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1993 Fiscal Year Final Research Report Summary

A New Area in Organic Electrochemistry-Electrode Processes in Peculier Electrode Interfacial Reaction Fields-

Research Project

Project/Area Number 04303007
Research Category

Grant-in-Aid for Co-operative Research (A)

Allocation TypeSingle-year Grants
Research Field 工業物理化学・複合材料
Research InstitutionTokyo Institute of Technology

Principal Investigator

NONAKA Tsutomu  Tokyo Institute of Technology, Professor, 大学院・総合理工学研究科, 教授 (00016528)

Co-Investigator(Kenkyū-buntansha) SASAKI Kazuo  Hiroshima University, Professor, 工学部, 教授 (00034322)
TAKEHARA Zen-ichiro  Kyoto University, Professor, 工学部, 教授 (00025892)
FUJISHIMA Akira  Tokyo University, Professor, 工学部, 教授 (30078307)
OSA Tetsuo  Tohoku University, Professor, 薬学部, 教授 (10010753)
SUGINOME Hiroshi  Hokkaido University, Professor, 工学部, 教授 (00000779)
Project Period (FY) 1992 – 1993
KeywordsElectrochemistry / Modified electrodes / Electrode interface / Reaction field / Organic chemistry
Research Abstract

A new area in organic electrochemistry was developed by cosidering deeply a new basic concept, that is to control purposively electrolytic reactions by controlling the structures and properties of electrode interfaces where they take place. From this concept, the following three principles and methodologies were suggested :
(1) Design and control of three-dimensionally modified electrode interfaces with functions of molecular discrimination, selective orientation, permeation and absorption, chirality, etc.
(2) Design and control of supla-ionic electrode interfaces consisting of systems of solid electrolyte, gas phase, super-acid and base, reactive and ultrahydrophobic electrodes, etc.
(3) Design and control of energy-irradiated electrode interfaces in plasma, magnetic field, ultrasonication, pholysis, high voltage, etc.

  • Research Products

    (106 results)

All Other

All Publications (106 results)

  • [Publications] M.Umezawa: "Electroreductive Polymerization of Dichlorocarbosilanes" Electrochimica Acta. 38. 529-533 (1993)

    • Description
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  • [Publications] Po-Chung Cheng: "Electroreduction of Methy.1 Cinnamate Using a Rotating Cylinder Electrode" Journal of Electrochemical Society of Japan. 61. 218-223 (1993)

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  • [Publications] Shu-Yong Guo: "Maximum in Oxidizing Power of Anodically-Generated Br-Cl Composite-Reqaqents" Journal of Electrochemical Society of Japan. 61. 245-246 (1993)

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      「研究成果報告書概要(和文)」より
  • [Publications] Po-Chang Chen: "Electron-Transfer Process in Emulsion Electrolysis" Journal of Electrochemical Society of Japan. 61. 886-887 (1993)

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  • [Publications] Yoshihito Kunugi: "Electroorganic Reactions on Organic Electrodes.Part 18" Journal of Electroanalytical Chemistry. 353. 209-215 (1993)

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      「研究成果報告書概要(和文)」より
  • [Publications] Yoshihito Kunugi: "Preparation of Hydrophobic Zinc and Lead Electrodes and Their Application to Electroreduction of Organic Compounds" Journal of Electroanalytical Chemistry. 356. 163-169 (1993)

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      「研究成果報告書概要(和文)」より
  • [Publications] Yoshihito Kunugi: "Electrolysis of Emulsions of Organic Compounds" Journal of Electrochemical Society. 140. 2833-2836 (1993)

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      「研究成果報告書概要(和文)」より
  • [Publications] 野中勉: "電極電子化学" 電気学会誌. 113. 727-731 (1993)

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  • [Publications] 野中勉: "有機電解用電極材料の新展開" 表面. 31. 737-745 (1993)

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  • [Publications] 野中勉: "疎水性電極による有機電解" 化学工業. 45. 127-130 (1994)

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  • [Publications] K.Momota et al.: "Electrochemical Fluorination of Aromatic Compounds in Liquid R_4NF・mHF-PartI. Basic propcrties of R_4NF・mHF and the fluorination of benzene,fluorobenzcne and 1,4-difluorobenzene" Electrochim.Acta. 38. 1123-1130 (1993)

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  • [Publications] Y.Matsuda et al.: "Electrochemical Fluorination of Aromatic Compounds" 1993 Intemat.Symp.Organic Reactions Tainan,Book of Abstracts. 51-52 (1993)

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  • [Publications] K.Momota et al.: "Electrochemical Fluorination of Aromatic Compounds in Liquid R_4NF・mHF-PartII.Fluorination of di-and tri-fluorobenzenes" Electrochim.Acta. 39. 41-49 (1994)

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  • [Publications] 百田邦尭 他: "電解フッ素化法によるポリフルオロシクロヘキサジェンの合成" 電気化学. 62. 33-38 (1994)

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  • [Publications] Yasuhiro Sato: "Electrochemical Oxy-trifluoromethylation of Butyl Acrylate" Bull.Chem.Soc.Jpn.,. 66. 1840-1843 (1993)

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  • [Publications] Masafumi Kobayashi: "Electrochemical Oxidation of 2-Substituted 3-N-(Arylamino)4,4,4,-trifluoro-2-butencate" J.Org.Chem.59. (1994)

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  • [Publications] Kenji Uneyama: "Electrochemical Oxidation of N,N'-Disubtituted Trifluoroethanimidumides" J.Org.Chem.59. 印刷中 (1994)

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  • [Publications] K.Momota et al.: "Electrochemical Fluorination of Aromatic Compounds in Liquid R_4NF・mHF-PartIII. Fluorination of trifluoromethylbenzenes" Electrochim.Acta. in press

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      「研究成果報告書概要(和文)」より
  • [Publications] K.Ohkawa: "Electrochemical Reduction of Carbon Dioxide on Hydrogen-Storing Materials PartI. The Effect of Hydrogen Absorption on the Electrochemical Behavior on Palladium Electrodes." J.Electroanal.Chem.345. 445-456 (1993)

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  • [Publications] J.Rabani: "Oxdation Kinetics of a Ru(bby)_3^<3+> Derivative in Langmuir-Blodgett Layers. Comparison to Ru(bby)_3^<3+> in Homogeneous Solution" Langmuir. 9. 819-823 (1993)

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  • [Publications] T.Amemiya: "Frequency-Resolved Faradaic Processes in Polypyrrole Films Observed by Electromodulation Techniques:Electrochemical Impedance and Color Impedance Spectroscopies" J.Phys.Chem.97. 4187-4191 (1993)

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  • [Publications] T.Amemiya: "Dynamics of Faradaic Processed in Polypyitole/Polystyrenesulfonate Composite Films in tthe Presence and Absences of Redox Species in Aqueou Solutions" J.Phys.Chem.97. 4192-4195 (1993)

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  • [Publications] O.Sato: "Self-Ordered Film of Hemicynine Derivative Characterized by Phase-Sensitive Optical Sccond-Harmonic Generation" Jpn.J.Appl.32 Part1. 1201-1203 (1993)

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  • [Publications] K.Morigaki: "Electrochemical Counting of Photon Number Using the Assembled Monolayer Film of Azo Compound" Sensors and ActuatorsB. 13-14. 226-229 (1993)

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  • [Publications] L.A.Nagahara: "Scanning Probe and Transmission Electron Microscopy Observations of Cobalt Naphthalocyanine Molecules Deposited onto a NaCl Substrate" J.Vac.Sci.Technol.A. 11. 781-785 (1993)

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  • [Publications] R.Baba: "Characterization of the Molecular Orientation in LB Films of Rhoxlamine B Derivatives by the Optical Second Harmonic Gencration Cohcrcnt Interferomctry" 電気化学. 61. 1030-1031 (1993)

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  • [Publications] K.Kobayakawa: "Enhancement of the photocatalytic Activity of CdS for Hydrogen Evolution from Aqucous Sulfite Solution by Heat Treatment with KCl" Solar Energy Materials and Solar Cells. 30. 201-209 (1993)

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  • [Publications] K.Morigaki: "In-Site Electrochemical Actinometry Using an Azobenzene Derivatibve Monolayer Film" Ber.Bunsengs.Phys.Chem.97. 860-864 (1993)

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  • [Publications] T.Amemiya: "Faradaic Charge Transfer with Double-Layer Charging and/or Adsorption-Rclated Charging at Polymer-Modified Electrodes as Obscrvcd by Color Impcdance Spcctroscopy," J.Phys.Chem.97. 9736-9740 (1993)

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  • [Publications] R.Cai: "Photoelectrochemistry of TiO_2 Particles:Efficient Electron Transfer from TiO_2 Particles to a Redox Enzyme," J.Electroanal.Chem.360. 237-245 (1993)

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  • [Publications] Shouryu Lee: "Enzyme-Modified Langmuir-Blodgett membranes in Glucose Electrodes Based on Avidin-Biotin Interaction" Sens.Actuators B. 12. 153-158 (1993)

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  • [Publications] Jun-ichi Anzai: "Use of the Avidin-Biotin System for Immobilization of an Enzyme on the Electrode Surface." Sens.Actuators B. 13-14. 73-75 (1993)

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  • [Publications] Jun-ichi Anzai: "Protein Sensors Based on the Potentiometric Photoresponse of Polymer Membranes Doped with Photochromic Spiropyran." Anal.Chim.Acta. 281. 543-548 (1993)

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  • [Publications] Jun-ichi Anzai: "Crown-Ether Amphiphilies for the Preparation of lon-Binding Langmuir-Blodgett Films." Mater.Sci.Eng.C1. L1-L3 (1993)

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  • [Publications] Jun-ichi Anzai: "Potentiometric Response of Glassy Carbon Electrodes Coated with Grown Ether LB Film." DENKI KAGAKU. 61. 830-831 (1993)

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  • [Publications] Yoshitomo Kashiwagi: "Electrocatalytic Oxidative Coupling Reaction of Naphthols and Naphthol Ethers." Chem.I.ett.81-84 (1993)

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  • [Publications] Yoshitomo Kashiwagi: "Electrocatalytic Oxidative Coupling of Methylquinolines on TEMPO-Modified Graphite Felt Electrodes." Chem.Lctt.257-260 (1993)

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  • [Publications] Yoshitomo Kashiwagi: "Electrocatalytic Oxidation of NADH on Thin Poly(acrylic acid)Film Coated Graphite Felt Electrode Coimmobilizing Ferrocene and Diaphorase." Chem.Lett.677-680 (1993)

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  • [Publications] Tetsuo Osa: "Electroenzymatic Oxidation of Alcohol on a Poly(acryl acid)-coated Graphite Felt Electrode Terimmobilizing Ferrocene,Diaphorase and Alcohol Dehydrogenase." Chem.Lctt.367-370 (1994)

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  • [Publications] Tomonori Hoshi: "Electrochemical Deposition of Avidin on the Surface of Platinum Electrode for Enzyme Sensor Applications." Anal.Chim.Acta. (1994)

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  • [Publications] Jun-ichi Anzai: "Avidin-Biotin Complexation for Enzyme Sensor Applications." Trends Anal.Chem.(1994)

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  • [Publications] Jun-ichi Anzai: "Electrochemical Preparation of Active Avidin Film for Enzyme Sensor Applications." Chem.Lett.1231-1234 (1993)

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  • [Publications] Iwao Suzuki: "Electrochemical Conversion of Alcohols into Aldehydes Mediated by Lipophilic γ-Cyclodextrin Bearing a Ferrocene Moiety." Chem.Lett.1719-1722 (1993)

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  • [Publications] 長哲郎: "光応答センサーの臨床応用" 日本臨床検査自動化学会会誌. 18. 739-741 (1993)

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  • [Publications] 長哲郎: "高分子修飾電極を用いる電解合成." 化学工業. 45. 121-126 (1994)

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  • [Publications] H.Yamada: "Determination of Active Diaphorase Immobilized at Electrode Surfaces" Bioelectrochem.Bioenerg.29. 387-346 (1993)

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  • [Publications] M.Nishizawa: "Surface Pretreatment for Electrochemical Fabrication of Ultrathin,Patterned Conducting Polymers" J.Electrochem.Soc.140. 1650-1655 (1993)

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  • [Publications] M.Nishizawa: "Fabrication of a pH-Sensitive Microarray Electrode and Applicability to Biosensors" Sensors and Actuators B. 13-14. 53-56 (1993)

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  • [Publications] M.Nishizawa: "Electrochemical in situ Conductivity Measurements of C60 Thin Films" J.Electroanal.Chem.353. 329-334 (1993)

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  • [Publications] T.Matsue: "Microring-ring Electrode for Manipulation of a Single Cell." Biochim.Biophys.Acta. 1157. 332-335 (1993)

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  • [Publications] A.Kabasawa: "Gas Sensing Using Microring-ring Electrode.Application to a Gas Chromatographic Detector." Denki Kagaku. 61. 825-826 (1993)

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  • [Publications] H.Yamada: "Electron-Transfer at a Planar Lipid Membrane Incorporated with 7,7,8,8-Tetracyanoquinodimethane Studied by AC Impedance Spectroscopy." J.Phys.Chem.97. 9547-9549 (1993)

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  • [Publications] 末永智一: "アレイ電極を用いる酵素センサ" 化学工業. 44. 801-804 (1993)

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  • [Publications] 西澤松彦: "“極微"電解重合反応とその応用" 化学工業. 45. 159-163 (1993)

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  • [Publications] Y.Iijima: "Influence of Magnetic Fields on Growth Pattern and Microstructure of Electrochemically Polymerized Thiophene(I)" Proc.of the Symp.on Electrochemically Deposited Thin Films. 93-26. 237-246 (1993)

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  • [Publications] S.Yamanaka: "Magnetic Field Effect on Electron Transfer Process in Electrochemical Reaction" Sci.Rep.RITU. 38. 399-405 (1993)

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  • [Publications] I.Mogi: "Effect of High Magnetic Fields on Morphology in Electroless Deposition of Silver" Proc.of the 2nd Int.Symp.on Electrochemical Processing of Tailored Materials. 93-12. 136-146 (1993)

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  • [Publications] S.Okubo: "A Morphological Study of Electroless Deposition in High Magnetic Fields" Sci.Rep.RITU. 38. 383-389 (1993)

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  • [Publications] I.Mogi: "Effect of High Magnetic Fields on Fractal Growth of Lead Metal-Leaves" J.Cryst.Growth. 128. 258-261 (1993)

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  • [Publications] Y.Sasaki: "Mixed Chromium(III)-Ruthenium(III) Trinuclear Complex,[GrRu2(M3-0)(M-CH3C00)6(pyridine)3]+^+" Chemistry Letters. 69-72 (1993)

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  • [Publications] 木谷晧: "可溶性導電性高分子" 高分子加工. 42. 418-423 (1993)

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  • [Publications] Akira Kitani: "Effect of Flavin Coenzymes on Current Response for Glucose at Glucose Oxidase/Polypyrrole Electrodes" Electrochim.Acta. 39. 7-8 (1994)

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  • [Publications] H.Yamada: "Microvoltammetric Characterization of Diaphorase Monolayer at Glass Surfaces." Bioelectrochem.Bioenerg.(印刷中).

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  • [Publications] T.Matsue: "Microamperometric Estimation of Photosynthesis Inhibition in a Single Protoplast" Biochem.Biophys.Res.Commun.(印刷中).

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  • [Publications] M.Nishizawa: "Ultrathin Polypyrrole Formed at a Twin-Microband Electrode in the Presence of Dodecyl Sulfate" J.Electroanal.Chem.(印刷中).

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  • [Publications] Tatsuya Shono: "An Electroreductively Promoted Unusual Coupling of Benzoic Acid Esters." Denki Kagaku. 61. 870-871 (1993)

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  • [Publications] Tatsuya Shono: "Reductive Homo-Coupling of 2-Aryl-2-Oxazolinium Salts." Tetrahednon Letters. 34. 3577-3580 (1993)

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  • [Publications] Tatsuya Shono: "Eleatroreduetively Promoted Diatereoselactive Coupling of Ketonos with Allylic Alihols.Synthesis of Optically Active 1.4-Diols." Journao of Organic Chemstry. 59. 印刷中 (1994)

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  • [Publications] Tatsuya Shono: "Electroreductive Coupling of Ketone with O-Methyl Oxime,N,N-Dimethyl hydrazone,and Nitrone.A Convenient Route to Synthesis of B-Amin・Alcohel" Journal of Organic Chemistry. 59. 印刷中 (1994)

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  • [Publications] Tatsuya Shono: "John Wiley & Sons Ltd." Supplement E:The Chemistry of Hydroxyl,Ether and Peroxide Groups,vol.2 Charpter 16. 10 (1993)

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  • [Publications] Sotaro Ito: "Evidence for Hydroxyl Radicals as an Active Species Generated from Udenfriend's Reagent" J.Chem.Soc.Perkin Trans.2. 1993. 255-259 (1993)

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  • [Publications] Toshihiro Koyama: "Electrochemical C-C Double Bond Cleavage Reaction of Styrene with Molecular Oxyqen Mediated by CuCl2" Chem.Lett.1993. 395-398 (1993)

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  • [Publications] Sotaro Ito: "Duet Electrosynthesis.II 1,4-Naphtoquinone from Naphthalene" J.Appl.Electrochem.23. 677-683 (1993)

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  • [Publications] Yoshihiro Shimizu: "Electrochemical Reduction of Nicotinamide Coenzyme Mediated with Rhodium Ion Immobilized in Polymer" Denki Kagaku. 61. 872-873 (1993)

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  • [Publications] Sotaro Ito: "A Possible Model Reaction of Dopamine Β-Monooxygenase" Chem.Lett.1993. 461-464 (1993)

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  • [Publications] Akira Kitani: "Improvement of Mechanical Properties of Electropolymerized Polyaniline" Synth.Met.57. 3566-3570 (1993)

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  • [Publications] M.Tezuka: "Voltammetric Study on CO2 Reduction Electrocatalyzed by Cobalt Tetraphenylporphine in DMF Solution" Chem.Lett.427-430 (1993)

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  • [Publications] M.Tezuka: "Anodic Hydrogen Evolution in Contact Glow-Discharge of Sulfuric Acid Solution" DENKI KAGAKU. 61. 794-795 (1993)

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  • [Publications] M.Inaba: "Application of the Solid Polymer Electrolyte Method to Organic Electrochemistry XIV" J.Electrochem.Soc.140. 19-22 (1993)

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  • [Publications] M.Inaba: "Application of the Solid Polymer Electrolyte Method to Organic Electrochemistry XV" J.Electrochem.Soc.140. 706-711 (1993)

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  • [Publications] M.Inaba: "Reduction of Nitrobenzene on Solid Polymer Electrolyte Composite Electrodes Using a Hydrocarbon Sulfonate Ion-Exchange Membrane" Chem.Lett.1993. 1779-1782 (1993)

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  • [Publications] 大塚,潔: "ケミカルズ/電力コジュネレイション法によるフェノールの一段合成" 触媒. 35. 422-425 (1993)

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  • [Publications] Kiyoshi Otsuka: "Reduction of Nitrous Oxide by Electrochemically-generated Spillover Hydrogen" Studies Surf.Sci.Catal.77. 117-123 (1993)

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  • [Publications] Ichiro Yamanaka: "Partial Oxidation of Cyclohexane with Reductively Activated Dioxygen on SmCl3 Supported on Graphite" J.Chem.Soc.Faraday Trans.89. 1791-1797 (1993)

    • Description
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  • [Publications] Kiyoshi Otsuka: "Epoxidation of Cyclohexene with the Nascent Oxygen Generated by Electrolysis of Water" J.Chem.Soc.,Chem.Commun.611-612 (1993)

    • Description
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  • [Publications] Ichiro Yamanaka: "Partial Oxidation of Alkanes and Aromatics with Activated Oxygen over an SmCl3-embedded Graphite Cathode" J.Alloys and Compounds. 193. 56-58 (1993)

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  • [Publications] M Shibata: "Selective oxidation of the aldehyde functional group in the glycolaldehyde molecule at Pt electrodes modified b Sb ad-atoms" J.Electroanal.Chem.344. 389-393 (1993)

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] 古屋長一: "燃料電池一高効率 無公害発電" 化学と教育. 41. 312-316 (1993)

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] M.Shibata: "Selectiveoxidation of the aldehyde functional group in the glxcd-aldehyde molecule at Pt electrodes modified by ad-atans" Electrochim.Acta. (印刷中). (1994)

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] 成塚智: "Electrolytic Partial Fluorination of Organic Compounds.8.Highly Regioselective Anodic Monofluorination of B-Lactans" The Journal of Organic Chemistry. 58. 4200-4201 (1993)

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] 成塚智: "Electrolytic Partial Fluorination of Organic Compounds.VII Diastereoselective Electrofluorination of 4-Thianae Derivatires" 電気化学協会誌. 61. 868-869 (1993)

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] 淵上寿雄: "Regioselective Anodic Mechoxylation of N-(Fluaroethyl)anines. Preparation of Highly Useful Fluoroalkylated Building Blocks" The Journal of Organic Chemistry. 59(印刷中). (1994)

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] 淵上寿雄: "Electrolytic Partial Fluorination of Organic Conpounds IX.Selective Anodic Monofluorination of Hydrazones" Journal of Electroanalytical Chemistry. (印刷中). (1994)

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] 淵上寿雄: "Selecive Anodic Partial Fluorination of Heteroatom Compounds" Reviews on Heteroatom Chemistry. 10(印刷中). (1994)

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] 手塚還: "グロー放電電解とそれを利用する有機反応" 化学工業. 45. 150-154 (1994)

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] 手塚還: "半導体工場の排水処理と環境安全対策" クリーンテクノロジー. 3-12. 30-33 (1993)

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] Kiyoshi Otsuka: "Synthesis of Dimethyl Carbonate by Electrolytic Carbonylation of Methanol in the Gas Phase" Chem.Lett. 1994(in press). (1994)

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] Kiyoshi Otsuka: "An Electrochemical Membrane Reactor for Selective Hydrogenation of Acetylene in Abundant Ethylene" J.Catal.145(in press). (1994)

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] 大塚潔: "電池を応用した合成反応" 表面. 32(in press). (1994)

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] T.Nonaka: "New Functionality Materials,Vol.C(ed by M.Doynama)" Elsevier Sci.Bub.B.V., 6 (1993)

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] Po-Chung Cheng: "Electroreduction of Methyl Cinnamate Using a Rotating Cylinder Electrode" Jounal of Electrochemical Society of Japan. 61. 218-223 (1993)

    • Description
      「研究成果報告書概要(欧文)」より
  • [Publications] Jun-ichi Anzai: "Use of Avidin-Biotin System for Immobilization of an Enzyme on the Electrode Surface" Sensor Actuators B. 13-14. 73-75 (1993)

    • Description
      「研究成果報告書概要(欧文)」より
  • [Publications] R.Cai: "Photoelectrochemistry of TiO_2 Paticles : Efficient Electron Transfer from TiO_2 Particles to a Redox Enzyme" Journal of Electroanalytical Chemistry. 360. 237-245 (1993)

    • Description
      「研究成果報告書概要(欧文)」より
  • [Publications] Masao Tokuda: "New Total Synthesis of (+) -N-Methylanisomycin by Anodic Cyclization of Alkenylamine" Tetrahedron. 49. 2413-2426 (1993)

    • Description
      「研究成果報告書概要(欧文)」より
  • [Publications] M.Inaba: "Application of the Solid Polymer Electrolyte Method to Organic Electrochemistry XIV" Journal of Electrochemical Society. 140. 19-22 (1993)

    • Description
      「研究成果報告書概要(欧文)」より
  • [Publications] Sotaro Ito: "Duet Electrosynthesis. II.1,4-Naphtoquinone from Naphthalene" Journal of Applied Electrochemistry. 23. 677-683 (1993)

    • Description
      「研究成果報告書概要(欧文)」より

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Published: 1996-04-15  

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