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High-Speed Cyclic Indentation Test and Fracture Mechanisms of DLC coatings

Research Project

Project/Area Number 15K21120
Research Category

Grant-in-Aid for Young Scientists (B)

Allocation TypeMulti-year Fund
Research Field Materials/Mechanics of materials
Design engineering/Machine functional elements/Tribology
Research InstitutionKyoto Institute of Technology

Principal Investigator

Nakamura Morimasa  京都工芸繊維大学, 機械工学系, 准教授 (00464230)

Project Period (FY) 2015-04-01 – 2018-03-31
Project Status Completed (Fiscal Year 2017)
Budget Amount *help
¥4,160,000 (Direct Cost: ¥3,200,000、Indirect Cost: ¥960,000)
Fiscal Year 2017: ¥650,000 (Direct Cost: ¥500,000、Indirect Cost: ¥150,000)
Fiscal Year 2016: ¥2,600,000 (Direct Cost: ¥2,000,000、Indirect Cost: ¥600,000)
Fiscal Year 2015: ¥910,000 (Direct Cost: ¥700,000、Indirect Cost: ¥210,000)
KeywordsDLC膜 / 強度 / 評価 / 破壊 / DLC / ラマン / ドライコーティング / 損傷 / 繰り返し / 面圧 / 表面改質
Outline of Final Research Achievements

As a new strength evaluation method for hard coatings such as Diamond-like Carbon (DLC), the cyclic indentation test method using ball indenter has been developed. And its test rig has also been fabricated. DLC coatings, which were prepared with UBM sputtering, were used in order to find validity of this test. Over 10000 times of indentations made DLC coating fracture on substrates under approximately 2.6 GPa of contact pressure and 120 per minute. Changing DLC coatings characteristics after the tests were found to be clear by Raman spectroscopy analysis for the indentation tracks.
On the other hand, the other test rig for 10 raised to the power of 7 times indentations within short time has also been developed and fabricated. DLC fracture was also found using it.

Report

(4 results)
  • 2017 Annual Research Report   Final Research Report ( PDF )
  • 2016 Research-status Report
  • 2015 Research-status Report
  • Research Products

    (12 results)

All 2018 2017 2015

All Journal Article (4 results) (of which Peer Reviewed: 3 results,  Acknowledgement Compliant: 2 results) Presentation (8 results) (of which Int'l Joint Research: 4 results)

  • [Journal Article] CYCLIC INDENTATION TEST FOR EVALUATING STRENGTH OF DLC FILMS2017

    • Author(s)
      Morimasa NAKAMURA, Ryohei KURIHARA, Fumihiro NAKAYAMA, Ken-ichi MIURA, Jyunpei KOBATA
    • Journal Title

      Proceedings of The JSME International Conference on Motion and Power Transmissions

      Volume: Vol. Ⅱ Pages: 388-392

    • NAID

      130006008620

    • Related Report
      2017 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Effects of Indentation Cycles on Damage of DLC Films through Cyclic Indentation Tests2017

    • Author(s)
      Morimasa Nakamura, Ryohei Kurihara, Ken-ichi Miura, Jyunpei Kobata and Takayuki Nagataki
    • Journal Title

      Proceedings of The 7th International Conference on Manufacturing, Machine Design and Tribology

      Volume: なし Pages: 24-24

    • Related Report
      2017 Annual Research Report
  • [Journal Article] CYCLIC INDENTATION TEST FOR EVALUTING STRENGTH OF DLC FILMS2017

    • Author(s)
      Morimasa NAKAMURA, Ryohei KURIHARA, Fumihiro NAKAYAMA, Ken-ichi MIURA, Jyunpei KOBATA
    • Journal Title

      Proceedings of The JSME International Conference on Motion and Power Transmissions

      Volume: - Pages: 388-392

    • Related Report
      2016 Research-status Report
    • Peer Reviewed / Acknowledgement Compliant
  • [Journal Article] Effects of Indentation Cycles on Damage of DLC Films through Cyclic Indentation Tests2017

    • Author(s)
      Morimasa Nakamura, Ryohei Kurihara, Ken-ichi Miura, Jyunpei Kobata, Takayuki Nagataki
    • Journal Title

      Proceedings The 7th International Conference on Manufacturing, Machine Design and Tribology

      Volume: - Pages: 24-24

    • Related Report
      2016 Research-status Report
    • Peer Reviewed / Acknowledgement Compliant
  • [Presentation] 繰返し押付け試験により生じたDLC 膜の損傷観察と 損傷DLC 膜のラマン分光分析2018

    • Author(s)
      髙川祐加
    • Organizer
      日本塑性加工学会関西支部 平成29年度 卒業研究発表会
    • Related Report
      2017 Annual Research Report
  • [Presentation] Effects of Indentation Cycles on Damage of DLC Films through Cyclic Indentation Tests2017

    • Author(s)
      Morimasa Nakamura, Ryohei Kurihara, Ken-ichi Miura, Jyunpei Kobata, Takayuki Nagataki
    • Organizer
      The 7th International Conference on Manufacturing, Machine Design and Tribology
    • Place of Presentation
      韓国
    • Year and Date
      2017-04-19
    • Related Report
      2016 Research-status Report
    • Int'l Joint Research
  • [Presentation] CYCLIC INDENTATION TEST FOR EVALUTING STRENGTH OF DLC FILMS2017

    • Author(s)
      Morimasa NAKAMURA, Ryohei KURIHARA, Fumihiro NAKAYAMA, Ken-ichi MIURA, Jyunpei KOBATA
    • Organizer
      MPT2017-Kyoto The JSME International Conference on Motion and Power Transmissions
    • Place of Presentation
      京都市
    • Year and Date
      2017-02-28
    • Related Report
      2016 Research-status Report
    • Int'l Joint Research
  • [Presentation] CYCLIC INDENTATION TEST FOR EVALUATING STRENGTH OF DLC FILMS2017

    • Author(s)
      中村守正
    • Organizer
      The JSME International Conference on Motion and Power Transmissions MPT2017
    • Related Report
      2017 Annual Research Report
    • Int'l Joint Research
  • [Presentation] Effects of Indentation Cycles on Damage of DLC Films through Cyclic Indentation Tests2017

    • Author(s)
      中村守正
    • Organizer
      The 7th International Conference on Manufacturing, Machine Design and Tribology
    • Related Report
      2017 Annual Research Report
    • Int'l Joint Research
  • [Presentation] 繰返し押付け試験によるDLC膜の強度評価 押付け速度の影響2017

    • Author(s)
      中村守正
    • Organizer
      2017 年度砥粒加工学会 学術講演会
    • Related Report
      2017 Annual Research Report
  • [Presentation] 樹脂歯車運転試験によるDLC 膜の強度評価(高速度カメラ映像による損傷モードの把握)2015

    • Author(s)
      山極洸士,中村守正,射場大輔,森脇一郎
    • Organizer
      2015 年度日本機械学会年次大会
    • Place of Presentation
      北海道大学
    • Year and Date
      2015-09-14
    • Related Report
      2015 Research-status Report
  • [Presentation] DLC膜の強度評価を目的とした歯車運転試験の適用可能性2015

    • Author(s)
      中村守正,山極洸士,三浦健一,小畠淳平,長瀧敬行,射場大輔,森脇一郎
    • Organizer
      トライボロジー会議2015春姫路
    • Place of Presentation
      姫路商工会議所
    • Year and Date
      2015-05-29
    • Related Report
      2015 Research-status Report

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Published: 2015-04-16   Modified: 2019-03-29  

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