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1996 Fiscal Year Final Research Report Summary

Development of High Performance Metallic Materials through Nano-crystalline Structure Control

Research Project

Project/Area Number 06044019
Research Category

Grant-in-Aid for international Scientific Research

Allocation TypeSingle-year Grants
SectionJoint Research
Research InstitutionTohoku University

Principal Investigator

FUJIIMORI Hiroyasu  Institute for Materials Research, Tohoku University, Professor, 金属材料研究所, 教授 (60005866)

Co-Investigator(Kenkyū-buntansha) 琴 榮和  韓国科学技術研究院(KIST), 研究院
文 仁ごう  韓国科学技術研究院(KIST), 研究員
金 喜中  韓国科学技術研究院(KIST), 研究員
盧 秦ふちん  韓国科学技術研究院(KIST), 研究員
SHIMA Toshiyuki  Institute for Materials Research, Tohoku University, 金属材料研究所, 助手 (50261508)
HANADA Shyuzi  Institute for Materials Research, Tohoku University, 金属材料研究所, 教授 (10005960)
MASUMOTO Tuyoshi  The Research Institute of Electric and Magnetic Materials, 所長 (20005854)
CHANG J.Y  Division of Metals, Korea Institute of Science and Technology
MOON I.G  Division of Metals, Korea Institute of Science and Technology
KIM H.S  Division of Metals, Korea Institute of Science and Technology
NOH T.H  Department of Metallurgical Engineering, Andong National University
Project Period (FY) 1994 – 1996
KeywordsHigh Strength Al Base Alloy / High Temperature Nb_3 Al Compound / Nano-crystalline Material / Structural Control / High Mechanical Strength / Ductility / Soft Magnet / Hard Magnet
Research Abstract

We investigated the effect of nano-crystalline structural control on mechanical, magnetic and electrical properties of various types of metallic materials. The results obtained are as follows :
1) The methods for nano-crystalline structural control : The methods ; a mechanical alloying followed by consolidation by HIP for Nb_3 Al based nano-crystalline intermetallic compounds, a crystallization of amorphous metal followed by consolidation for Al based nano-crystalline bulk alloys, a N or O reactive sputtering for Fe based nano-crystalline or granular alloys thin films, were investigated, respectively. The alloy compositions were also investigated. Through these investigations, the following properties were obtained.
2) Nb_3 Al based nano-crystalline intermetallic compounds : Mechanically very strong and ductile properties, typical in about 60% elongation, were obtained.
3) Al based nano-crystalline bulk alloys : A nano-crystalline bulk Material of Al_<92>Mn_6Ce_2 Al_<94.5>Cr_3Ce_1Co_<1.5> and a nano-structurally mixed amorphous-crystalline bulk material of Al_<94>V_4Fe_2 were found to show mechanically very strong and ductile properties. In addition, a strong effect of rare earth elements on the formation of nano-crystalline state was found in the Al-Si based alloys.
4) Fe based nanocrystalline magnetic alloys : It was found to show high magnetic flux density and high permeability in nano-crystalline thin Fe- (Hf, Zr, Nb) -C-N alloys, high electrical resistivity and giant magnetoresistace in metal-insulator nano-granular thin films of a Fe-MgO system, high coercivity in structurally nano-columnar FeNdB/Cr multilayred thin films, and permanent magnetic properties with high magnetic flux density in nano-crystalline bulk materials of Fe-Nd-B alloys.

  • Research Products

    (22 results)

All Other

All Publications (22 results)

  • [Publications] H.Fujimori: "Tunnel-type GMR in Co-Al-O insulated granular system -Its oxygen-concentration dependence" Journal of Magnetism and Magnetic Materials. 156. 311-314 (1996)

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] S.Mitani: "Spin-dependent tunneling phenomena in insulating granular systems" Journal of Magnetism and Magnetic Materials. 165. 141-148 (1997)

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] 大沼繁弘: "Co-Al-O系 グラニュラー構造膜の高周波軟磁気特性" 日本応用磁気学会誌. 20. 489-492 (1996)

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] 小林伸聖: "Fe-X-O(X=Y,Nd,Sm,Gd,Tb,Dy)系高電気抵抗膜の軟磁気特性" 日本応用磁気学会誌. 20. 469-472 (1996)

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] 小林伸聖: "Fe-X-O(X=Y,Nd,Sm,Gd,Tb,Dy)系薄膜の磁気特性に及ぼすNi,Pd,Ptの添加効果" 日本応用磁気学会誌. 20. 473-476 (1996)

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] S.Ohnuma: "High-Frequency magnetic properties in metal-nonmetal granular films (invited)" Journal of Applied Physics. 79. 5130-5135 (1996)

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] T.Wada: "High Temperature Deformation of Nb_3Al/Nb Alloys" Materials Science Forum. 233-234. 311-318 (1997)

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] A.Inoue: "Soft and Hard Magnetic Properties of Nanocrystalline Fe-M-B (M=Zr,Nd) Base Alloys Containing Intergranular Amorphous Phase" Science Report RITU. A41. 143-156 (1996)

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] A.Inoue: "Formation and High strength of Nanoamorphous Structure in Rapidly Solidified Al-Cr-Co-Ce and Al-V-Fe Alloys" International Journal of Rapid Solidification. 103-120 (1996)

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] A.Inoue: "High Mechanical Strength of Al- (V,Cr,Mn) - (Fe,Co,Ni) Quasicrystalline Alloys Prepared by Rapid Solidification" Materials Transactions,JIM. 37. 1287-1292 (1996)

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] A.Inoue: "Synthesis and high mechanical strength of Al-based alloys consisting mainly of nanogranular amorphous particles" Materials Science and Engineering. A217/218. 401-406 (1996)

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] H.Fujimori: "Tunnel-type GMR in Co-Al-O insulated granular system -Its oxygen-concentration dependence" Journal of Magnetism and Magnetic Materials. 156. 311-314 (1996)

    • Description
      「研究成果報告書概要(欧文)」より
  • [Publications] S.Mitani: "Spin-dependent tunneling phenomena in insulating granular systems" Journal of Magnetism and Magnetic Materials. 165. 141-148 (1997)

    • Description
      「研究成果報告書概要(欧文)」より
  • [Publications] S.Ohnuma: "Soft Magnetic Properties at High Frequency of Co-Al-O Films with Granular Structure" Journal of Magnetic Society of Japan. 20. 489-492 (1996)

    • Description
      「研究成果報告書概要(欧文)」より
  • [Publications] N.Kobayashi: "Soft Magnetic Properties of Highly Electrically Resistive Fe-X-O (X=Y,Nd, Sm, Gd, Tb, Dy) Films" Journal of Magnetic Society of Japan. 20. 469-472 (1996)

    • Description
      「研究成果報告書概要(欧文)」より
  • [Publications] N.Kobayashi: "Effect of Ni, Pd, or Pt Addition on the Magnetic Properties of Fe-X-O (X=Y,Nd, Sm, Gd, Tb, Dy) Films" Journal of Magnetic Society of Japan. 20. 473-476 (1996)

    • Description
      「研究成果報告書概要(欧文)」より
  • [Publications] S.Ohnuma: "High-frequency magnetic properties in metal-nonmetal granular films (invited)" Journal of Applied Physics. 79. 5130-5135 (1996)

    • Description
      「研究成果報告書概要(欧文)」より
  • [Publications] T.Wada: "High Temperature Deformation of Nb_3Al/Nb Alloys" Materials Science Forum. 233-234. 311-318 (1997)

    • Description
      「研究成果報告書概要(欧文)」より
  • [Publications] A.Inoue: "Soft and Hard Magnetic Properties of Nanocrystalline Fe-M-B (M=Zr, Nd) Base Alloys Containing Intergranular Amorphous Phase" Science Report.RITU. A42. 143-156 (1996)

    • Description
      「研究成果報告書概要(欧文)」より
  • [Publications] A.Inoue: "Formation and High Strength of Nanoamorphous Structure in Rapidly Solidified Al-Cr-Co-Ce ad Al-V-Fe Alloys" International Journal of Rapid Solidification. 103-120 (1996)

    • Description
      「研究成果報告書概要(欧文)」より
  • [Publications] A.Inoue: "High Mechanical Strength of Al- (V,Cr, Mn) - (Fe, Co, Ni) Quasicrystalline Alloys Prepared by Bapid Solidification" Materials Transactions. JIM. 37. 1287-1292 (1996)

    • Description
      「研究成果報告書概要(欧文)」より
  • [Publications] A.Inoue: "Synthesis and high mechanical strength of Al-based alloys consisting mainly of nanogranular amorphous particles" Materials Science and Engineering. A217/218. 401-406 (1996)

    • Description
      「研究成果報告書概要(欧文)」より

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Published: 1999-03-09  

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