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1991 Fiscal Year Final Research Report Summary

Cooperative study for micro crystal and cluster, and its growth process using the synchrotron radiation beam

Research Project

Project/Area Number 01045006
Research Category

Grant-in-Aid for international Scientific Research

Allocation TypeSingle-year Grants
SectionUniversity-to-University Cooperative Research
Research InstitutionUniversity of Tsukuba and State University of New York at Stony Brook

Principal Investigator

WAKATSUKI Masao  University of Tsukuba, Institute of materials science, 物質工学系, 教授 (50114153)

Co-Investigator(Kenkyū-buntansha) WEIDENR D. J.  State Univ. New York at Stony Brook, Dept. earth & space sciences, State Univ, Proffessor
VAUGHAN M. T  State Univ. New York at Stony Brook, Dept. earth & space sciences, State Univ, Professor
PARISE J. B.  State Univ. New York at Stony Brook, Dept. earth & space sciences, State Univ, Professor
YURIMOTO Hisayoshi  University of Tsukuba, Institute of geoscience, 地球科学系, 助手 (80191485)
NAKAI Izumi  University of Tsukuba, Institute of chemistry, 化学系, 講師 (90155648)
TAKANO Kaoru  University of Tsukuba, Institute of materials science, 物質工学系, 助教授 (60133005)
KURITA Kei  University of Tsukuba, Institute of geoscience, 地球科学系, 助教授 (00111451)
FUKUTANI Hirohito  University of Tsukuba, Institute of physics, 物理学系, 教授 (40011580)
OHSHIMA Kenichi  University of Tsukuba, Institute of applied physics, 物理工学系, 助教授 (70109271)
AOKI Sadao  University of Tsukuba, Institute of applied physics, 物理工学系, 助教授 (50016804)
FUJII Yasuhiko  University of Tsukuba, Institute of materials science, 物質工学系, 教授 (00013524)
SUENO Shigeho  University of Tsukuba, Institute of geoscience, 地球科学系, 教授 (30110513)
Project Period (FY) 1989 – 1991
KeywordsSynchrotron radiation / Crystal synthesis / X-ray diffraction / High pressure experiment / Phase transition / Multiple thin film / Earth's deep material / Na-matal
Research Abstract

University of Tsukuba (UT) and State University of New York at Stony Brook (SB) have advanced several cooperative researches in connection with the field of growth mechanism of micro particles and micro crystals for both experimental and theoretical view points. Last three years, both universities have exchanged two to four researchers every year in the period of several days to one month for the cooperative researches, lectures, and discussion. Main mutually interested research fields are as follows :
(a) High temperature-high pressure material research : This research is popular for both universities in the field of geoscience. Experiments of crystal synthesis under static high pressure condition were carried out mostly in SB (Liebermann, Weidner and Kurita), and in situ observations of high pressure synthesis using SOR beam were performed in KEK, Tsukuba (Kurita, Wakatsuki, Liebermann, Weidner and Vaughan).
(b) Single crystal structure analysis and chemical composition analysis : Hydr … More ogen and trace elements analysis were carried out (Yurimoto, Sueno and Nakai) in UT for the mineral specimens synthesized in SB.
(c) Small angle scattering : Application of CCD detector on the scattering experiments were discussed and cooperatively studies (Chu, Sueno).
(d) Micro crystal analysis : Techniques on the sub-micron size single crystal structure analysis were studied. Especially, techniques for making a micro-beam and method for holding a specimen were the object of mutual interest.
(e) EXAFS : EXAFS spectra analysis using SOR beam were carried out in NSLS for the metal elements in a amorphous material (Parise and Nakai).
(f) X-ray microscope : Development of X-ray microscope continuing using SOR beam in NSLS and KEK (Aoki and Kirtz),
(g) Phase transition and X-ray diffuse scattering : Martensite transition on Na and other metal elements were studied cooperatively by Stephens and Ohsima.
(h) Lecture : Exchange researchers most of time had chances to have lectures in both universities. Most fruitful effects of this exchange program is the establishment of the mutual confidence and the friendship. Less

  • Research Products

    (11 results)

All Other

All Publications (11 results)

  • [Publications] 若槻 雅男: "An optical high pressure cell with spherical sapphire anvils" Rev.Sci.Instrum.62. 1576-1580 (1991)

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] 末野 重穂: "Impurities dislocation diffusion in singleーcrystal MgO" Mater.Sci.Eng.B. (1992)

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] 藤井 保彦: "Systematics in the modulated phases of 〔N(CH_3)_4〕_2MnCl_4" J.Phys.:Condens.Matter. 3. 3387-3391 (1991)

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] 大嶋 建一: "Xーray diffraction study of Fe/MgO multilayered films with an enhanced magnetization" J.Phys.:Condens.Matter. 3. 5921-5927 (1991)

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] Weidner,D.J.: "Phase transition and thermal expansion of MgSiO perovskite:Implications for the compositon of the Earth's lower mantle" Science. 251. 410-413 (1991)

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] Vaughan,M.T.: "Large volume high pressure research using the wiggler port at NSLS" High Pressure Research. (1992)

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] Wakatsuki, Masao: "An optical high pressure cell with spherical sapphire anvils" Rev. Sci. Instrum.62. 1576-1580 (1991)

    • Description
      「研究成果報告書概要(欧文)」より
  • [Publications] Sueno, Shigeho: "Impurities dislocation diffusion in single-crystal MgO" Mater. Sci. Eng. B. (1992)

    • Description
      「研究成果報告書概要(欧文)」より
  • [Publications] Fujii, Yasuhiko: "Systematics in the modulated phases of N (CH_3) _4 _2 MnCl_4" J. Phys. : Condens. Matter. 3. 3387-3391 (1991)

    • Description
      「研究成果報告書概要(欧文)」より
  • [Publications] Ohshima, Kenichi: "X-ray diffraction study of Fe/MgO multilayered films with an enhanced magnetization" J. Phys. : Condens. Matter. 3. 5921-5927 (1991)

    • Description
      「研究成果報告書概要(欧文)」より
  • [Publications] Weidner, D. J.: "Phase transition and thermal expansion of MgSiO_3 perovskite : Implications for the composition of the Earth's lower mantle" Science. 251. 410-413 (1991)

    • Description
      「研究成果報告書概要(欧文)」より

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Published: 1993-03-16  

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