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Microstructure formation in high-Strength ductility high oxygen concentration additively manufactured Ti alloys

Research Project

Project/Area Number 20K05155
Research Category

Grant-in-Aid for Scientific Research (C)

Allocation TypeMulti-year Fund
Section一般
Review Section Basic Section 26050:Material processing and microstructure control-related
Research InstitutionOsaka University

Principal Investigator

Umeda Junko  大阪大学, 接合科学研究所, 教授 (50345162)

Project Period (FY) 2020-04-01 – 2024-03-31
Project Status Completed (Fiscal Year 2023)
Budget Amount *help
¥4,290,000 (Direct Cost: ¥3,300,000、Indirect Cost: ¥990,000)
Fiscal Year 2023: ¥910,000 (Direct Cost: ¥700,000、Indirect Cost: ¥210,000)
Fiscal Year 2022: ¥1,040,000 (Direct Cost: ¥800,000、Indirect Cost: ¥240,000)
Fiscal Year 2021: ¥1,170,000 (Direct Cost: ¥900,000、Indirect Cost: ¥270,000)
Fiscal Year 2020: ¥1,170,000 (Direct Cost: ¥900,000、Indirect Cost: ¥270,000)
Keywordsチタン / 積層造形体
Outline of Research at the Start

選択的レーザ溶融法(SLM)により作製した高濃度酸素(α-Ti相安定化元素)含有チタン積層造形体において,固溶強化による顕著な強度向上と同時に高延性を有する新奇な力学挙動の解明を目的に,急速凝固・冷却過程で形成される特異な組織形態(acicular α/α’マルテンサイト相)と結晶配向性および酸素固溶分布に着目し,これらの組織構造因子と変形機構の関係を解き明かす.その結果に基づき,延性低下が著しいチタン積層造形体において,高強度と高延性の同時発現を可能とする新規な材料・プロセス設計原理の構築を目指す.

Outline of Final Research Achievements

Focusing on oxygen as a stabilizing element of the α-phase, which was considered to be a negative material factor, it was clarified that a small amount of oxygen contributes to the formation of a specific crystal structure through microscopic structural analysis of the behavior of oxygen atoms during the layer fabrication process. The dissociated oxygen atoms after decomposition of TiO2 particles, which are the source of oxygen, were found to solid-solubilize into α-Ti grains, and the transformation from coarse columnar grains to fine needle-like martensite phase was observed.

Academic Significance and Societal Importance of the Research Achievements

チタン材料では,酸素成分の粒界偏析に起因した脆化現象が報告されており,特に規格上限値を超える高濃度では,伸び値が激減する.しかし,酸素は本当に負の因子であるのか?と問い,レアメタルの代替物質として酸素に着目した.積層造形時の溶融・超急冷凝固過程での酸素原子の振舞いを理解し,チタン材の延性低下を招く結晶粒界近傍での酸素濃化による化合物相の形成を抑制し,酸素元素をα-Ti内に均一固溶することで結晶粒径や集合組織を制御することで,高強度と高延性の同時発現が可能であることを明らかにした.その結果,チタン合金の高強度化に必須であるレアメタル使用撤廃の可能性を示したことは学術的な意義であると考える.

Report

(5 results)
  • 2023 Annual Research Report   Final Research Report ( PDF )
  • 2022 Research-status Report
  • 2021 Research-status Report
  • 2020 Research-status Report
  • Research Products

    (8 results)

All 2024 2023 2022 2021 Other

All Int'l Joint Research (2 results) Journal Article (2 results) (of which Int'l Joint Research: 1 results,  Peer Reviewed: 2 results,  Open Access: 2 results) Presentation (4 results) (of which Int'l Joint Research: 2 results,  Invited: 1 results)

  • [Int'l Joint Research] Chinese Academy of Sciences/Xi’an University of Technology(中国)

    • Related Report
      2023 Annual Research Report
  • [Int'l Joint Research] Chinese Academy of Sciences/Xi’an University of Technology(中国)

    • Related Report
      2022 Research-status Report
  • [Journal Article] Mechanical Functionalization of Additively Manufactured Titanium with Light Elements2024

    • Author(s)
      近藤勝義, 市川絵理, A. Issariyapat, 梅田純子
    • Journal Title

      Journal of the Japan Society of Powder and Powder Metallurgy

      Volume: 71 Issue: 12 Pages: 586-595

    • DOI

      10.2497/jjspm.23-00031

    • ISSN
      0532-8799, 1880-9014
    • Year and Date
      2024-12-15
    • Related Report
      2023 Annual Research Report
    • Peer Reviewed / Open Access
  • [Journal Article] Tribological Behavior of Titanium-Sintered Composites with Ring-Shaped TiN Dispersoids2022

    • Author(s)
      21.J. Umeda, H. Fujii, R. Takizawa, T. Teramae, A. Issariyapat, S. Kariya, Y. Yang, S. Li, K. Kondoh
    • Journal Title

      Lubricants

      Volume: 10 Issue: 10 Pages: 254-254

    • DOI

      10.3390/lubricants10100254

    • Related Report
      2022 Research-status Report
    • Peer Reviewed / Open Access / Int'l Joint Research
  • [Presentation] 軽元素を利用したチタン積層造形材の力学機能化2023

    • Author(s)
      近藤勝義, A. Issariyapat, 梅田純子,市川絵理
    • Organizer
      粉体粉末冶金協会2023年度春季大会
    • Related Report
      2023 Annual Research Report
  • [Presentation] High Strength Ti-Zr Alloys With Balanced Ductility Fabricated By Powder Metallurgy And Additive Manufacturing Routes2022

    • Author(s)
      Katusyoshi Kondoh
    • Organizer
      PM2022
    • Related Report
      2022 Research-status Report
    • Int'l Joint Research / Invited
  • [Presentation] SLM Induced Carbon Solid Solution in Titanium Alloys2021

    • Author(s)
      J. E. Peterson, E. Ichikawa, J. Umeda, K. Kondoh
    • Organizer
      粉末冶金協会2021年度秋季大会
    • Related Report
      2021 Research-status Report
  • [Presentation] Additively Manufactured High-Performance Commercially Pure Titanium Strengthened with Ubiquitous Light Elements2021

    • Author(s)
      A. Issariyapat, J. Umeda, K. Kondoh
    • Organizer
      LightMAT 2021
    • Related Report
      2021 Research-status Report
    • Int'l Joint Research

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Published: 2020-04-28   Modified: 2025-01-30  

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