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Element identification and mass detection with a high frequency micro oscillator, and implementation of a liquid atomic force microscope

Research Project

Project/Area Number 21241035
Research Category

Grant-in-Aid for Scientific Research (A)

Allocation TypeSingle-year Grants
Section一般
Research Field Microdevices/Nanodevices
Research InstitutionThe University of Tokyo

Principal Investigator

KAWAKATS Hideki  東京大学, 生産技術研究所, 教授 (30224728)

Project Period (FY) 2009 – 2011
Project Status Completed (Fiscal Year 2011)
Budget Amount *help
¥47,190,000 (Direct Cost: ¥36,300,000、Indirect Cost: ¥10,890,000)
Fiscal Year 2011: ¥13,780,000 (Direct Cost: ¥10,600,000、Indirect Cost: ¥3,180,000)
Fiscal Year 2010: ¥16,120,000 (Direct Cost: ¥12,400,000、Indirect Cost: ¥3,720,000)
Fiscal Year 2009: ¥17,290,000 (Direct Cost: ¥13,300,000、Indirect Cost: ¥3,990,000)
KeywordsAFM / 表面界面 / APM / STM / TEMAFM / 固液界面 / 力計測 / SPM / マルチモード / 液中AFM / 環境制御型SPM
Research Abstract

Atomic Force Microscopy(AFM) with chemical contrast at the atomiclevel was implemented by changing the established equifrequency shift FM mode to a new mode where the tip sample distance is regulated to give the local minima of the frequency shift. As a result atomic resolution images with angstroem order featufrersentof difcolours were readily acquired. As for application of emission to the measurement of molecules and nanooscillators, a FIMAFM was implemented. Self assembled monolayers deposited on a metal tip gave vibratory emission patterns. It was also ddetmhoantstrate molecules of different rigidity show different vibratory emission patterns. For liquidAFM, a photothermal excitation method was employed to enable simultaneous excitation oftorsion and deflection. Both modes showed good atomic resolution.oMfobifloigtgy zoneson mica was observed for mica immersed in pure water. Hight histogram showed that the foggy zone has discreet population of height, implying formation of an ice like structure that moves about.

Report

(4 results)
  • 2011 Annual Research Report   Final Research Report ( PDF )
  • 2010 Annual Research Report
  • 2009 Annual Research Report
  • Research Products

    (56 results)

All 2013 2012 2011 2010 2009 Other

All Journal Article (9 results) (of which Peer Reviewed: 9 results) Presentation (43 results) (of which Invited: 5 results) Book (1 results) Remarks (2 results) Patent(Industrial Property Rights) (1 results)

  • [Journal Article] 光熱高周波振動励振を用いた超高分解能原子間力顕微鏡2013

    • Author(s)
      川勝英樹
    • Journal Title

      光学

      Volume: 42巻2号77

    • Related Report
      2011 Final Research Report
    • Peer Reviewed
  • [Journal Article] Molecular Resolution of a DOPC Lipid Bilayer in Liquid by Phase Modulation Atomic Force Microscopy2012

    • Author(s)
      A. Hoel, T. Osaki,S. Takeuchi, S. Volz and H. Kawakatsu
    • Journal Title

      APL 101

      Pages: 63117-63117

    • Related Report
      2011 Final Research Report
    • Peer Reviewed
  • [Journal Article] Application of a new microcantilever biosensor resonating at the air-liquid interface for direct insulin detection and continuous monitoring of enzymatic reactions2012

    • Author(s)
      J. Park, S. Karsten, S. Nishida,H. Kawakatsu, and H. Fujita
    • Journal Title

      Lab on a chip

      Volume: 11 Pages: 4115-4115

    • Related Report
      2011 Final Research Report
    • Peer Reviewed
  • [Journal Article] High-resolution cantilever biosensor resonating at air-liquid in a microchannelPark2011

    • Author(s)
      J., Nishida, S., Lambert, P.,Kawakatsu, H., Fujita, H.
    • Journal Title

      Lab on a Chip -Miniaturisation for Chemistry and Biology volume 11

      Volume: 24 Pages: 4187-4187

    • Related Report
      2011 Final Research Report
    • Peer Reviewed
  • [Journal Article] Small single-crystal silicon cantilevers formed by crystal facets for atomic force microscopy2009

    • Author(s)
      Kazuhisa Nakagawa, Gen Hashiguchi,and Hideki Kawakatsu
    • Journal Title

      RSI 80

      Pages: 95104-95104

    • Related Report
      2011 Final Research Report
    • Peer Reviewed
  • [Journal Article] Dithering-amplitude dependence of STM-regulated dynamic lateral force microscopy maps on Si(111)7x72009

    • Author(s)
      Naruo Sasaki, Shigeki Kawai and Hideki Kawakatsu
    • Journal Title

      Phys. Rev B80

      Pages: 193402-193402

    • Related Report
      2011 Final Research Report
    • Peer Reviewed
  • [Journal Article] Photothermal excitation of a single-crystalline silicon cantilever for higher vibration modes in liquid2009

    • Author(s)
      Shuhei Nishida, Dai Kobayashi, and Hideki Kawakatsu
    • Journal Title

      J. Vac. Sci. Technol. B

      Volume: 27 Pages: 964-964

    • Related Report
      2011 Final Research Report
    • Peer Reviewed
  • [Journal Article] Direct mapping of the lateral force gradient on Si(111)-7x72009

    • Author(s)
      S Kawai, N.Sasaki and H. Kawakatsu
    • Journal Title

      Phys. Rev B

      Volume: 79 Pages: 195412-195412

    • Related Report
      2011 Final Research Report
    • Peer Reviewed
  • [Journal Article] Surface-relaxation-induced giant corrugation on graphite(0001)2009

    • Author(s)
      S.Kawai,and H. Kawakatsu
    • Journal Title

      Phys. Rev. B

      Volume: 79 Pages: 115440-115440

    • Related Report
      2011 Final Research Report
    • Peer Reviewed
  • [Presentation] 液中原子間力顕微鏡ならびに超 高真空TEM・AFM,FIM・AFM2012

    • Author(s)
      川勝英樹
    • Organizer
      応用物理学会、応用電子物性分科会
    • Place of Presentation
      東京
    • Year and Date
      2012-07-30
    • Related Report
      2011 Final Research Report
  • [Presentation] Atomic resolution imaging by dynamic mode liquid lateral force microscopy2012

    • Author(s)
      H.Kawakatsu
    • Organizer
      68th Japan Society of Microscopy
    • Place of Presentation
      Tsukuba, Japan
    • Year and Date
      2012-05-16
    • Related Report
      2011 Final Research Report
  • [Presentation] Friction and Wear on Nano-Contact with vibration2011

    • Author(s)
      小幡佳弘
    • Organizer
      応用物理学会
    • Place of Presentation
      洞爺湖万世閣 北海道
    • Year and Date
      2011-12-20
    • Related Report
      2010 Annual Research Report
  • [Presentation] Study of Time and Temperature Dependence on Structural Transitions of Solid/Liquid Interfaces using Liquid AFM2011

    • Author(s)
      村上弘明
    • Organizer
      応用物理学会
    • Place of Presentation
      洞爺湖万世閣 北海道
    • Year and Date
      2011-12-20
    • Related Report
      2010 Annual Research Report
  • [Presentation] Time-Dependent Structural Changes of Solid/Liquid Interfaces Observed using Dynamic Lateral Force Microscopy2011

    • Author(s)
      西田周平
    • Organizer
      応用物理学会
    • Place of Presentation
      洞爺湖万世閣 北海道
    • Year and Date
      2011-12-19
    • Related Report
      2010 Annual Research Report
  • [Presentation] High Frequency Low Amplitude Atomic Force Microscopy and Related Techniques2011

    • Author(s)
      川勝英樹
    • Organizer
      Colloquium on Nanotechnology
    • Place of Presentation
      Busan, Korea
    • Year and Date
      2011-10-26
    • Related Report
      2010 Annual Research Report
  • [Presentation] High Frequency Low Amplitude Atomic Force Microscopy2011

    • Author(s)
      川勝英樹
    • Organizer
      2011 Asia Micro Mechatronics Forum
    • Place of Presentation
      Daegu, Korea
    • Year and Date
      2011-10-25
    • Related Report
      2010 Annual Research Report
  • [Presentation] Methods for measuring vibrations at the nanometer scale for atomic force microscopy and related techniques2011

    • Author(s)
      Hideki Kawakatsu
    • Organizer
      Nanotrends 2011
    • Place of Presentation
      Hefei, Wuxi, China
    • Year and Date
      2011-10-11
    • Related Report
      2011 Final Research Report
  • [Presentation] Methods for measuring vibrations at the nanometer scale for atomic force microscopy and related techniques2011

    • Author(s)
      川勝英樹
    • Organizer
      The 1^<st> Forum on Trends in Nano-Manufacturing
    • Place of Presentation
      Hefei, Chine
    • Year and Date
      2011-10-11
    • Related Report
      2010 Annual Research Report
  • [Presentation] Methods for measuring vibrations at the nanometer scale for atomic force microscopy and related techniques2011

    • Author(s)
      Hideki Kawakatsu
    • Organizer
      Nanotrends 2011
    • Place of Presentation
      Hefei,China
    • Related Report
      2011 Annual Research Report
    • Invited
  • [Presentation] Morphological changes observed with the liquid AFM2011

    • Author(s)
      Hideki Kawakatsu
    • Organizer
      NC AFM2011
    • Place of Presentation
      Lindau,Germany
    • Related Report
      2011 Annual Research Report
  • [Presentation] Time-Dependent Structural Changes of Solid/Liquid Interfaces Observed using Dynamic Lateral Force Microscopy2011

    • Author(s)
      Shuhei Nishida
    • Organizer
      ICSPM 19
    • Place of Presentation
      Hokkaido,Japan
    • Related Report
      2011 Annual Research Report
  • [Presentation] Friction and Wear on Nano-Contact with Vibration2011

    • Author(s)
      Hideki Kawakatsu
    • Organizer
      ICSPM 19
    • Place of Presentation
      Hokkaido,Japan
    • Related Report
      2011 Annual Research Report
  • [Presentation] Study of Time and Temperature Dependence on Structural Transitions of Solid/Liquid Interfaces using Liquid AFM2011

    • Author(s)
      Hiroaki Murakami
    • Organizer
      ICSPM 19
    • Place of Presentation
      Hokkaido,Japan
    • Related Report
      2011 Annual Research Report
  • [Presentation] Preliminary Results Obtained with a UHV TEM AFM on Si and KBr Filiform Neck Formation2010

    • Author(s)
      C.K.YEOH, H.KAWAKATSU
    • Organizer
      18th International Colloquium on Scanning Probe Microscopy
    • Place of Presentation
      伊豆熱川 熱川ハイツ
    • Year and Date
      2010-12-11
    • Related Report
      2009 Annual Research Report
  • [Presentation] Measurement of Vibration of a Molecule Nanometric Oscillator by Emission2010

    • Author(s)
      H.NISIZAWA, H.KAWAKATSU
    • Organizer
      18th International Colloquium on Scanning Probe Microscopy
    • Place of Presentation
      伊豆熱川 熱川ハイツ
    • Year and Date
      2010-12-10
    • Related Report
      2009 Annual Research Report
  • [Presentation] Towards Measuement of Vibration of Nanocantilevers-Imaging the Vibration of Alkanethiols as Bottom-up Fabricated Oscillators2010

    • Author(s)
      Y.HONDA, H.KAWAKATSU
    • Organizer
      18th International Colloquium on Scanning Probe Microscopy
    • Place of Presentation
      伊豆熱川 熱川ハイツ
    • Year and Date
      2010-12-09
    • Related Report
      2009 Annual Research Report
  • [Presentation] Development of TEM-AFM and Observation2010

    • Author(s)
      Y.OBATA, H.KAWAKATSU
    • Organizer
      18th International Colloquium on Scanning Probe Microscopy
    • Place of Presentation
      伊豆熱川 熱川ハイツ
    • Year and Date
      2010-12-09
    • Related Report
      2009 Annual Research Report
  • [Presentation] Methods for measuring vibrations at the nanometer scale2010

    • Author(s)
      Hideki Kawakatsu
    • Organizer
      ICS 2010
    • Place of Presentation
      Ise-Shima, Mie, Japan
    • Year and Date
      2010-09-15
    • Related Report
      2011 Final Research Report
  • [Presentation] High Frequency Low Amplitude Atomic Force Microscopy

    • Author(s)
      Hideki Kawakatsu
    • Organizer
      2011 Asia Micro Mechatronics Forum
    • Place of Presentation
      Daegu, Korea
    • Related Report
      2011 Annual Research Report
    • Invited
  • [Presentation] High frequency low amplitude AFM and measurement of very small oscillators

    • Author(s)
      Hideki Kawakatsu
    • Organizer
      Invited lecture at PNU
    • Place of Presentation
      Busan, Korea
    • Related Report
      2011 Annual Research Report
    • Invited
  • [Presentation] Atomic resolution imaging by dynamic mode liquid lateral force microscopy

    • Author(s)
      Hideki Kawakatsu
    • Organizer
      68th Japanese Society of Microscopy 2012
    • Place of Presentation
      つくば(つくば国際会議場)
    • Related Report
      2011 Annual Research Report
    • Invited
  • [Presentation] 液中原子間力顕微鏡ならびに超高真空TEM・AFM , FIM・AFM

    • Author(s)
      川勝 英樹
    • Organizer
      応物学会・応物電子分性分科会 7月研究例会
    • Place of Presentation
      秋葉原(首都大学東京サテライトキャンパス)
    • Related Report
      2011 Annual Research Report
    • Invited
  • [Presentation] A variable temperature liquid AFM and observation of morphological changes of an ice-like structure on mica

    • Author(s)
      Hideki Kawakatsu
    • Organizer
      NCAFM2012
    • Place of Presentation
      Cesky Krumlov, Czech Republic
    • Related Report
      2011 Annual Research Report
  • [Presentation] Towards multimodal all-optic UHV Atomic Force Microscopy

    • Author(s)
      Denis Damiron
    • Organizer
      NCAFM2012
    • Place of Presentation
      Cesky Krumlov, Czech Republic
    • Related Report
      2011 Annual Research Report
  • [Presentation] An ‘all-optic’ lateral liquid AFM and UHV(TEM/FIM)AFM

    • Author(s)
      Hideki Kawakatsu
    • Organizer
      Seeing at the Nanoscale 2012
    • Place of Presentation
      Bristol, England
    • Related Report
      2011 Annual Research Report
  • [Presentation] Real-time atomic resolution imaging with chemical contrast

    • Author(s)
      Hideki Kawakatsu
    • Organizer
      Multifrequency AFM 2012
    • Place of Presentation
      Madrid, Spain
    • Related Report
      2011 Annual Research Report
  • [Presentation] Onset of lateral and vertical dynamic modes in liquid AFM

    • Author(s)
      Hiroaki Murakami
    • Organizer
      Multifrequency AFM 2012
    • Place of Presentation
      Madrid, Spain
    • Related Report
      2011 Annual Research Report
  • [Presentation] 元素コントラストAFMにおけるラテラルモード

    • Author(s)
      Hideki Kawakatsu
    • Organizer
      京大・基研研究会「摩擦、レオロジー、地震の新展開 ー異なる階層と舞台をつなぐー」
    • Place of Presentation
      京都(京大基礎物理学研究所パナソニックホール)
    • Related Report
      2011 Annual Research Report
  • [Presentation] AFM with chemical contrast and its application in lateral force microscopy

    • Author(s)
      Denis Damiron
    • Organizer
      京大・基研研究会「摩擦、レオロジー、地震の新展開 ー異なる階層と舞台をつなぐー」
    • Place of Presentation
      京都(京大基礎物理学研究所パナソニックホール)
    • Related Report
      2011 Annual Research Report
  • [Presentation] TEMAFMを用いた摩擦研究-垂直振動印加による摩擦低減のその場観測

    • Author(s)
      中野 憲
    • Organizer
      京大・基研研究会「摩擦、レオロジー、地震の新展開 ー異なる階層と舞台をつなぐー」
    • Place of Presentation
      京都(京大基礎物理学研究所パナソニックホール)
    • Related Report
      2011 Annual Research Report
  • [Presentation] ラテラル液中AFMによるフォースカーブを用いた固液界面の計測

    • Author(s)
      鳥山 陽平
    • Organizer
      京大・基研研究会「摩擦、レオロジー、地震の新展開 ー異なる階層と舞台をつなぐー」
    • Place of Presentation
      京都(京大基礎物理学研究所パナソニックホール)
    • Related Report
      2011 Annual Research Report
  • [Presentation] 液中AFMにおけるラテラルモードと垂直モードの比較

    • Author(s)
      村上 弘明
    • Organizer
      京大・基研研究会「摩擦、レオロジー、地震の新展開 ー異なる階層と舞台をつなぐー」
    • Place of Presentation
      京都(京大基礎物理学研究所パナソニックホール)
    • Related Report
      2011 Annual Research Report
  • [Presentation] 三次元アトムプローブにおける電界蒸発の結晶方位依存性の解析

    • Author(s)
      清水 真人
    • Organizer
      第60回応用物理学会春季学術講演会
    • Place of Presentation
      厚木(神奈川工科大学)
    • Related Report
      2011 Annual Research Report
  • [Presentation] 垂直モード高真空原子間力顕微鏡による化学的同定法

    • Author(s)
      鳥山 陽平
    • Organizer
      第60回応用物理学会春季学術講演会
    • Place of Presentation
      厚木(神奈川工科大学)
    • Related Report
      2011 Annual Research Report
  • [Presentation] テラルモード光励振式 UHVAFM による化学的同定法

    • Author(s)
      Denis Damiron
    • Organizer
      第60回応用物理学会春季学術講演会
    • Place of Presentation
      厚木(神奈川工科大学)
    • Related Report
      2011 Annual Research Report
  • [Presentation] TEM-AFMによるナノ領域の測定

    • Author(s)
      武田 俊
    • Organizer
      第60回応用物理学会春季学術講演会
    • Place of Presentation
      厚木(神奈川工科大学)
    • Related Report
      2011 Annual Research Report
  • [Presentation] 自己組織化単分子膜振動 は電界イオン顕微鏡で観察

    • Author(s)
      Pierre Allain
    • Organizer
      第60回応用物理学会春季学術講演会
    • Place of Presentation
      厚木(神奈川工科大学)
    • Related Report
      2011 Annual Research Report
  • [Presentation] Toward real time chemical contrast atomic force microscopy

    • Author(s)
      Mohammad Othman
    • Organizer
      ICSPM20
    • Place of Presentation
      那覇(沖縄かりゆしアーバンリゾート)
    • Related Report
      2011 Annual Research Report
  • [Presentation] AFM with chemical contrast and its application in lateral force microscopy

    • Author(s)
      Yohei Toriyama
    • Organizer
      ICSPM20
    • Place of Presentation
      那覇(沖縄かりゆしアーバンリゾート)
    • Related Report
      2011 Annual Research Report
  • [Presentation] Comparison of lateral and vertical modes with bimodal Liquid AFM

    • Author(s)
      Hiroaki Murakami
    • Organizer
      ICSPM20
    • Place of Presentation
      那覇(沖縄かりゆしアーバンリゾート)
    • Related Report
      2011 Annual Research Report
  • [Presentation] Development of Atom Probe Atomic Force Microscope for Chemical Identification

    • Author(s)
      Hidenobu Nishizawa
    • Organizer
      ICSPM20
    • Place of Presentation
      那覇(沖縄かりゆしアーバンリゾート)
    • Related Report
      2011 Annual Research Report
  • [Presentation] Using TEM-AFM three dimensional nano-range measurement

    • Author(s)
      Ken Nakano
    • Organizer
      ICSPM20
    • Place of Presentation
      那覇(沖縄かりゆしアーバンリゾート)
    • Related Report
      2011 Annual Research Report
  • [Book] Noncontact Atomic Force Microscopy:Volume 2 (NanoScience and Technology)2009

    • Author(s)
      H.Kawakatsu, Shuhei Nishida, Dai Kobayashi, Kazuhisa Nakagawa and Shigeki Kawai
    • Total Pages
      347
    • Publisher
      Editors S. Morita, f. Giessibl and R.Wiesendanger, (共著)High-Frequency Low amplitude Atomic Force Microscopy
    • Related Report
      2011 Final Research Report
  • [Remarks]

    • URL

      http://www.inventio.iis.u-tokyo.ac.jp/

    • Related Report
      2011 Final Research Report
  • [Remarks] 川勝研究室HP

    • URL

      http://www.inventio.iis.u-tokyo.ac.jp

    • Related Report
      2011 Annual Research Report
  • [Patent(Industrial Property Rights)] 気液界面で共振するマイクロカンチレ バーセンサ2011

    • Inventor(s)
      朴柾〓、西田周平、藤田博之、川勝英樹
    • Industrial Property Rights Holder
      東京大学
    • Filing Date
      2011-01-21
    • Related Report
      2011 Final Research Report

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Published: 2009-04-01   Modified: 2016-04-21  

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