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A trial approach for tomographic microstructure examination towards evaluation of tensor quantity

Research Project

Project/Area Number 18K18944
Research Category

Grant-in-Aid for Challenging Research (Exploratory)

Allocation TypeMulti-year Fund
Review Section Medium-sized Section 26:Materials engineering and related fields
Research InstitutionKyoto University

Principal Investigator

OKUDA HIROSHI  京都大学, 工学研究科, 教授 (50214060)

Project Period (FY) 2018-06-29 – 2021-03-31
Project Status Completed (Fiscal Year 2020)
Budget Amount *help
¥6,240,000 (Direct Cost: ¥4,800,000、Indirect Cost: ¥1,440,000)
Fiscal Year 2020: ¥910,000 (Direct Cost: ¥700,000、Indirect Cost: ¥210,000)
Fiscal Year 2019: ¥1,690,000 (Direct Cost: ¥1,300,000、Indirect Cost: ¥390,000)
Fiscal Year 2018: ¥3,640,000 (Direct Cost: ¥2,800,000、Indirect Cost: ¥840,000)
Keywords放射光小角散乱法 / トモグラフィー / 析出強化材料 / 軽金属複合材料 / 拡散相変態 / 定量散乱トモグラフィー / SAXS絶対測定 / 組成傾斜材料 / 異方性散乱体 / ナノ組織分布 / 放射光小角散乱 / 散乱トモグラフィー / 複合材料 / 放射光 / 異方性散乱回折 / ピンクビーム / 軽金属合金 / 散乱トモグラフ / ナノ構造分布 / 小角散乱 / ベクトルトモグラフィー / 金属基複合材料
Outline of Final Research Achievements

Small-Angle X-ray Scattering tomography has been applied to multilayered precipitation hardened sample or pillar sample with concentration gradient, to assess quantitative information of the distribution of precipitation nanostructures, and extended to weakly anisotropic samples. As the first step, quantitative SAXS tomography of target light-metal composite sample with isotropic nanoprecipitates have been examined to realize SAXS tomography with absolute units. Then, brute-force measurements for the weakly anisotropic samples have been tried to examine if such natural extension of isotropic SAXS tomography works out in principle. We concluded that with precise control of stages, it is in principle technically possible to perform SAXS absolute measurements for such materials, but with huge amount of measurement time. For

Academic Significance and Societal Importance of the Research Achievements

本研究の前半部分では、接合や傾斜組成といったマクロな不均一構造を持つ構造材料の内部のナノ構造分布を非破壊で評価することができる散乱トモグラフィー法の定量化を金属材料に対して実現するという点で、これまでの材料試験評価法で抜け落ちていたスケールである、ナノスケール構造のマクロ領域にわたる分布状況の評価を実現するという意義を持ち、後半部分でその実用材への拡張に不可欠な展開の考え方を検討した。

Report

(4 results)
  • 2020 Annual Research Report   Final Research Report ( PDF )
  • 2019 Research-status Report
  • 2018 Research-status Report
  • Research Products

    (11 results)

All 2021 2020 2019 Other

All Journal Article (2 results) (of which Peer Reviewed: 2 results,  Open Access: 2 results) Presentation (8 results) (of which Int'l Joint Research: 3 results) Remarks (1 results)

  • [Journal Article] Nanostructure Distribution and Strengthening Mechanisms in the Interface Regions of Al–Zn/Al–Mg Multilayered Composites2021

    • Author(s)
      S. Lin, H.Okuda, K.Matsumoto, M.Yamaguchi, K.Sato
    • Journal Title

      MATERIALS TRANSACTIONS

      Volume: 62 Issue: 5 Pages: 603-609

    • DOI

      10.2320/matertrans.MT-M2020312

    • NAID

      130008029726

    • ISSN
      1345-9678, 1347-5320
    • Year and Date
      2021-05-01
    • Related Report
      2020 Annual Research Report
    • Peer Reviewed / Open Access
  • [Journal Article] Small-angle scattering tomoguraphy of precipitation-hardened multilayer Al-Al-Zn-Al model alloys2019

    • Author(s)
      H.Okuda,S.Lin,Y.Nishikawa
    • Journal Title

      Applied Physics Express

      Volume: 12 Pages: 105503-105503

    • Related Report
      2019 Research-status Report
    • Peer Reviewed / Open Access
  • [Presentation] SAXS tomography of precipitation hardened multilayer Al alloy sheets2021

    • Author(s)
      S.Lin, H.Okuda, Y.Nishikawa
    • Organizer
      TMS2021
    • Related Report
      2020 Annual Research Report
    • Int'l Joint Research
  • [Presentation] 析出強化複層Al材料における小角トモグラフィー測定2021

    • Author(s)
      林杉 常盤大樹 奥田浩司 増永啓康 加部泰三
    • Organizer
      日本金属学会2021年春季大会
    • Related Report
      2020 Annual Research Report
  • [Presentation] マイクロビームX線を用いたAl/Al-Zn積層材における トモグラフィー再構成の定量化の検討2021

    • Author(s)
      林杉 常盤大樹 奥田浩司 増永啓康 加部泰三 櫻井伸一
    • Organizer
      軽金属学会2021年春季大会
    • Related Report
      2020 Annual Research Report
  • [Presentation] Microstructure analysis of graded interface layers in a model muotilayer Al/AlZn/Al by scanning microbeam small-angle X-ray scattering measurements2020

    • Author(s)
      S.Lin H.Okuda, K.Matsumoto, K.Sato
    • Organizer
      TMS2020
    • Related Report
      2019 Research-status Report
    • Int'l Joint Research
  • [Presentation] Al/Al-Zn粗結晶積層材量の組成傾斜領域における組織解析2019

    • Author(s)
      林杉 奥田浩司 松本克史 佐藤和史
    • Organizer
      日本金属学会
    • Related Report
      2019 Research-status Report
  • [Presentation] Nanostructure distribution analysis in multilayered aluminium alloys by conbined use of scalar tomography and scanning small-angle scattering2019

    • Author(s)
      S.Lin H.Okuda,Y.Nishikawa
    • Organizer
      MRM2019
    • Related Report
      2019 Research-status Report
    • Int'l Joint Research
  • [Presentation] アルミニウム複合潜在中のナノ組織分布のトモグラフィーによる解析法の検討2019

    • Author(s)
      林杉 奥田浩司 松本克史 佐藤和史
    • Organizer
      軽金属学会関西支部
    • Related Report
      2019 Research-status Report
  • [Presentation] マイクロビーム走査/再構成法によるアルミニウム合金のナノ組織分布の評価2019

    • Author(s)
      奥田浩司 林杉 西川幸宏
    • Organizer
      放射光学会年会
    • Related Report
      2018 Research-status Report
  • [Remarks] (研究室研究内容HP)

    • URL

      https://mcmd.mtl.kyoto-u.ac.jp

    • Related Report
      2020 Annual Research Report

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Published: 2018-07-25   Modified: 2022-01-27  

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