Preparation of nanoparticles and porous structure particles by a new spray pyrolysis method

• Project/Area Number: 20760516
• Research Category: Grant-in-Aid for Young Scientists (B)
• Allocation Type: Single-year Grants
• Research Field: Properties in chemical engineering process/Transfer operation/Unit operation
• Research Institution: Hiroshima University
• Principal Investigator: FERRY Iskandar Hiroshima University, 大学院・工学研究科, 助教 (00452607)
• Project Period (FY): 2008 – 2009
• Project Status: Completed (Fiscal Year 2009)
• Budget Amount: ¥4,160,000 (Direct Cost: ¥3,200,000、Indirect Cost: ¥960,000); Fiscal Year 2009: ¥1,170,000 (Direct Cost: ¥900,000、Indirect Cost: ¥270,000); Fiscal Year 2008: ¥2,990,000 (Direct Cost: ¥2,300,000、Indirect Cost: ¥690,000)
• Keywords: ナノ粒子 / ナノ構造体 / 化学工学 / ナノ材料 / 材料加工

Research Abstract

1) Silica and barium titanate nanoparticles have been successfully prepared by a new developed spray pyrolysis method. 2) Effect of preparation conditions on the prepared nanoparticles properties has been investigated experimentally and theoretically. 3) Effect of additive materials into the prepared sample properties has been revealed. 4) Silica and titania porous particles with controlled particle and porous sizes have been successfully prepared. 5) Effect of preparation conditions on the prepared porous particles has been investigated experimentally and theoretically. 6) Photocatalytic of the titania porous particles were examined.

Research Products

• [Journal Article] Design of a Highly Ordered and Uniform Porous Structure with Multisized Pores in Film and Particle form using a Template-driven Self-Assembly Technique (2010)
  • Author(s): Nandiyanto, A.B.D., N. Hagura, F. Iskandar, K. Okuyama
  • Journal Title: Acta Mater 58(1) Pages: 282-289
  • Peer Reviewed
• [Journal Article] Design of a Highly Ordered and Uniform Porous Structure with Multisized Pores in Film and Particle form using a Template-driven Self-Assembly Technique (2010)
  • Author(s): Nandiyanto, A.B.D
  • Journal Title: Acta Mater. 58 Pages: 282-289
  • Peer Reviewed
• [Journal Article] Direct synthesis of highly crystalline transparent conducting oxide nanoparticles by low pressure spray pyrolysis (2009)
  • Author(s): Ogi, T., D. Hidayat, F. Iskandar, A. Purwanto, K. Okuyama
  • Journal Title: Adv. Powder Technol 20(2) Pages: 203-209
  • Peer Reviewed
• [Journal Article] Macroporous Anatase Titania Particle: Aerosol Self-Assembly Fabrication with Photocatalytic Performance (2009)
  • Author(s): Nandiyanto, A.B.D., F. Iskandar, K. Okuyama
  • Journal Title: Chem. Eng. J 152 Pages: 293-296
  • Peer Reviewed
• [Journal Article] Rapid Synthesis of a BN/CNT Composite Particle via Spray Routes using Ferrocene/Ethanol as a Catalyst/Carbon Source (2009)
  • Author(s): Nandiyanto, A.B.D., Y. Kaihatsu, F. Iskandar, K. Okuyama
  • Journal Title: Mater. Lett 63(21) Pages: 1847-1850
  • Peer Reviewed
• [Journal Article] A Role of Template Surface Charge in the Preparation of Porous and Hollow Particle Using a Spray-drying Method (2009)
  • Author(s): Hagura, N., A.B.D. Nandiyanto, F. Iskandar, K. Okuyama
  • Journal Title: Chem. Lett 38(11) Pages: 1076-1077
  • Peer Reviewed
• [Journal Article] Macroporous Anatase Titania Particle : Aerosol Self-Assembly Fabrication with Photocatalytic Performance (2009)
  • Author(s): Nandiyanto, A.B.D.
  • Journal Title: Chem.Eng.J. 152 Pages: 293-296
  • Peer Reviewed
• [Journal Article] Rapid Synthesis of a BN/CNT Composite Particle via Spray Routes using Ferrocene/Ethanol as a Catalyst/Carbon Source (2009)
  • Author(s): Nandiyanto, A.B.D.
  • Journal Title: Mater.Lett. 63 Pages: 1847-1850
  • Peer Reviewed
• [Journal Article] A Role of Template Surface Charge in the Preparation of Porous and Hollow Particle Using a Spray-drying Method (2009)
  • Author(s): Hagura, N.
  • Journal Title: Chem.Lett. 38 Pages: 1076-1077
  • Peer Reviewed
• [Journal Article] Nano-sized Polymer Particle- Facilitated Preparation of Mesoporous Silica Particles Using a Spray Method (2008)
  • Author(s): Nandiyanto, A.B.D., F. Iskandar, K. Okuyama
  • Journal Title: Chem. Lett 37 Pages: 1040-1041
  • Peer Reviewed
• [Journal Article] Role of Urea Addition in the Preparation of Tetragonal BaTiO3 Nanoparticles Using Flame Assisted Spray Pyrolysis (2008)
  • Author(s): Terashi, Y., A. Purwanto, W.N. Wang, F. Iskandar, K. Okuyama
  • Journal Title: J. Eur. Ceram. Soc 28 Pages: 2573-2580
  • Peer Reviewed
• [Journal Article] Nano-sized Polymer Particle-Facilitated Preparation of Mesoporous Silica Particles Using a Spray Method (2008)
  • Author(s): Nandiyanto, A. B. D.
  • Journal Title: Chem. Lett. 37 Pages: 1040-1041
  • Peer Reviewed
• [Journal Article] Role of Urea Addition in the Preparation of Tetragonal BaTiO3 Nanoparticles Using Flame Assisted Spray Pyrolysis (2008)
  • Author(s): Terashi, Y.
  • Journal Title: J. Eur. Ceram. Soc. 28 Pages: 2573-2580
  • Peer Reviewed
• [Journal Article] Direct synthesis of highly crystalline transparent conducting oxidenanoparticles by low pressure spray Pyrolysis
  • Author(s): Ogi, T.
  • Journal Title: Adv. Powder Technol. (印刷中)
  • Peer Reviewed
• [Presentation] Tunable Nanometer Pore Size of Silica Nanoparticles with Controllable Outer Diameters (2009)
  • Author(s): Nandiyanto, A.B.D.
  • Organizer: 第41回化学工学会秋季大会
  • Place of Presentation: 広島大学
  • Year and Date: 2009-09-17
• [Presentation] Tunable Nanometer Pore Size of Silica Nanoparticles with Controllable Outer Diameters (2009)
  • Author(s): Nandiyanto A.B.D., F. Iskandar, K. Okuyama
  • Organizer: 化学工学会第41回秋季大会
  • Place of Presentation: 広島大学東広島キャンパス
• [Presentation] Strategies for Particle Design using Spray Method (2008)
  • Author(s): Ferry Iskandar
  • Organizer: International Aerosol Symposium 2008
  • Place of Presentation: 金沢
  • Year and Date: 2008-08-22
• [Presentation] Strategies for Particle Design using Spray Method (2008)
  • Author(s): F. Iskandar, K. Okuyama
  • Organizer: International Aerosol Symposium 2008
  • Place of Presentation: Kanazawa, Japan
• [Book] 21世紀の吸入療法 (2008)
  • Author(s): 奥山喜久夫、Ferry Iskandar
  • Publisher: (株)仙台気道研究所
• [Book] 21世紀の吸入療法 (2008)
  • Author(s): 奥山喜久夫
  • Publisher: (株)仙台気道研究所