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Aerosol-assisted synthesis of metal-organic frameworks

Research Project

Project/Area Number 26820344
Research Category

Grant-in-Aid for Young Scientists (B)

Allocation TypeMulti-year Fund
Research Field Reaction engineering/Process system
Research InstitutionHiroshima University

Principal Investigator

Kubo Masaru  広島大学, 工学(系)研究科(研究院), 助教 (00633752)

Project Period (FY) 2014-04-01 – 2016-03-31
Project Status Completed (Fiscal Year 2015)
Budget Amount *help
¥4,030,000 (Direct Cost: ¥3,100,000、Indirect Cost: ¥930,000)
Fiscal Year 2015: ¥1,690,000 (Direct Cost: ¥1,300,000、Indirect Cost: ¥390,000)
Fiscal Year 2014: ¥2,340,000 (Direct Cost: ¥1,800,000、Indirect Cost: ¥540,000)
KeywordsMetal-organic frameworks / 多孔質材料 / 噴霧乾燥 / エアロゾル / 結晶成長 / 多孔性配位高分子 / 液滴噴霧 / Metal-Organic Frameworks / 窒素吸着 / ナノ粒子
Outline of Final Research Achievements

Novel aerosol-assisted synthetic process of metal-organic frameworks (MOFs), which are porous materials consisting of metal ion and organic linkers, was developed. Effects of process parameters on the physico-chemical characteristics of the products was investigated.
The spraying of precursor solution of MOF and subsequent evaporation of the sprayed droplets by heating generated MOF crystals continuously. Effects of process parameters, such as heating temperature, evaporation time, concentration of the solution, and precursor, on the crystal structure, morphology, porous characteristics of the products was clarified.

Report

(3 results)
  • 2015 Annual Research Report   Final Research Report ( PDF )
  • 2014 Research-status Report
  • Research Products

    (8 results)

All 2015 2014

All Presentation (7 results) (of which Invited: 1 results) Funded Workshop (1 results)

  • [Presentation] エアロゾルプロセスで合成した磁性ナノ粒子内包MOFの吸着挙動2015

    • Author(s)
      久保 優、森山 黎奈、島田 学
    • Organizer
      第29回日本吸着学会研究発表会
    • Place of Presentation
      徳島
    • Year and Date
      2015-11-19
    • Related Report
      2015 Annual Research Report
  • [Presentation] 磁性ナノ粒子を内包した多孔性配位高分子HKUST-1の気中連続合成2015

    • Author(s)
      森山 黎奈、久保 優、島田 学
    • Organizer
      化学工学会 第47回秋季大会
    • Place of Presentation
      北海道
    • Year and Date
      2015-09-09
    • Related Report
      2015 Annual Research Report
  • [Presentation] エアロゾルプロセスによる材料合成2015

    • Author(s)
      久保優
    • Organizer
      第9回中四国若手CE合宿
    • Place of Presentation
      広島
    • Year and Date
      2015-09-04
    • Related Report
      2015 Annual Research Report
    • Invited
  • [Presentation] エアロゾルプロセスによる多孔性配位高分子の連続合成2015

    • Author(s)
      久保 優、斎藤輝晶、島田 学
    • Organizer
      化学工学会 第80年会
    • Place of Presentation
      東京
    • Year and Date
      2015-03-21
    • Related Report
      2014 Research-status Report
  • [Presentation] 多孔性配位高分子の気中連続合成プロセス2014

    • Author(s)
      斎藤輝晶、久保 優、島田 学
    • Organizer
      化学工学会中国四国支部大学院生発表会
    • Place of Presentation
      広島
    • Year and Date
      2014-12-05
    • Related Report
      2014 Research-status Report
  • [Presentation] 多孔性配位高分子HKUST-1の気中連続合成プロセス2014

    • Author(s)
      斎藤輝晶、久保 優、島田 学
    • Organizer
      化学工学会 第46回秋季大会
    • Place of Presentation
      福岡
    • Year and Date
      2014-09-19
    • Related Report
      2014 Research-status Report
  • [Presentation] エアロゾルプロセスによるナノ材料の開発2014

    • Author(s)
      久保 優
    • Organizer
      材料化学システム討論会2014
    • Place of Presentation
      東京
    • Year and Date
      2014-09-08
    • Related Report
      2014 Research-status Report
  • [Funded Workshop] 2015 AIChE Annual Meeting2015

    • Place of Presentation
      Saltlake City (USA)
    • Year and Date
      2015-11-07
    • Related Report
      2015 Annual Research Report

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Published: 2014-04-04   Modified: 2017-05-10  

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