The calibration free detector for high performance liquid ography
| Project/Area Number |
23750089
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| Research Category |
Grant-in-Aid for Young Scientists (B)
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| Allocation Type | Multi-year Fund |
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| Research Field |
Analytical chemistry
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| Research Institution | Kumamoto University |
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Principal Investigator |
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| Project Period (FY) |
2011 – 2013
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| Project Status |
Completed (Fiscal Year 2013)
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| Budget Amount *help |
¥4,290,000 (Direct Cost: ¥3,300,000、Indirect Cost: ¥990,000)
Fiscal Year 2013: ¥910,000 (Direct Cost: ¥700,000、Indirect Cost: ¥210,000)
Fiscal Year 2012: ¥1,300,000 (Direct Cost: ¥1,000,000、Indirect Cost: ¥300,000)
Fiscal Year 2011: ¥2,080,000 (Direct Cost: ¥1,600,000、Indirect Cost: ¥480,000)
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| Keywords | キャリブレーションフリー / クロマトグラフィー / 高速液体クロマトグラフィー / 電荷量検出器 / 緩衝溶液ジェネレータ / pHグラジエント |
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| Research Abstract |
The calibration free detecro for high performance liquid chromatography has been studied. The procedure for the detection, oxidation, collection and detection has been optimized. The quantitative oxidation was achieved. Furthermore, the results of developped detector was well agreed with the theoretical values.
The eluent with no organic solvent was also studied. The pH gradient method was selected for the purpose. The pH gradient was achieved by electro dialytic pH generator. The generator was well optimized with feed back control.
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Report
(4 results)
Research Products
(4 results)
