2011 Fiscal Year Final Research Report
The determination of vital reactions in charred bodies by GC-MS analysis of pyrolysis products in blood
Project/Area Number |
21590751
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Research Category |
Grant-in-Aid for Scientific Research (C)
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Allocation Type | Single-year Grants |
Section | 一般 |
Research Field |
Legal medicine
|
Research Institution | Fukuoka University |
Principal Investigator |
HARA Kenji 福岡大学, 医学部, 講師 (00090738)
|
Co-Investigator(Kenkyū-buntansha) |
KUBO Shinichi 福岡大学, 医学部, 教授 (10205122)
KASHIWAGI Masayuki 福岡大学, 医学部, 助教 (70301687)
|
Project Period (FY) |
2009 – 2011
|
Keywords | 焼死体 / 揮発性物質 / 高熱分解産物 / ガスクロマトグラフィー / 質量分析法 / 固相マイクロ抽出 / 生活反応 |
Research Abstract |
We studied the analysis of pyrolysis products, or smoke components, from the blood of charred bodies. The analysis method included cryogenic-focusing gas chromatography-mass spectrometry following solid-phase micro-extraction of the volatile compounds from the headspace of a blood sample vial. Using this method, pyrolysis products such as phenylacetylene, styrene, indene, and naphthalene were detected from the blood of charred bodies that had accompanying heat wounds. The smoke components generated from a fire event being found in a charred body's blood could serve as evidence of the charred body having been alive at the start of the fire.
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Research Products
(2 results)
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[Presentation] Faster gas chromatography-mass spectrometry analysis using tandem columns2011
Author(s)
Hara, K., Kashiwagi, M., Waters, B., Matsusue, A., Sugimura, T., Hamasato, S., Kubo, S.
Organizer
8th International Symposium Advances in Legal Medicine(ISALM)
Place of Presentation
Frankfurt am Main, Germany
Year and Date
20110000
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[Presentation] Demonstration of pyrolysis products in blood from charred cadaver by cryogenic gas chromatography-mass spectrometry following low-temperature headspace solid-phase microextraction2009
Author(s)
Hara, K., Kubo, S., Kashiwagi, M., Matsusue, A., Kageura, M.
Organizer
47th TIAFT
Place of Presentation
Geneva, Switzerland
Year and Date
20090823-27