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Analysis of polymer dynamics by in-situ NMR measurements.

Research Project

Project/Area Number 20550106
Research Category

Grant-in-Aid for Scientific Research (C)

Allocation TypeSingle-year Grants
Section一般
Research Field Polymer chemistry
Research InstitutionGunma University

Principal Investigator

YAMANOBE Takeshi  Gunma University, 大学院・工学研究科, 教授 (40183983)

Project Period (FY) 2008 – 2010
Project Status Completed (Fiscal Year 2010)
Budget Amount *help
¥5,070,000 (Direct Cost: ¥3,900,000、Indirect Cost: ¥1,170,000)
Fiscal Year 2010: ¥1,040,000 (Direct Cost: ¥800,000、Indirect Cost: ¥240,000)
Fiscal Year 2009: ¥1,040,000 (Direct Cost: ¥800,000、Indirect Cost: ¥240,000)
Fiscal Year 2008: ¥2,990,000 (Direct Cost: ¥2,300,000、Indirect Cost: ¥690,000)
KeywordsNMR / 高分子構造 / 運動状態解析 / in-situ / 高分子
Research Abstract

In this research, in-situ NMR system which can measure relaxation times under stress was developed in order to analyze dynamic behavior during processing. Especially, dynamics during drawing can be measured. Control system of temperature by infrared radiation is also developed. This infrared radiation control system can heat the local part of samples. The new parameter which is related to the relaxation parameters is presented and applicability of this parameter is confirmed.

Report

(4 results)
  • 2010 Annual Research Report   Final Research Report ( PDF )
  • 2009 Annual Research Report
  • 2008 Annual Research Report
  • Research Products

    (22 results)

All 2010 2009 2008

All Journal Article (4 results) (of which Peer Reviewed: 4 results) Presentation (17 results) Book (1 results)

  • [Journal Article] Structure and curing mechanism of high-orhto and random novolac resins as studied by NMR2010

    • Author(s)
      Masahiro Nomoto, Tadashi Komoto, Takeshi Yamanobe
    • Journal Title

      Journal of Molecular Structure Vol.976, No.1-3

      Pages: 419-426

    • Related Report
      2010 Final Research Report
    • Peer Reviewed
  • [Journal Article] Precise side-chain conformation analysis of L-phenylalanine in α-helical polypeptide by quantum chemical calculation and 13C CPMAS NMR measurement2010

    • Author(s)
      Subaru Niimura, Junya Suzuki, Hiromichi Kurosu, Takeshi Yamanobe, Akira Shoji
    • Journal Title

      Journal of Molecular structure Vol.969, No.1-3

      Pages: 40-47

    • Related Report
      2010 Final Research Report
    • Peer Reviewed
  • [Journal Article] Structure and curing mechanism of high-ortho and random novolac resinsas studied by NMR2010

    • Author(s)
      Masahiro Nomoto, Yukio Fujikawa, Tadashi Komoto, Takeshi Yamanobe
    • Journal Title

      J.Mol.Struct.

      Volume: 976 Pages: 419-426

    • Related Report
      2010 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Novel In-Situ NMR Measurement System for Evaluating Molecular Mobility during Drawing from Highly Entangled Polyethylene Melts2008

    • Author(s)
      Masaki Kakiage, Hiroki Uehara, Takeshi Yamanobe
    • Journal Title

      Macromolecular Rapid Communication Vol.29

      Pages: 1571-1576

    • Related Report
      2010 Final Research Report
    • Peer Reviewed
  • [Presentation] ケイ素系ブロック共重合体の昇温過程における構造変化2010

    • Author(s)
      山岸師、上原宏樹、山延健、野口圭太、大石香月、秋山映一
    • Organizer
      日本化学会関東支部群馬地区地域懇談会
    • Place of Presentation
      原研高崎(群馬県)
    • Year and Date
      2010-11-22
    • Related Report
      2010 Final Research Report
  • [Presentation] 新規シリコーンの一軸延伸過程のin-situ計測による架橋構造解析と調製条件による構造制御2010

    • Author(s)
      齊藤正純、上原宏樹、山延健、秋山映一
    • Organizer
      第59回高分子学会討論会
    • Place of Presentation
      北海道大学(北海道)
    • Year and Date
      2010-09-15
    • Related Report
      2010 Final Research Report
  • [Presentation] 無機酸化物粉体と高分子の相互作用に関する研究2010

    • Author(s)
      浜本彰子、上原宏樹、山延健、都竹浩一郎
    • Organizer
      第59回高分子学会討論会
    • Place of Presentation
      北海道大学(北海道)
    • Year and Date
      2010-09-15
    • Related Report
      2010 Final Research Report
  • [Presentation] 超高分子量ポリエチレンフィルムの延伸/圧縮による単斜晶の生成と消失2010

    • Author(s)
      森田翔、撹上将規、上原宏樹、山延健
    • Organizer
      第58回高分子学会年次大会
    • Place of Presentation
      パシフィコ横浜(神奈川)
    • Year and Date
      2010-05-27
    • Related Report
      2010 Final Research Report
  • [Presentation] 超高分子量ポリエチレンフィルムの延伸/圧縮2010

    • Author(s)
      山延健
    • Organizer
      高分子年次大会
    • Place of Presentation
      パシフィコ横浜
    • Year and Date
      2010-05-27
    • Related Report
      2010 Annual Research Report
  • [Presentation] 無機酸化物粉体と高分子の相互作用に関する研究2010

    • Author(s)
      浜本彰子、上原宏樹、山延健、都竹浩一郎
    • Organizer
      10-1 NMR研究会(高分子学会)
    • Place of Presentation
      産総研・臨海副都心センター(東京都)
    • Year and Date
      2010-05-21
    • Related Report
      2010 Final Research Report
  • [Presentation] Transition and Molecular Orientation Behavior of Crystalline Silicon-Based Polymer2009

    • Author(s)
      Hiroki Uehara, Tomohiro Obana, Masaki Kakiage, Takeshi Yamanobe, Keita Noguchi, Katsuki Oishi, Eiichi Akiyama
    • Organizer
      11th Pacific Polymer Conference 2009
    • Place of Presentation
      Cairns (Australia)
    • Year and Date
      2009-12-06
    • Related Report
      2010 Final Research Report
  • [Presentation] 結晶性高分子の延伸過程におけるNMR測定2009

    • Author(s)
      宮崎紀明、森田翔、撹上将規、上原宏樹、山延健
    • Organizer
      第58回高分子学会討論会
    • Place of Presentation
      熊本大学(熊本県)
    • Year and Date
      2009-09-16
    • Related Report
      2010 Final Research Report
  • [Presentation] 結晶性高分子の延伸過程におけるNMR測定2009

    • Author(s)
      宮崎紀明・森田翔・撹上将規・上原宏樹・山延健
    • Organizer
      高分子討論会
    • Place of Presentation
      熊本
    • Year and Date
      2009-09-16
    • Related Report
      2009 Annual Research Report
  • [Presentation] 溶液及び溶融状態から調製した超高分子量ポリエチレンフィルムの延伸/圧縮による単斜晶の生成2009

    • Author(s)
      森田翔・撹上将規・上原宏樹・山延健
    • Organizer
      高分子討論会
    • Place of Presentation
      熊本
    • Year and Date
      2009-09-16
    • Related Report
      2009 Annual Research Report
  • [Presentation] 超高分子量ポリエチレンフィルムの延伸・圧縮による単斜晶の生成と消失2009

    • Author(s)
      森田翔・撹上将規・上原宏樹・山延健
    • Organizer
      高分子学会・NMR研究会
    • Place of Presentation
      神奈川
    • Year and Date
      2009-08-27
    • Related Report
      2009 Annual Research Report
  • [Presentation] 結晶性高分子の延伸過程におけるNMR測定2009

    • Author(s)
      宮崎紀明・森田翔・撹上将規・上原宏樹・山延健
    • Organizer
      相模ケイ素材料フォーラム
    • Place of Presentation
      神奈川
    • Year and Date
      2009-08-27
    • Related Report
      2009 Annual Research Report
  • [Presentation] Poly(m-xylylene adipamide)の結晶化挙動のin-situ解析2009

    • Author(s)
      宇津木洋平・上原宏樹・山延健
    • Organizer
      高分子学会・NMR研究会
    • Place of Presentation
      東京
    • Year and Date
      2009-05-15
    • Related Report
      2009 Annual Research Report
  • [Presentation] 様々な環境下におけるパルスNMR測定による高分子材料のin-situ解析手法の開発2008

    • Author(s)
      山延健、撹上将規、上原宏樹
    • Organizer
      ポリマー材料フォーラム
    • Place of Presentation
      広島国際会議場(広島県)
    • Year and Date
      2008-11-27
    • Related Report
      2010 Final Research Report
  • [Presentation] 溶液および溶融状態から調製した超高分子量ポリエチレンフィルムの延伸/圧縮による単斜晶の生成2008

    • Author(s)
      森田翔、撹上将規、上原宏樹、山延健
    • Organizer
      第57回高分子学会討論会
    • Place of Presentation
      大阪市立大学(大阪府)
    • Year and Date
      2008-09-26
    • Related Report
      2010 Final Research Report
  • [Presentation] 溶液及び溶融状態から調製した超高分子量ポリエチレンフィルムの延伸/圧縮による単斜晶の生成2008

    • Author(s)
      山延健
    • Organizer
      高分子討論会
    • Place of Presentation
      大阪市立大学
    • Year and Date
      2008-09-26
    • Related Report
      2008 Annual Research Report
  • [Presentation] 高分子材料の変形過程における分子運動性変化のin-situ NMR計測2008

    • Author(s)
      撹上将規、上原宏樹、山延健
    • Organizer
      日本化学会第2回関東支部大会
    • Place of Presentation
      群馬大学工学部(群馬県)
    • Year and Date
      2008-09-18
    • Related Report
      2010 Final Research Report
  • [Book] Annual Reports on NMR Spectroscopy Volume 702010

    • Author(s)
      T.Yamanobe, M.Kakiage, H.Uehara
    • Publisher
      Academic Press
    • Related Report
      2010 Final Research Report

URL: 

Published: 2008-04-01   Modified: 2016-04-21  

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