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2011 Fiscal Year Final Research Report

Development and application of nano-analysis of optical materials by multi-dimensional spectrum image technique

Research Project

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Project/Area Number 21360321
Research Category

Grant-in-Aid for Scientific Research (B)

Allocation TypeSingle-year Grants
Section一般
Research Field Inorganic materials/Physical properties
Research InstitutionNagoya University

Principal Investigator

MUTO Shunsuke  名古屋大学, 工学研究科, 教授 (20209985)

Co-Investigator(Kenkyū-buntansha) YOSHIDA Tomoko  名古屋大学, エコトピア科学研究所, 准教授 (90283415)
TATSUMI Kazuyoshi  名古屋大学, 工学研究科, 講師 (00372532)
Project Period (FY) 2009 – 2011
Keywords発光材料 / 透過電子顕微鏡 / カソードルミネッセンス / 電子エネルギー損失分光 / スペクトラムイメージ / 多変量解析 / 蛍光材料
Research Abstract

The main achievement of this study is summarized in the following(1) We succeeded in developing a TEM specimen holder with the light-collecting system integrated, whose collection efficiency was increased by two orders of magnitude. We confirmed that it was able to measure cathodoluminescence from nanometer areas of optical materials.(2) We improved a program for multivariate curve resolution and clarified the nano-structure and spatial distributions of the chemical bonding states of the white-luminescent carbonized meso-porous silica nanocomposite, consisting of only ubiquitous elements.

  • Research Products

    (22 results)

All 2012 2011 2010 2009 Other

All Journal Article (6 results) (of which Peer Reviewed: 6 results) Presentation (14 results) Remarks (1 results) Patent(Industrial Property Rights) (1 results)

  • [Journal Article] White light emission from amorphous silicon-oxycarbide materials2012

    • Author(s)
      Y. Ishikawa, K. Sato, S. Kawasaki, Y. Ishii, A. Matsumura and S. Muto
    • Journal Title

      Phys. Stat

      Pages: 1-4

    • DOI

      DOI:10.1002/pssa.201100816

    • Peer Reviewed
  • [Journal Article] Site occupancy determination of Eu/Y doped in Ca_2SnO_4 phosphor by electron channeling microanalysis2011

    • Author(s)
      S. Muto, Y. Fujimichi, K. Tatsumi, H. Yamane and T. Kawano
    • Journal Title

      Optical materials

      Volume: 33 Pages: 1015-1018

    • DOI

      DOI:10.1016/J.optmat.2010.09.022

    • Peer Reviewed
  • [Journal Article] Attribution of white-light emitting centers with carbonized surface in nano-structured SiO_2 : C layers2011

    • Author(s)
      A. V. Vasin, S. Muto, Y. Ishikawa, J. Salonen, A. N. Nazarov and V. S. Lysenko
    • Journal Title

      Thin Solid Films

      Volume: 519 Pages: 4008-4011

    • DOI

      DOI:10.1016/j.tsf.2011.01.199

    • Peer Reviewed
  • [Journal Article] Comparative study of annealing and oxidation effects in a-SiC : H and a-SiC thin films deposited by radio-frequency magnetron sputtering2011

    • Author(s)
      A. V. Vasin, S. Muto, Y. Ishikawa, A. V. Rusavsky, T. Kimura, V. S. Lysenko and A. N. Nazarov
    • Journal Title

      Thin Solid Films

      Volume: 519 Pages: 2218-2224

    • DOI

      DOI:10.1016/j.tsf.2010.11.005

    • Peer Reviewed
  • [Journal Article] Qantitative determination of site occupancy of multi-rare-earth elements doped into Ca_2SnO_4 phosphor by electron channeling microanalysis2010

    • Author(s)
      Y. Fujimichi, S. Muto, K. Tatsumi, T. Kawano and H. Yamane
    • Journal Title

      Journal of Solid State Chemistry

      Volume: 183 Pages: 2127-2132

    • DOI

      DOI:10.1016/j.jssc.2010.07.026

    • Peer Reviewed
  • [Journal Article] Diagnostic nano-analysis of materials properties by multivariate curve resolution applied to spectrum images by S/TEM-EELS2009

    • Author(s)
      S. Muto, T. Yoshida and K. Tatsumi
    • Journal Title

      Materials Transactions

      Volume: 50 Pages: 964-969

    • Peer Reviewed
  • [Presentation] 反応触媒濃度によるメソポーラスカーボンシリカの発光色制御2012

    • Author(s)
      佐藤功二、石川由加里、石井陽祐、川崎晋司、武藤俊介
    • Organizer
      公益社団法人日本セラミック協会2012年年会
    • Place of Presentation
      京都
    • Year and Date
      20120319-20
  • [Presentation] サブナノ領域分光イメージング-最新TEM分析技術2011

    • Author(s)
      武藤俊介
    • Organizer
      金属学会鉄鋼協会東海支部若手材料研究会第60回研究会「最新の分析評価技術」
    • Place of Presentation
      名古屋
    • Year and Date
      2011-12-13
  • [Presentation] Ge添加シリカガラス発光材料のXAFS-S/TEM局所構造解析2011

    • Author(s)
      吉田朋子、武藤俊介、レニユリアティ、吉田寿雄
    • Organizer
      日本金属学会第149回秋期講演大会
    • Place of Presentation
      沖縄
    • Year and Date
      2011-11-08
  • [Presentation] Analysis of nanostructure of Mesoporous Carbon-Silica Nanocomposites2011

    • Author(s)
      ファンウェイ、武藤俊介
    • Organizer
      日本金属学会第149回秋期講演大会
    • Place of Presentation
      沖縄
    • Year and Date
      2011-11-07
  • [Presentation] Ge添加シリカガラスの紫外発光サイト局所構造のEXAFS-RMC解析2010

    • Author(s)
      吉田朋子、武藤俊介、Leny Yuliati、吉田寿雄
    • Organizer
      日本金属学会2010年秋期(第147回)講演大会
    • Place of Presentation
      北海道
    • Year and Date
      2010-09-25
  • [Presentation] Quantitative site Occupancy Determination of Multi-Rare-Earth Elements Doped in Ca2SnO4 Phosphor by Electron Channeling Microanalysis2010

    • Author(s)
      Y. Fujimichi, S. Muto, K. Tatsumi, H. Yamane and K. Kawano
    • Organizer
      The 2nd International Symposium on Advanced Microscopy and Theoretical Calculation(AMTC2)
    • Place of Presentation
      名古屋
    • Year and Date
      2010-06-25
  • [Presentation] Site occupancy determination of Eu/Y doped in Ca2SnO4 phosphor by electron channeling microanalysis2010

    • Author(s)
      S. Muto, Y. Fujimichi, K. Tatsumi, H. Yamane and T. Kawano
    • Organizer
      E-MRS 2010 Spring Meeting
    • Place of Presentation
      Strasbourg, France
    • Year and Date
      2010-06-10
  • [Presentation] 白色発光を示すSi-O-Cナノ構造体の化学結合イメージング2010

    • Author(s)
      武藤俊介、Vasin Andriy、石川由加里、柴田典義
    • Organizer
      日本顕微鏡学会第66回学術講演会
    • Place of Presentation
      名古屋
    • Year and Date
      2010-05-24
  • [Presentation] Eu, Y添加Ca2SnO4赤色蛍光材料の電子チャネリングTEM-EELS/EDXによる状態分析2010

    • Author(s)
      武藤俊介、藤通有希、巽一厳、山根久典、川野哲也
    • Organizer
      日本顕微鏡学会第66回学術講演会
    • Place of Presentation
      名古屋
    • Year and Date
      2010-05-24
  • [Presentation] Eu, Y添加Ca2SnO4赤色蛍光材料のTEM-EELS/EDXによる状態分析2010

    • Author(s)
      藤通有希,武藤俊介,巽一厳,山根久典,川野哲也
    • Organizer
      日本金属学会2010年春期大会
    • Place of Presentation
      筑波
    • Year and Date
      2010-03-29
  • [Presentation] 白色発光を示すSi-O-Cナノ構造体の化学結合マッピング2010

    • Author(s)
      武藤俊介, A. V. Vasin,石川由加里,柴田典義
    • Organizer
      日本金属学会2010年春期大会
    • Place of Presentation
      筑波
    • Year and Date
      2010-03-29
  • [Presentation] 多変量スペクトル分解法によるSTEM-EELS化学結合マップ2009

    • Author(s)
      武藤俊介
    • Place of Presentation
      東京
    • Year and Date
      2009-10-31
  • [Presentation] 多変量スペクトル分解法の基礎とスペクトラムイメージングへの応用2009

    • Author(s)
      武藤俊介
    • Organizer
      第25回分析電子顕微鏡討論会
    • Place of Presentation
      幕張
    • Year and Date
      2009-09-01
  • [Presentation] TEM関連スペクトロスコピーによる情報抽出法2009

    • Author(s)
      武藤俊介
    • Organizer
      金属学会セミナー「機能元素のナノ材料科学」
    • Place of Presentation
      京都
    • Year and Date
      2009-07-24
  • [Remarks]

    • URL

      http://www.jfcc.or.jp/25_press/r10_3.html

  • [Patent(Industrial Property Rights)] 発光体およびその製造方法2009

    • Inventor(s)
      石川由加里、柴田典義、A. V. Vasin、J. Salonen,武藤俊介
    • Industrial Property Rights Holder
      (財)ファインセラミックスセンター
    • Industrial Property Number
      特許、特願2009-18031
    • Filing Date
      2009-01-29

URL: 

Published: 2013-07-31  

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