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Dark-field electron holography studies on strain and magnetization: methodology and applications to magnetic materials

Research Project

Project/Area Number 15H04112
Research Category

Grant-in-Aid for Scientific Research (B)

Allocation TypeSingle-year Grants
Section一般
Research Field Physical properties of metals/Metal-base materials
Research InstitutionKyushu University

Principal Investigator

MURAKAMI Yasukazu  九州大学, 工学研究院, 教授 (30281992)

Co-Investigator(Kenkyū-buntansha) 赤瀬 善太郎  東北大学, 多元物質科学研究所, 講師 (90372317)
新津 甲大  国立研究開発法人理化学研究所, 創発物性科学研究センター, 特別研究員 (90733890)
Co-Investigator(Renkei-kenkyūsha) AKASE Zentaro  東北大学, 多元物質科学研究所, 講師 (90372317)
NIITSU Kodai  理化学研究所, 創発物性科学研究センター, 特別研究員 (90733890)
Project Period (FY) 2015-04-01 – 2018-03-31
Project Status Completed (Fiscal Year 2017)
Budget Amount *help
¥16,120,000 (Direct Cost: ¥12,400,000、Indirect Cost: ¥3,720,000)
Fiscal Year 2017: ¥3,770,000 (Direct Cost: ¥2,900,000、Indirect Cost: ¥870,000)
Fiscal Year 2016: ¥3,770,000 (Direct Cost: ¥2,900,000、Indirect Cost: ¥870,000)
Fiscal Year 2015: ¥8,580,000 (Direct Cost: ¥6,600,000、Indirect Cost: ¥1,980,000)
Keywords電子顕微鏡 / 磁性材料 / 磁気イメージング / 歪解析 / 電子線ホログラフィー
Outline of Final Research Achievements

We have developed a method that allows for separation of the crystal-strain information from the electromagnetic information stored in a dark-field electron hologram. The method was applied to a strain analysis of Nd-Fe-B permanent magnet which contained several types of precipitates. The observation provided useful information about the relationship between precipitates and lattice strain in the sintered magnet. This study accordingly demonstrated the usefulness of dark-field electron holography, which can be a tool of strain analysis not only for non-magnetic systems but also magnetic systems.

Report

(4 results)
  • 2017 Annual Research Report   Final Research Report ( PDF )
  • 2016 Annual Research Report
  • 2015 Annual Research Report
  • Research Products

    (15 results)

All 2018 2017 2016 2015

All Journal Article (6 results) (of which Peer Reviewed: 6 results,  Open Access: 1 results,  Acknowledgement Compliant: 2 results) Presentation (9 results) (of which Int'l Joint Research: 9 results,  Invited: 9 results)

  • [Journal Article] Morphology of Phase-separated VO2 Films Deposited on TiO2-(001) Substrate2018

    • Author(s)
      Y. Cho, S. Aritomi, T. Kanki, K. Kinoshita, N. Endo, Y. Kondo, D. Shindo, H. Tanaka, and Y. Murakami
    • Journal Title

      Materials Research Bulletin

      Volume: 102 Pages: 289-293

    • DOI

      10.1016/j.materresbull.2018.02.030

    • Related Report
      2017 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Cellular microstructures superposed on martensite plates in Mn55. 2Ga19. 0Cu25. 8 alloy showing large coercivity2017

    • Author(s)
      R Sawada, T Yamamoto, K Minakuchi, M Nagasako, Y Hayasaka, K Niitsu, Y Cho, R Kainuma, Y Murakami
    • Journal Title

      Scripta Materialia

      Volume: 135 Pages: 33-36

    • DOI

      10.1016/j.scriptamat.2017.03.013

    • Related Report
      2017 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Atomic-resolution evaluation of microsegregation and degree of atomic order at antiphase boundaries in Ni50Mn20In30 Heusler alloy2017

    • Author(s)
      K.Niitsu, K.Minakuchi, X.Xu, M.Nagasako, I.Ohnuma, T.Tanigaki, Y.Murakami, D.Shindo, R.Kainuma
    • Journal Title

      ACTA MATERIALIA

      Volume: 122 Pages: 166-177

    • DOI

      10.1016/j.actamat.2016.09.035

    • Related Report
      2017 Annual Research Report
    • Peer Reviewed / Open Access
  • [Journal Article] Strain Measurement in Ferromagnetic Crystals using Dark-field Electron Holography2016

    • Author(s)
      Y. Murakami, K. Niitsu, S. Kaneko, T. Tanigaki, T.T. Sasaki, Z. Akase, D. Shindo, T. Ohkubo, and K. Hono
    • Journal Title

      Applied Physics Letters

      Volume: 109

    • Related Report
      2016 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Application of strain to orbital-spin-coupled system MnV2O4 at cryogenic temperatures within a transmission electron microscope2016

    • Author(s)
      Y. Murakami, T. Suzuki, Y. Nii, S.Murai, T. Arima, R. Kainuma, and D. Shindo
    • Journal Title

      Microscopy

      Volume: in press Issue: 3 Pages: 223-232

    • DOI

      10.1093/jmicro/dfv377

    • Related Report
      2015 Annual Research Report
    • Peer Reviewed / Acknowledgement Compliant
  • [Journal Article] Strain Measurements from Nd2Fe14B Grains in Sintered Magnets using Artificial Moire Fringes2015

    • Author(s)
      Y. Murakami, T. T. Sasaki, T. Ohkubo and K. Hono
    • Journal Title

      Acta Materialia

      Volume: 101 Pages: 101-106

    • DOI

      10.1016/j.actamat.2015.08.058

    • Related Report
      2015 Annual Research Report
    • Peer Reviewed / Acknowledgement Compliant
  • [Presentation] Toward Ultrahigh Precision of Electron Holography2018

    • Author(s)
      Y. Murakami
    • Organizer
      Sanken International Symposium on AI Evolution in Science and Technology
    • Related Report
      2017 Annual Research Report
    • Int'l Joint Research / Invited
  • [Presentation] Transmission electron microscopy studies of premartensitic phenomena in Ti- and Ni-based alloys2017

    • Author(s)
      Y. Murakami, K. Niitsu, Y. Kimura, R. Kainuma, and D. Shindo
    • Organizer
      International Conference of Martensitic Transformations
    • Related Report
      2017 Annual Research Report
    • Int'l Joint Research / Invited
  • [Presentation] Dark-field electron holography studies on magnetic materials2017

    • Author(s)
      Y. Murakami
    • Organizer
      The 3rd East-Asia Microscopy Conference
    • Related Report
      2017 Annual Research Report
    • Int'l Joint Research / Invited
  • [Presentation] Electron Holography Studies on Interface Magnetism and Lattice Strain in Nd-Fe-B Permanent Magnet2017

    • Author(s)
      Y. Murakami
    • Organizer
      Electron Holography Workshop 2017
    • Related Report
      2016 Annual Research Report
    • Int'l Joint Research / Invited
  • [Presentation] Analysis of Interface Magnetism by Transmission Electron Microscopy2016

    • Author(s)
      Y. Murakami
    • Organizer
      Energy Materials Nanotechnology (EMN) 2016
    • Related Report
      2016 Annual Research Report
    • Int'l Joint Research / Invited
  • [Presentation] Electron Microscopy Studies on Magnetic Nanostructures2016

    • Author(s)
      Y. Murakami
    • Organizer
      Japan-Germany Joint Symposium on Advanced Characterization of Nanostructured Materials for Energy and Environment
    • Related Report
      2016 Annual Research Report
    • Int'l Joint Research / Invited
  • [Presentation] Electron Holography Studies on Magnetic Anomaly in Antiphase Boundaries Produced in Fe-Al Alloy2016

    • Author(s)
      Y. Murakami
    • Organizer
      11th Polish-Japanese Joint Seminar on Micro and Nano Analysis
    • Related Report
      2016 Annual Research Report
    • Int'l Joint Research / Invited
  • [Presentation] Analysis of Electromagnetic Field in Nanostructures2016

    • Author(s)
      Y. Murakami
    • Organizer
      The 36th Annual NANO Testing Symposium
    • Related Report
      2016 Annual Research Report
    • Int'l Joint Research / Invited
  • [Presentation] Interface Magnetism Studied by Electron Holography with Multiple-biprisms2015

    • Author(s)
      Y. Murakami
    • Organizer
      Microscopy & Microanalysis 2015
    • Place of Presentation
      Portland, USA
    • Year and Date
      2015-08-03
    • Related Report
      2015 Annual Research Report
    • Int'l Joint Research / Invited

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Published: 2015-04-16   Modified: 2019-03-29  

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