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Clarification of crystallization mechanisms through evaluating a residual amorphous state

Research Project

Project/Area Number 16K18227
Research Category

Grant-in-Aid for Young Scientists (B)

Allocation TypeMulti-year Fund
Research Field Physical properties of metals/Metal-base materials
Research InstitutionTohoku University

Principal Investigator

Yamada Rui  東北大学, 学際科学フロンティア研究所, 助教 (40706892)

Research Collaborator TANAKA Naoyuki  東北大学, 大学院工学研究科, 院生
GUO Wei  東北大学, 学際科学フロンティア研究所, 教育研究支援者
SAIDA Junji  東北大学, 学際科学フロンティア研究所, 教授
Project Period (FY) 2016-04-01 – 2018-03-31
Project Status Completed (Fiscal Year 2017)
Budget Amount *help
¥4,160,000 (Direct Cost: ¥3,200,000、Indirect Cost: ¥960,000)
Fiscal Year 2017: ¥910,000 (Direct Cost: ¥700,000、Indirect Cost: ¥210,000)
Fiscal Year 2016: ¥3,250,000 (Direct Cost: ¥2,500,000、Indirect Cost: ¥750,000)
Keywords残留アモルファス構造 / 結晶化 / 残留アモルファス状態 / 急冷装置機構の構築 / ランダム構造の制御 / 結晶化初期段階の形成 / 金属ガラス / 残留アモルファス
Outline of Final Research Achievements

Rapid cooling system for bulk meallic glassy samples was constructed and Zr,Pd based samples with various random structures were successfully prepared. TEM observations were conducted to observe the initial nucleation and crystal growth stages in metallic glasses and viscoelastic measurements were performed to evaluate the residual amorphous states. It was difficult to clarify which relaxation regions relates to each crystallization step, but we got another new findings cocerning the crystallization of metallic glasses. We revealed for the first time that the crystallization and rejuvenation area, which are apparently oposite energy state regions, can be coexisted in the glassy structure.
Our findings will provide beneficial information for the crystallization studies of metallic glasses.

Report

(3 results)
  • 2017 Annual Research Report   Final Research Report ( PDF )
  • 2016 Research-status Report
  • Research Products

    (4 results)

All 2017 2016

All Journal Article (1 results) (of which Peer Reviewed: 1 results,  Open Access: 1 results) Presentation (3 results) (of which Int'l Joint Research: 1 results)

  • [Journal Article] Crystallization Behavior of Thermally Rejuvenated Zr<sub>50</sub>Cu<sub>40</sub>Al<sub>10</sub> Metallic Glass2017

    • Author(s)
      Rui Yamada, Naoyuki Tanaka, Wei Guo, Junji Saida
    • Journal Title

      MATERIALS TRANSACTIONS

      Volume: 58 Issue: 10 Pages: 1463-1468

    • DOI

      10.2320/matertrans.MAW201703

    • NAID

      130006096743

    • ISSN
      1345-9678, 1347-5320
    • Related Report
      2017 Annual Research Report
    • Peer Reviewed / Open Access
  • [Presentation] 回復熱処理を利用した金属ガラスのガラス状態と結晶化との関係性の検討2017

    • Author(s)
      山田 類
    • Organizer
      第160回 日本金属学会春季講演大会
    • Place of Presentation
      首都大学東京(東京都八王子市南大沢)
    • Year and Date
      2017-03-15
    • Related Report
      2016 Research-status Report
  • [Presentation] 回復熱処理を利用した金属ガラスのガラス状態と結晶化との関係性の検討2017

    • Author(s)
      山田 類, 田中 直行, 郭 威, 才田 淳治
    • Organizer
      日本金属学会
    • Related Report
      2017 Annual Research Report
  • [Presentation] Rejuvenation mechanism and crystallization behavior of recovery annealed Zr-based metallic glass2016

    • Author(s)
      Rui Yamada
    • Organizer
      2016 MRS Fall Meeting & Exhibit
    • Place of Presentation
      Boston(アメリカ)
    • Year and Date
      2016-11-27
    • Related Report
      2016 Research-status Report
    • Int'l Joint Research

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Published: 2016-04-21   Modified: 2019-03-29  

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