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Effects of high pressure hydrogen on materials failure studied By a new simple testing method.

Research Project

Project/Area Number 20360321
Research Category

Grant-in-Aid for Scientific Research (B)

Allocation TypeSingle-year Grants
Section一般
Research Field Structural/Functional materials
Research InstitutionNational Institute for Materials Science

Principal Investigator

OGATA Toshio  National Institute for Materials Science, 材料信頼性センター, センター長 (20354243)

Co-Investigator(Kenkyū-buntansha) SHIBATA Kouji  独立行政法人物質・材料研究機構, 材料信頼性センター, NIMS特別研究員 (90011121)
YURI Tetsumi  独立行政法人物質・材料研究機構, 材料信頼性センター, 主任研究員 (10354242)
ONO Yoshinori  独立行政法人物質・材料研究機構, 材料信頼性センター, 主任研究員 (90354240)
Project Period (FY) 2008 – 2010
Project Status Completed (Fiscal Year 2010)
Budget Amount *help
¥17,290,000 (Direct Cost: ¥13,300,000、Indirect Cost: ¥3,990,000)
Fiscal Year 2010: ¥3,510,000 (Direct Cost: ¥2,700,000、Indirect Cost: ¥810,000)
Fiscal Year 2009: ¥4,160,000 (Direct Cost: ¥3,200,000、Indirect Cost: ¥960,000)
Fiscal Year 2008: ¥9,620,000 (Direct Cost: ¥7,400,000、Indirect Cost: ¥2,220,000)
Keywords強度 / 靭性 / 破壊 / 疲労 / クリープ / 応力腐食割れ / 超塑性 / 水素脆性 / 金属材料 / ステンレス鋼 / 水素環境脆化 / 水素分析 / 応力の影響
Research Abstract

A very simple and safe mechanical properties testing procedure to evaluate hydrogen environment embrittlement (HEE) in the environment of high pressure and low temperature hydrogen has been developed. In this method the high-pressure hydrogen environment is produced inside the hole in the specimen. With this testing method, effects of HEE on the tensile properties for austenitic stainless steels and movement of hydrogen gas just before the specimen failure were investigated.
The effect of HEE increased with hydrogen pressure and the decrease of temperature, however, it decreased below 190K and almost disappeared at cryogenic temperatures, below 120K even in 70MPa. Although it was assumed that hydrogen would be moved abruptly just before the specimen failure, no hydrogen was detected before th failure. Through the discussion using computer simulation, it is considered that even aα'b.c.c. phase, concentration of hydrogen decreased before the specimensurfce.

Report

(4 results)
  • 2010 Annual Research Report   Final Research Report ( PDF )
  • 2009 Annual Research Report
  • 2008 Annual Research Report
  • Research Products

    (33 results)

All 2011 2010 2009 2008 Other

All Journal Article (14 results) (of which Peer Reviewed: 14 results) Presentation (16 results) Book (1 results) Remarks (1 results) Patent(Industrial Property Rights) (1 results)

  • [Journal Article] 構造材料の極限環境での特性評価及び国際標準化2010

    • Author(s)
      緒形俊夫
    • Journal Title

      ふぇらむ 15巻

      Pages: 436-440

    • Related Report
      2010 Final Research Report
    • Peer Reviewed
  • [Journal Article] HYDROGEN EMBRITTLEMENT EVALUATION IN FATIGUE PROPERTIES OF STAINLESS STEEL SUS304L AT CRYOGENIC TEMPERATURES2010

    • Author(s)
      緒形俊夫
    • Journal Title

      ADVANCES IN CRYOGENIC ENGINEERING 56巻

      Pages: 25-32

    • Related Report
      2010 Final Research Report
    • Peer Reviewed
  • [Journal Article] 社会を支える金属材料の機械的特性試験2010

    • Author(s)
      緒形俊夫
    • Journal Title

      標準化と品質管理 63巻

      Pages: 5-7

    • Related Report
      2010 Final Research Report
    • Peer Reviewed
  • [Journal Article] 構造材料の極限環境での特性評価及び国際標準化2010

    • Author(s)
      緒形俊夫
    • Journal Title

      ふぇらむ

      Volume: 15 Pages: 436-440

    • Related Report
      2010 Annual Research Report
    • Peer Reviewed
  • [Journal Article] 社会を支える金属材料の機械的特性試験2010

    • Author(s)
      緒形俊夫
    • Journal Title

      標準化と品質管理

      Volume: 63 Pages: 5-7

    • Related Report
      2010 Annual Research Report
    • Peer Reviewed
  • [Journal Article] HYDROGEN EMBRITTLEMENT EVALUATION IN FATIGUE PROPERTIES OF STAINLESS STEEL SUS304L AT CRYOGENIC TEMPERATURES2010

    • Author(s)
      T.Ogata
    • Journal Title

      ADVANCES IN CRYOGENIC ENGINEERING MATERIALS 56

      Pages: 25-32

    • Related Report
      2009 Annual Research Report
    • Peer Reviewed
  • [Journal Article] 液体水素中における300系ステンレス鋼の引張変形挙動の計算機シミュレーション2009

    • Author(s)
      柴田浩司、緒形俊夫、由利哲美、A.Nyilas、藤井秀樹、大宮慎一
    • Journal Title

      圧力技術 47巻

      Pages: 70-77

    • NAID

      10024827144

    • Related Report
      2010 Final Research Report
    • Peer Reviewed
  • [Journal Article] 液体水素中における300系ステンレス鋼の引張変形挙動の計算機シミュレーション2009

    • Author(s)
      柴田浩司、緒形俊夫、由利哲美、A.Nyilas、藤井秀樹、大宮慎一
    • Journal Title

      圧力技術 47

      Pages: 70-77

    • NAID

      10024827144

    • Related Report
      2009 Annual Research Report
    • Peer Reviewed
  • [Journal Article] HYDROGEN EMBRITTLEMENT EVALUATION IN TENSILE PROPERTIES OF STAINLESS STEELS AT CRYOGENIC TEMPERATURE2008

    • Author(s)
      緒形俊夫
    • Journal Title

      ADVANCES IN CRYOGENIC ENGINEERING 54巻

      Pages: 124-131

    • Related Report
      2010 Final Research Report
    • Peer Reviewed
  • [Journal Article] Ti-5Al-2.5Sn ELI合金鍛造材における極低温疲労破壊起点部の結晶方位解析2008

    • Author(s)
      小野嘉則,出村雅彦,由利哲美、緒形俊夫,松岡三郎,堀秀輔
    • Journal Title

      機械学会論文集A A74巻

      Pages: 329-334

    • NAID

      110006643454

    • Related Report
      2010 Final Research Report
    • Peer Reviewed
  • [Journal Article] 簡便な水素環境試験法によるステンレス鋼の低温での特性評価2008

    • Author(s)
      緒形俊夫
    • Journal Title

      圧力技術 46巻

      Pages: 200-204

    • NAID

      10024273862

    • Related Report
      2010 Final Research Report
    • Peer Reviewed
  • [Journal Article] 簡便な水素環境試験法によるステンレス鋼の低温での特性評価2008

    • Author(s)
      緒形俊夫
    • Journal Title

      圧力技術 46

      Pages: 200-204

    • NAID

      10024273862

    • Related Report
      2008 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Ti-5Al-2.5Sn ELI合金鍛造材における極低温疲労破壊起点部の結晶方位解析2008

    • Author(s)
      小野嘉則, 出村雅彦, 由利哲美, 緒形俊夫, 松岡三郎, 堀秀輔
    • Journal Title

      機械学会論文集A A74

      Pages: 329-334

    • NAID

      110006643454

    • Related Report
      2008 Annual Research Report
    • Peer Reviewed
  • [Journal Article] HYDROGEN EMBRITTLEMENT EVALUATION IN TENSILE PROPERTIES OF STAINLESS STEELS AT CRYOGENIC TEMPERATURES2008

    • Author(s)
      T. Ogata
    • Journal Title

      ADVANCES IN CRYOGENIC ENGINEERING 54

      Pages: 124-131

    • Related Report
      2008 Annual Research Report
    • Peer Reviewed
  • [Presentation] Materials Safety for High-Pressure Hydrogen Storage for Fuel Cell Vehicles2010

    • Author(s)
      緒形俊夫、横川清志
    • Organizer
      韓国機械学会
    • Place of Presentation
      韓国・済州島(招待講演)
    • Year and Date
      2010-11-05
    • Related Report
      2010 Final Research Report
  • [Presentation] 液体水素中におけるTi-6Al-4V ELI合金の強度と靱性2010

    • Author(s)
      由利哲美,小野嘉則,緒形俊夫,砂川英生
    • Organizer
      日本金属学会
    • Place of Presentation
      北海道大学
    • Year and Date
      2010-09-27
    • Related Report
      2010 Final Research Report
  • [Presentation] 液体水素中におけるTi-6Al-4V ELI合金の強度と靱性2010

    • Author(s)
      由利哲美, 小野嘉則, 緒形俊夫, 砂川英生
    • Organizer
      日本金属学会講演
    • Place of Presentation
      北海道大学(北海道)
    • Year and Date
      2010-09-27
    • Related Report
      2010 Annual Research Report
  • [Presentation] 構造材料の極限環境での特性評価2010

    • Author(s)
      緒形俊夫
    • Organizer
      日本鉄鋼協会第159回講演大会
    • Place of Presentation
      筑波大学,つくば市(招待講演:浅田賞受賞講演)
    • Related Report
      2010 Final Research Report
  • [Presentation] 宇宙関連材料とNIMS材料データシート2010

    • Author(s)
      緒形俊夫
    • Organizer
      先進材料・非破壊計測技術シンポジウム
    • Place of Presentation
      産総研,つくば市(招待講演)
    • Related Report
      2010 Final Research Report
  • [Presentation] Materials Safety for High-Pressure Hydrogen Storage for Fuel Cell Vehicles2010

    • Author(s)
      緒形俊夫、横川清志
    • Organizer
      韓国機械学会
    • Place of Presentation
      韓国・済州島(韓国)
    • Related Report
      2010 Annual Research Report
  • [Presentation] 構造材料の極限環境での特性評価(招待講演:浅田賞受賞講演)2010

    • Author(s)
      緒形俊夫
    • Organizer
      日本鉄鋼協会第159回講演大会
    • Place of Presentation
      筑波大学,つくば市
    • Related Report
      2009 Annual Research Report
  • [Presentation] 宇宙関連材料とNIMS材料データシート(招待講演)2010

    • Author(s)
      緒形俊夫
    • Organizer
      先進材料・非破壊計測技術シンポジウム
    • Place of Presentation
      産総研,つくば市
    • Related Report
      2009 Annual Research Report
  • [Presentation] 準安定オーステナイト系ステンレス鋼の高圧水素ガスによる脆化の温度依存性2009

    • Author(s)
      柴田浩司,緒形俊夫,由利哲美,小野嘉則
    • Organizer
      2009年春季低温工学・超電導学会
    • Place of Presentation
      早稲田大学,東京都
    • Related Report
      2010 Final Research Report 2009 Annual Research Report
  • [Presentation] YDROGEN EMBRITTLEMENT EVALUATION IN FATIGUE PROPERTIES OF STAINLESS STEEL SUS304L AT CRYOGENIC TEMPERATURES2009

    • Author(s)
      T.Ogata
    • Organizer
      International Cryogenic Materials Conference 2009
    • Place of Presentation
      ツーソン国際会議場,アリゾナ州、米国
    • Related Report
      2009 Annual Research Report
  • [Presentation] 液体水素中におけるCP Tiのセレーションに及ぼす核沸騰・膜沸騰遷移挙動の影響2008

    • Author(s)
      柴田浩司,緒形俊夫,由利哲美, 他
    • Organizer
      2008年秋季低温工学・超電導学会
    • Place of Presentation
      高知市文化プラザかるぽーと,高知市
    • Related Report
      2010 Final Research Report 2008 Annual Research Report
  • [Presentation] 小型冷凍機を用いた極低温での高圧水素環境脆性評価試験2008

    • Author(s)
      緒形俊夫
    • Organizer
      2008年秋季低温工学・超電導学会
    • Place of Presentation
      高知市文化プラザかるぽーと,高知市
    • Related Report
      2010 Final Research Report 2008 Annual Research Report
  • [Presentation] 工業用純チタンの液体水素中における変形挙動の計算機シミュレーションによる解析2008

    • Author(s)
      柴田浩司,緒形俊夫,由利哲美, 他
    • Organizer
      日本鉄鋼協会第156回秋季講演大会
    • Place of Presentation
      熊本大学,熊本市
    • Related Report
      2010 Final Research Report 2008 Annual Research Report
  • [Presentation] 簡便法によるオーステナイト系ステンレス鋼の低温疲労特性に及ぼす高圧水素の影響2008

    • Author(s)
      緒形俊夫
    • Organizer
      日本鉄鋼協会第156回秋季講演大会
    • Place of Presentation
      熊本大学,熊本市
    • Related Report
      2010 Final Research Report 2008 Annual Research Report
  • [Presentation] SIMPLE EVALUATION OF HYDROGEN ENVIRONMENT EMBRITTLEMENT OF STAINLESS STEELS AT CRYOGENIC TEMPERATURE2008

    • Author(s)
      緒形俊夫
    • Organizer
      ICEC22-ICMC2008
    • Place of Presentation
      COEX Convention & Exhibition Centerソウル,韓国
    • Related Report
      2010 Final Research Report
  • [Presentation] SIMPLE EVALUATION OF HYDROGEN ENVIRONMENT EMBRITTLEMENT OF STAINLESS STEELS AT CRYOGENIC TEMPERATURE2008

    • Author(s)
      T. Ogata
    • Organizer
      ICEC22-ICMC2008
    • Place of Presentation
      COEX Convention, & Exhibition Center ソウル,韓国
    • Related Report
      2008 Annual Research Report
  • [Book] チタンの基礎・加工と最新応用技術-極低温特性応用2010

    • Author(s)
      緒形俊夫, 他
    • Total Pages
      341
    • Publisher
      シーエムシー出版
    • Related Report
      2009 Annual Research Report
  • [Remarks] ホームページ等

    • URL

      http://www.nims.go.jp/cmg

    • Related Report
      2010 Final Research Report
  • [Patent(Industrial Property Rights)] 材料試験片及びその製造方法2011

    • Inventor(s)
      緒形俊夫
    • Industrial Property Rights Holder
      独立行政法人物質・材料研究機構
    • Industrial Property Number
      2006-060027
    • Acquisition Date
      2011-03-11
    • Related Report
      2010 Final Research Report

URL: 

Published: 2008-04-01   Modified: 2016-04-21  

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