Journal Title

      Optical Materials 27

      Pages: 18-191

    • Description
      「研究成果報告書概要(欧文)」より
  • [Journal Article] Microwave Synthesis of Iridium(III) Complexes : Synthesis of Highly Efficient Orange Emitters in Organic Light-Emitting Devices2004

    • Author(s)
      K.Saito, N.Matsusue, H.Kanno, Y.Hamada, H.Takahashi, T.Matsumura
    • Journal Title

      Japanese Journal of Applied Physics 43

      Pages: 2733-2734

    • Description
      「研究成果報告書概要(欧文)」より
  • [Journal Article] Introduction to Microwave Chemistry

    • Author(s)
      T.Matsumura
    • Journal Title

      Chemistry and Education 53, 52

      Pages: 251-252, 356-357, 412-413, 344-343,420-421,495-496,565-566,721-722,863-864

    • Description
      「研究成果報告書概要(欧文)」より

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Published: 2008-05-27  

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