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2013 Fiscal Year Final Research Report

Concurrent material damage evaluation using diffraction contrast imaging by ultra-bright synchrotron radiation

Research Project

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Project/Area Number 23360056
Research Category

Grant-in-Aid for Scientific Research (B)

Allocation TypeSingle-year Grants
Section一般
Research Field Materials/Mechanics of materials
Research InstitutionKobe University

Principal Investigator

NAKAI Yoshikazu  神戸大学, 工学(系)研究科(研究院), 教授 (90155656)

Co-Investigator(Kenkyū-buntansha) SHIOZAWA Daiki  神戸大学, 大学院工学研究科, 准教授 (60379336)
TANAKA Hiroshi  神戸大学, 大学院工学研究科, 准教授 (80236629)
Project Period (FY) 2011-04-01 – 2014-03-31
Keywordsマイクロ材料力学 / シンクロトロン放射光 / 疲労 / 金属組織
Research Abstract

The three dimensional grain mapping technique for polycrystalline material, which is called X-ray diffraction contrast tomography (DCT) has proposed. In the present study, the measurement of DCT was conducted in SPring-8, which is the brightest synchrotron radiation facility in Japan, and the condition of measurement and data procedure are discussed. Developed technique was applied to aluminium alloy and stainless steel. The shape and location of grain could be determined by the developed three-dimensional mapping technique using the apparatus in a bending beam line of SPring-8. To evaluate plastic deformation, the grain orientation spreads of individual grains were measured. The grain orientation spread is caused by the mosaicity, which relates to the dislocation structure in a grain. The grain orientation spread was found to increase with increasing plastic strain. Fatigue damage also could be evaluated by the grain orientation spread in the DCT measurement.

  • Research Products

    (63 results)

All 2014 2013 2012 2011 Other

All Journal Article (15 results) (of which Peer Reviewed: 11 results) Presentation (44 results) (of which Invited: 2 results) Book (3 results) Remarks (1 results)

  • [Journal Article] Observation of Rolling Contact Fatigue Cracks by Laminography Using Ultra-bright Synchrotron Radiation2014

    • Author(s)
      D.Shiozawa, T.Makino, Y.Neishi, and Y.Nakai
    • Journal Title

      Procedia Materials Science

      Volume: (To be published)

    • Peer Reviewed
  • [Journal Article] Evaluation of Rolling Contact Fatigue Crack Path in High Strength Steel with Artificial Defects2014

    • Author(s)
      T.Makino, Y.Neishi, D.Shiozawa, Y.Fukuda, K.Kajiwara and Y.Nakai
    • Journal Title

      International Journal of Fatigue

    • DOI

      10.1016/j.ijfatigue.2014.05.006

    • Peer Reviewed
  • [Journal Article] Evaluation of Fatigue Damage by Diffraction Contrast Tomography Using Synchrotron Radiation2014

    • Author(s)
      Daiki Shiozawa, Yoshikazu Nakai, Ryotaro Miura, and Shota Matsuda
    • Journal Title

      Materials Science Forum

      Volume: Vols.783-786 Pages: 2359-2364

    • Peer Reviewed
  • [Journal Article] Fatigue of Ultra-fine Grained α-brass2014

    • Author(s)
      Yoshikazu Nakai, Takuto Imanaka and Daiki Shiozawa
    • Journal Title

      Advanced Materials Research

      Volume: Vols.891-892 Pages: 1125-1130

    • Peer Reviewed
  • [Journal Article] Evaluation of Fatigue Damage by Diffraction Contrast Imaging using Ultra-bright Synchrotron Radiation2014

    • Author(s)
      Daiki Shiozawa, Yoshikazu Nakai, Ryotaro Miura, and Shota Matsuda
    • Journal Title

      Advanced Materials Research

      Volume: Vols.891-892 Pages: 600-605

    • Peer Reviewed
  • [Journal Article] Observation of 3D Shape and Propagation Mode Transition of Fatigue Cracks in Ti-6Al-4V under Cyclic Torsion Using CT Imaging with Ultra-Bright Synchrotron Radiation2014

    • Author(s)
      D.Shiozawa, Y.Nakai, T.Murakami, and H.Nosho
    • Journal Title

      International Journal of Fatigue

      Volume: Vol.58 Pages: 158-165

    • Peer Reviewed
  • [Journal Article] 水素チャージしたTiNi 形状記憶合金細線の力学特性2012

    • Author(s)
      宮部成央,田中拓,中井善一,川西翔
    • Journal Title

      材料

      Volume: Vol.61, No.11 Pages: 905-911

    • Peer Reviewed
  • [Journal Article] Evaluation of Rolling Contact Fatigue Crack Path of High Strength Steel with Artificial Defect2012

    • Author(s)
      T.Makino, Y.Neishi, D.Shiozawa, Y.Fukuda and Y.Nakai
    • Journal Title

      Proceedings of the 4th International Conference on Crack Paths

      Volume: CD-ROM, No.071

  • [Journal Article] Observation of Fatigue Crack Prop -agation Mode Transition under Cyclic Torsion Using Micro-CT Imaging with Ultra-Bright Synchrotron Radiation2012

    • Author(s)
      Y.Nakai, D.Shiozawa, T.Murakami, and H.Nosho
    • Journal Title

      Proceedings of the 4th International Conference on Crack Paths

      Volume: CD-ROM, No.035

  • [Journal Article] Observation of Cracks in Carbon Steel under Contact Rolling Fatigue by Micro CT Imaging using Ultra-bright Synchrotron Radiation2012

    • Author(s)
      Daiki Shiozawa, Yoshikazu Nakai, Yoshiyuki Fukuda, Yutaka Neishi, and Taizo Makino
    • Journal Title

      Proceedings of the 15th International Conference on Experimental Mechanics

      Volume: CD-ROM, No.2635

  • [Journal Article] Development of Three-Dimensional Grain Mapping Technique in Spring-8 and Evaluation of Plastic Strain2012

    • Author(s)
      Daiki Shiozawa, Yoshikazu Nakai, Kenta Tsutsumi, Ryotaro Miura Kentaro Kajiwara
    • Journal Title

      Proceedings of the 15th International Conference on Experimental Mechanics

      Volume: CD-ROM, 2772

  • [Journal Article] TiNi 形状記憶合金細線のSSRT 強度に及ぼす水素吸収の影響2012

    • Author(s)
      宮部成央,田中拓,中井善一,川西翔
    • Journal Title

      日本機械学会論文集(A編)

      Volume: Vol.78, No.786 Pages: 190-200

    • Peer Reviewed
  • [Journal Article] 工業用純鉄細線の疲労損傷に及ぼす降伏現象の影響2011

    • Author(s)
      宮部成央,田中拓,中井善一,中村太郎
    • Journal Title

      日本機械学会論文集(A編)

      Volume: 77巻784号 Pages: 2098-2106

    • Peer Reviewed
  • [Journal Article] Initiation and Growth of Pits and Cracks in Corrosion Fatigue for High Strength Aluminium Alloy Observed by Micro Computed-tomography Using Ultra-bright Synchrotron Radiation2011

    • Author(s)
      Yoshikazu Nakai and Daiki Shiozawa
    • Journal Title

      Applied Mechanics and Materials

      Volume: Vol.83 Pages: 162-167

    • Peer Reviewed
  • [Journal Article] Observation of Fatigue Crack Propagation Behavior under Torsional Loading by Using Synchrotron Radiation Micro-CT Imaging2011

    • Author(s)
      Daiki Shiozawa, Yoshikazu Nakai, Tomonori Murakami, and Hiroaki Nosho
    • Journal Title

      Procedia Engineering

      Volume: Volume 10 Pages: 1483-1488

    • Peer Reviewed
  • [Presentation] 4D Evaluation of Grain Shape and Fatigue Damage of Individual Grain in Polycrystalline Alloys by Diffraction Contrast Tomography Using Ultra-bright Synchrotron Radiation2014

    • Author(s)
      D.Shiozawa, Y.Nakai, R.Miura, and S.Matsuda
    • Organizer
      International Conference on Fatigue Damage of Structural Materials X
    • Place of Presentation
      The Resort and Conference Center at Hyannis, MA, USA
    • Year and Date
      20140921-26
  • [Presentation] 高輝度放射光ラミノグラフィを用いた高強度鋼中の転動疲労き裂の観察2014

    • Author(s)
      小濱友也,塩澤大輝,佐藤一矢,根石豊,牧野泰三,中井善一
    • Organizer
      日本機械学会材料力学講演会(M&M2014)
    • Place of Presentation
      福島市
    • Year and Date
      20140719-21
  • [Presentation] Observation of Rolling Contact Fatigue Cracks by Laminography Using Ultra-bright Synchrotron Radiation2014

    • Author(s)
      D.Shiozawa, T.Makino, Y.Neishi, and Y.Nakai
    • Organizer
      20th European Conference on Fracture (ECF20)
    • Place of Presentation
      Trondheim, Norway
    • Year and Date
      20140630-0704
  • [Presentation] 放射光回折コントラストトモグラフィによる低サイクル疲労の損傷評価2014

    • Author(s)
      中尾亮太,塩澤大輝,中井善一,政田尚也,松田翔太
    • Organizer
      日本材料学会第63期学術講演会
    • Place of Presentation
      福岡市
    • Year and Date
      20140517-18
  • [Presentation] バルク金属ガラスの腐食環境下での下限界近傍における疲労き裂伝ぱに関する研究2014

    • Author(s)
      上野晃平,中井善一,今井 貴文
    • Organizer
      日本機械学会関西支部 第89期定時総会講演会
    • Place of Presentation
      堺市
    • Year and Date
      20140318-19
  • [Presentation] 疲労破面の粗さより破壊力学パラメータを推定する手法の開発に関する研究2014

    • Author(s)
      大邊優,中井善一
    • Organizer
      日本機械学会関西支部 第89期定時総会講演
    • Place of Presentation
      堺市
    • Year and Date
      20140318-19
  • [Presentation] Evaluation of Fatigue Damage by Diffraction Contrast Imaging using Ultra-bright Synchrotron Radiation2014

    • Author(s)
      D.Shiozawa, Y.Nakai, R.Miura, and S.Matsuda
    • Organizer
      11th International Fatigue Congress (Fatigue 2014)
    • Place of Presentation
      Melbourne, Australia
    • Year and Date
      20140302-07
  • [Presentation] Fatigue of ultra-fine grained α-brass2014

    • Author(s)
      Y.Nakai, T.Imanaka and D.Shiozawa
    • Organizer
      11th International Fatigue Congress (Fatigue 2014)
    • Place of Presentation
      Melbourne, Australia
    • Year and Date
      20140302-07
  • [Presentation] Evaluation of Fatigue Damage by Diffraction Contrast Imaging using Ultra-bright Synchrotron Radiation2013

    • Author(s)
      Y.Nakai, D.Shiozawa, and R.Miura
    • Organizer
      International Conference on Processing & Manufacturing of Advanced Materials (THERMEC'2013)
    • Place of Presentation
      Las Vegas, USA
    • Year and Date
      20131202-06
  • [Presentation] 放射光μCT イメージングによる腐食疲労におけるピットの成長及びき裂発生過程の4D 解析2013

    • Author(s)
      岡田宗大, 塩澤大輝, 中井善一
    • Organizer
      日本材料学会第16回破壊力学シンポジウム
    • Place of Presentation
      熊本県阿蘇郡
    • Year and Date
      20131120-22
  • [Presentation] 高輝度放射光を用いた回折コントラストイメージによるき裂発生過程の結晶組織観察2013

    • Author(s)
      政田尚也, 松田翔太, 塩澤大輝, 中井善一
    • Organizer
      日本材料学会第16回破壊力学シンポジウム
    • Place of Presentation
      熊本県阿蘇郡
    • Year and Date
      20131120-22
  • [Presentation] 水素環境下における繰返し応力がTiNi 形状記憶合金の寿命に及ぼす影響2013

    • Author(s)
      河野久晃,田中拓,中井善一,西本匡志
    • Organizer
      日本機械学会材料力学講演会(M&M2013)
    • Place of Presentation
      岐阜市
    • Year and Date
      20131011-14
  • [Presentation] 放射光μCT イメージングを用いたTi-6Al-4V 内部に発生する微小疲労き裂の検出2013

    • Author(s)
      中山慎也,中村孝,小熊博幸,塩澤大輝,中井善一,上杉健太朗
    • Organizer
      日本機械学会材料力学講演会(M&M2013)
    • Place of Presentation
      岐阜市
    • Year and Date
      20131011-14
  • [Presentation] 放射光μCT 及び小型転動疲労試験機を用いた転動疲労き裂進展過程の観察2013

    • Author(s)
      佐藤一矢,塩澤大輝,根石豊,牧野泰三,中井善一,岡田宗大
    • Organizer
      日本機械学会材料力学講演会(M&M2013)
    • Place of Presentation
      岐阜市
    • Year and Date
      20131011-14
  • [Presentation] 高輝度放射光を用いた回折コントラストトモグラフィによる疲労損傷評価に関する検討2013

    • Author(s)
      松田翔太,政田尚也,塩澤大輝,中井善一,三浦亮太郎
    • Organizer
      日本機械学会材料力学講演会(M&M2013)
    • Place of Presentation
      岐阜市
    • Year and Date
      20131011-14
  • [Presentation] α黄銅超微細結晶粒材の疲労強度2013

    • Author(s)
      中井善一,今中拓人,塩澤大輝
    • Organizer
      日本機械学会材料力学講演会(M&M2013)
    • Place of Presentation
      岐阜市
    • Year and Date
      20131011-14
  • [Presentation] 放射光μCT イメージモデルに基づいた有限要素解析によるねじり疲労き裂進展挙動の評価2013

    • Author(s)
      納庄宏明,塩澤大輝,中井善一
    • Organizer
      日本機械学会関西支部第88期定時総会講演会
    • Place of Presentation
      大阪市
    • Year and Date
      20130316-17
  • [Presentation] 水素吸収がTiNi 形状記憶合金細線の破壊強度に及ぼす影響2013

    • Author(s)
      西本匡志,田中拓,中井善一,宮部成央
    • Organizer
      日本機械学会関西支部 第88期定時総会講演会
    • Place of Presentation
      大阪市
    • Year and Date
      20130316-17
  • [Presentation] 高輝度放射光による三次元結晶マッピング法を用いた多結晶金属組織観察2013

    • Author(s)
      三浦亮太郎,松田翔太,塩澤大輝,中井善一
    • Organizer
      日本機械学会関西支部第88期定時総会講演会
    • Place of Presentation
      大阪市
    • Year and Date
      20130316-17
  • [Presentation] 工業用純鉄細線の引張特性と疲労寿命に及ぼす線径の影響2013

    • Author(s)
      小林亮,田中拓,中井善一,宮部成央,赤穂健太
    • Organizer
      日本機械学会関西支部第88期定時総会講演会
    • Place of Presentation
      大阪市
    • Year and Date
      20130316-17
  • [Presentation] 黄銅超微細結晶粒材作製法の開発とその強度評価2013

    • Author(s)
      今中拓人,堤湧貴,中井善一,塩澤大輝
    • Organizer
      日本機械学会関西支部第88期定時総会
    • Place of Presentation
      大阪市
    • Year and Date
      20130316-17
  • [Presentation] Effect of Loading Frequency on Corrosion Fatigue Crack Growth of Zr-based Bulk Metallic Glass in the Region near Threshold2013

    • Author(s)
      Y.Nakai, T.Koyama, B.He, K.Ueno
    • Organizer
      142nd Annual Meeting & Exhibition (TMS2013)
    • Place of Presentation
      San Antonio, Texas, USA
    • Year and Date
      20130303-07
  • [Presentation] 放射光μCT イメージングを用いた高強度鋼における転動疲労き裂進展挙動の観察2012

    • Author(s)
      塩澤大輝, 岡田宋大, 根石豊, 牧野泰三, 中井善一,福田嘉之
    • Organizer
      日本材料学会第31回疲労シンポジウム
    • Place of Presentation
      横浜市
    • Year and Date
      20121120-21
  • [Presentation] Evaluation of Plastic Strain by Three-Dimensional Grain Mapping Technique Using SPring-82012

    • Author(s)
      R.Miura, D.Shiozawa, Y.Nakai, N.Masada
    • Organizer
      The 5th International Symposium on Designing, Processing and Properties of Advanced Engineering Materials (ISAEM-2012)
    • Place of Presentation
      Toyohashi, Japan
    • Year and Date
      20121105-08
  • [Presentation] Observation of Crack Propagation under Rolling Contact Fatigue in High-Strength Steels by Micro CT Imaging2012

    • Author(s)
      S.Okada, D.Shiozawa, Y.Neishi, T.Makino, Y.Nakai
    • Organizer
      The 5th International Symposium on Designing, Processing and Properties of Advanced Engineering Materials (ISAEM-2012)
    • Place of Presentation
      Toyohashi, Japan
    • Year and Date
      20121105-08
  • [Presentation] Observation of Fatigue Crack Propagation Mode Transition under Cyclic Torsion Using Micro-CT Imaging with Ultra-Bright Synchrotron Radiation2012

    • Author(s)
      Y.Nakai, D.Shiozawa, T.Murakami, and H.Nosho
    • Organizer
      The 4th International Conference on Crack Paths (CP 2012)
    • Place of Presentation
      Gaeta, Italy
    • Year and Date
      20120919-21
  • [Presentation] Evaluation of rolling contact fatigue crack path of high strength steel with artificial defect2012

    • Author(s)
      T.Makino, Y.Neishi, D.Shiozawa, Y.Fukuda and Y.Nakai
    • Organizer
      The 4th International Conference on Crack Paths (CP 2012)
    • Place of Presentation
      Gaeta, Italy
    • Year and Date
      20120919-21
  • [Presentation] Observation of Cracks in Carbon Steel under Contact Rolling Fatigue by Micro CT Imaging using Ultra-bright Synchrotron Radiation2012

    • Author(s)
      D.Shiozawa, Y.Nakai, Y.Fukuda, Y.Neishi, and T.Makino
    • Organizer
      15th International Conference on Experimental Mechanics
    • Place of Presentation
      Porto, Portugal
    • Year and Date
      20120722-27
  • [Presentation] Development of Three-Dimensional Grain Mapping Technique in Spring-8 and Evaluation of Plastic Strain2012

    • Author(s)
      D.Shiozawa, Y.Nakai, Kenta Tsutsumi, Ryotaro Miura Kentaro Kajiwara
    • Organizer
      15th International Conference on Experimental Mechanics
    • Place of Presentation
      Porto, Portugal
    • Year and Date
      20120722-27
  • [Presentation] 結晶3D マッピング法による塑性ひずみ評価法の開2012

    • Author(s)
      塩澤大輝, 三浦亮太郎, 政田尚也, 中井善一
    • Organizer
      日本材料学会第61期学術講演会
    • Place of Presentation
      岡山市
    • Year and Date
      20120525-27
  • [Presentation] 放射光μCT を用いた高強度鋼における転動疲労下のき裂観察2012

    • Author(s)
      福田嘉之,岡田宗大,根石豊,牧野泰三,塩澤大輝,中井善一
    • Organizer
      日本機械学会関西支部第87期定時総会講演会
    • Place of Presentation
      吹田市
    • Year and Date
      20120316-17
  • [Presentation] 高輝度放射光の回折コントラストイメージを用いた三次元結晶マッピング法2012

    • Author(s)
      堤健太,中井善一,塩澤大輝,三浦亮太郎,政田尚也
    • Organizer
      日本機械学会関西支部第87期定時総会講演会
    • Place of Presentation
      吹田市
    • Year and Date
      20120316-17
  • [Presentation] 工業用純鉄細線の疲労損傷に及ぼす線径と負荷方法の影響2012

    • Author(s)
      赤穂健太,宮部成央,槻木佑馬,田中拓,中井善一
    • Organizer
      日本機械学会関西支部第87期定時総会講演会
    • Place of Presentation
      吹田市
    • Year and Date
      20120316-17
  • [Presentation] Environment Assisted Cracking of Zr-based Bulk Metallic Glass in the Region near Threshold2012

    • Author(s)
      Y.Nakai, and T.Koyama
    • Organizer
      141st Annual Meeting & Exhibition (TMS2012)
    • Place of Presentation
      Orlando, FL, USA
    • Year and Date
      20120311-15
    • Invited
  • [Presentation] Effect of Yield Stress on Fatigue Damage in Commercially Pure Iron Thin Wires2011

    • Author(s)
      N.Miyabe, H.Tanaka, K.Ako, and Y.Nakai
    • Organizer
      International Conference on Advanced Technology in Experimental Mechanics 2011 (ATEM'11)
    • Place of Presentation
      Kobe, Japan
    • Year and Date
      20110919-21
  • [Presentation] Observation of Delamination Defects and Cracks in High-strength Steels under Rolling Contact Fatigue by SR Micro CT Imaging2011

    • Author(s)
      D.Shiozawa, Y.Neishi, Y.Fukuda, T.Makino, and Y.Nakai
    • Organizer
      International Conference on Advanced Technology in Experimental Mechanics 2011 (ATEM'11)
    • Place of Presentation
      Kobe, Japan
    • Year and Date
      20110919-21
  • [Presentation] Development of Three-dimensional Grain Mapping Technique Using SPring-82011

    • Author(s)
      D.Shiozawa, K.Tsutsumi, Y.Nakai, and K.Kajiwara
    • Organizer
      International Conference on Advanced Technology in Experimental Mechanics 2011 (ATEM'11)
    • Place of Presentation
      Kobe, Japan
    • Year and Date
      20110919-21
  • [Presentation] Evaluation of Torsional Fatigue Crack Propagation by Synchrotron Radiation Micro-CT Imaging2011

    • Author(s)
      D.Shiozawa, Y.Nakai, T.Murakami, and H.Nosho
    • Organizer
      International Conference on Advanced Technology in Experimental Mechanics 2011 (ATEM'11)
    • Place of Presentation
      Kobe, Japan
    • Year and Date
      20110919-21
  • [Presentation] 放射光μCT を用いた高強度鋼の転動疲労下のき裂検出2011

    • Author(s)
      福田嘉之,塩澤大輝,根石 豊,牧野泰三,中井善一
    • Organizer
      日本機械学会M&M2011 材料力学カンファレンス
    • Place of Presentation
      北九州市
    • Year and Date
      20110706-18
  • [Presentation] Observation of Fatigue Crack Propagation Behavior under Torsional Loading by Using Synchrotron Radiation Micro-CT Imaging2011

    • Author(s)
      D.Shiozawa, Y.Nakai, T.Murakami, and H.Nosho
    • Organizer
      ICM11 (International Conference on Mechanical Behavior of Materials)
    • Place of Presentation
      Lake Como, Italy
    • Year and Date
      20110705-09
  • [Presentation] 高輝度放射光CT によるねじり疲労き裂の進展・分岐挙動の観察と評価2011

    • Author(s)
      塩澤大輝,納庄宏明,村上智宣,中井善一
    • Organizer
      日本材料学会第60期学術講演会
    • Place of Presentation
      吹田市
    • Year and Date
      20110523-26
  • [Presentation] 環境および負荷条件の異なるTiNi 記憶合金細線の水素劣化挙動2011

    • Author(s)
      宮部成央,田中拓,川西翔,西本匡志,中井善一
    • Organizer
      日本材料学会第60期学術講演会
    • Place of Presentation
      吹田市
    • Year and Date
      20110523-26
  • [Presentation] 工業用純鉄細線の疲労寿命に及ぼす降伏現象の影響2011

    • Author(s)
      宮部成央,赤穂健太,田中拓,小林亮太,中井善一
    • Organizer
      日本材料学会第60期学術講演会
    • Place of Presentation
      吹田市
    • Year and Date
      20110523-26
  • [Presentation] Fatigue of Bulk Metallic Glass2011

    • Author(s)
      Yoshikazu Nakai
    • Organizer
      2nd Japan-China Joint Symposium on Fatigue of Engineering Materials and Structures
    • Place of Presentation
      Chengdu, China
    • Year and Date
      2011-10-17
    • Invited
  • [Book] 破壊力学2014

    • Author(s)
      中井善一,久保司郎
    • Publisher
      朝倉書店
  • [Book] 材料力学2013

    • Author(s)
      中井善一,三村耕司,阪上隆英,多田直哉,岩本剛,田中拓
    • Publisher
      朝倉書店
  • [Book] 疲労の基礎, 破壊力学体系-壊れない製品設計へ向けて2012

    • Author(s)
      中井善一(服部敏雄,川田宏之,田川哲哉,東郷敬一郎,中井善一,三浦英生編)
    • Total Pages
      392-402
    • Publisher
      エヌ・ティー・エス
  • [Remarks]

    • URL

      http://www.research.kobe-u.ac.jp/eng-fracture/

URL: 

Published: 2015-06-25  

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