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Construction of the precipitation and growth model of nano-sized oxide particles in oxide dispersion strengthened steel

Research Project

Project/Area Number 26820325
Research Category

Grant-in-Aid for Young Scientists (B)

Allocation TypeMulti-year Fund
Research Field Material processing/Microstructural control engineering
Research InstitutionHokkaido University

Principal Investigator

OONO Naoko  北海道大学, 工学研究院, 助教 (40512489)

Project Period (FY) 2014-04-01 – 2017-03-31
Project Status Completed (Fiscal Year 2016)
Budget Amount *help
¥3,120,000 (Direct Cost: ¥2,400,000、Indirect Cost: ¥720,000)
Fiscal Year 2016: ¥1,170,000 (Direct Cost: ¥900,000、Indirect Cost: ¥270,000)
Fiscal Year 2015: ¥1,170,000 (Direct Cost: ¥900,000、Indirect Cost: ¥270,000)
Fiscal Year 2014: ¥780,000 (Direct Cost: ¥600,000、Indirect Cost: ¥180,000)
Keywords酸化物粒子 / 分散強化 / 析出 / 自由エネルギー / ODS鋼 / 析出の活性化エネルギー / Y-(Al, Ti, Zr)複合酸化物 / ナノ酸化物粒子 / Al, Ti, Zr添加 / 微細組織
Outline of Final Research Achievements

The process of precipitating oxide particles in oxide dispersion strengthened (ODS) steels during the temperature rising stage of sintering is studied, by analyzing the microstructure of the systematically heat treated mechanically alloyed (MA) powders, and classified by free energy of precipitation. Comparing the Ti, Al and Zr added / solute elements-free ODS steel, the calculation result of the precipitation critical radius and the activation energy of the precipitation at 700° C, which is the precipitation starting temperature of Y2O3, is small in the order of Y2Zr2O7 < Y2O3 < Y2Ti2O7 < YAlO3. This order agreed with the experimental result of this research.

Report

(4 results)
  • 2016 Annual Research Report   Final Research Report ( PDF )
  • 2015 Research-status Report
  • 2014 Research-status Report
  • Research Products

    (9 results)

All 2017 2016 2015 2014

All Journal Article (1 results) Presentation (8 results) (of which Int'l Joint Research: 2 results,  Invited: 1 results)

  • [Journal Article] 酸化物分散強化(ODS)フェライト鋼の添加元素によって異なる酸化物粒子析出プロセスの解明2017

    • Author(s)
      大野直子、礒部重人、宮里一旗、金野杏彩、柴田博紀、鵜飼重治、林重成、大塚智史、奥田隆成、本間徹生
    • Journal Title

      SPring-8 産業新分野支援課題・一般課題(産業分野)実施報告書

      Volume: 2016A

    • Related Report
      2016 Annual Research Report
  • [Presentation] ODSフェライト鋼の酸化物粒子析出プロセスの解明2016

    • Author(s)
      大野直子、礒部重人、宮里一旗、金野杏彩、柴田博紀、鵜飼重治、林重成、大塚智史、奥田隆成、本間徹生
    • Organizer
      日本金属学会2016年秋期(第159回)講演大会
    • Place of Presentation
      大阪大学豊中キャンパス
    • Year and Date
      2016-09-21
    • Related Report
      2016 Annual Research Report
  • [Presentation] ODSフェライト鋼の添加元素が酸化物粒子形成に及ぼす効果2016

    • Author(s)
      大野直子、中村顕、鵜飼重治、林重成、大塚智史、奥田隆成、海老澤直樹、戸村恵子、外山健、永井康介
    • Organizer
      日本金属学会2016年春期講演大会
    • Place of Presentation
      東京理科大学葛飾キャンパス(東京都葛飾区)
    • Year and Date
      2016-03-25
    • Related Report
      2015 Research-status Report
  • [Presentation] ODSフェライト鋼の添加元素が酸化物粒子形成に及ぼす効果2015

    • Author(s)
      大野直子、中村顕、鵜飼重治、林重成、大塚智史、奥田隆成
    • Organizer
      平成2 7年度 日本鉄鋼協会 ・日本金属学会 両北海道支部 合同 冬季講演大会
    • Place of Presentation
      北海道大学(札幌市)
    • Year and Date
      2015-12-18
    • Related Report
      2015 Research-status Report
  • [Presentation] Precipitation of oxide particles in ODS ferritic steels2015

    • Author(s)
      N. Oono, K. Nakamura, S. Ukai, N. Ebisawa, K. Tomura, Y. Nagai, S. Hayashi, S. Yoneda, T. Okuda, T. Ohtsuka
    • Organizer
      the 17th International Conference on Fusion Reactor Materials (ICFRM-17)
    • Place of Presentation
      Aachen, Germany
    • Year and Date
      2015-10-15
    • Related Report
      2015 Research-status Report
    • Int'l Joint Research
  • [Presentation] ODS鋼におけるナノ酸化物粒子・クラスターの形成機構2015

    • Author(s)
      大野直子、中村顕、鵜飼重治、林重成、大塚智史、奥田隆成
    • Organizer
      日本金属学会2015年秋期講演大会
    • Place of Presentation
      九州大学伊都キャンパス(福岡市)
    • Year and Date
      2015-09-17
    • Related Report
      2015 Research-status Report
  • [Presentation] Nucleation of oxide particles in ODS ferritic steels2015

    • Author(s)
      N. Oono, K. Nakamura, S. Ukai, S. Hayashi, S. Ohtsuka and T. Okuda
    • Organizer
      the 2015 International Symposium for Advanced Materials Research (ISAMR 2015)
    • Place of Presentation
      Sun Moon Lake, Taiwan
    • Year and Date
      2015-08-17
    • Related Report
      2015 Research-status Report
    • Int'l Joint Research / Invited
  • [Presentation] ODSフェライト鋼のナノ酸化物粒子析出過程2015

    • Author(s)
      大野直子, 中村顕, 鵜飼重治, 林重成, 米田鈴枝, 海老澤直樹, 戸村恵子, 永井康介, 奥田隆成, 大塚智史
    • Organizer
      日本金属学会第156回春期講演大会
    • Place of Presentation
      東京大学(東京都目黒区)
    • Year and Date
      2015-03-19
    • Related Report
      2014 Research-status Report
  • [Presentation] ODSフェライト鋼の酸化物粒子析出機構(Presipitation mechanism of Oxide Particle in Oxide Dispersion Strengthened (ODS) Steel)2014

    • Author(s)
      N. Oono, K. Nakamura, S. Ukai, N. Ebisawa, K. Tomura, K. Nagai, S. Hayashi, S. Yoneda, T. Okuda, S. Ohtsuka
    • Organizer
      International Symposium on Utilization of Research Reactors for Material Studies
    • Place of Presentation
      東北大学(宮城県仙台市)
    • Year and Date
      2014-12-11
    • Related Report
      2014 Research-status Report

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Published: 2014-04-04   Modified: 2018-03-22  

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