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2001 Fiscal Year Final Research Report Summary

Preparation of Insulating Aluminum Nitride Film by Enhanced Shielded Vacuum

Research Project

Project/Area Number 11450122
Research Category

Grant-in-Aid for Scientific Research (B)

Allocation TypeSingle-year Grants
Section一般
Research Field Electronic materials/Electric materials
Research InstitutionToyohashi University of Technology

Principal Investigator

SAKAKIBARA Takeki  Toyohashi University of Technology, Faculty of Engineering, Professor, 工学部, 教授 (10023243)

Co-Investigator(Kenkyū-buntansha) NAGAO Masayuki  Toyohashi University of Technology, Faculty of Engineering, Professor, 工学部, 教授 (30115612)
TAKIKAWA Hirofumi  Toyohashi University of Technology, Faculty of Engineering, Associate Professor, 工学部, 助教授 (90226952)
Project Period (FY) 1999 – 2001
Keywordsaluminum nitride film / vacuum arc deposition / enhanced shielded method / droplet-free / superconductor shield / magnetically filtered arc / film properties
Research Abstract

In order to fabricate the AlN film, which exhibits high electrical insulation property with high thermal conduction and is available for of electric power device, which is available for electric power devices, new reactive vacuum arc deposition system was developed. In the shielded method (S-CAD: shielded cathodic arc deposition), we found that the transparent AlN films with different crystalline orientations could be prepared by using different substrate bias. The S-CAD was further available to prepare various droplet-free films of other nitride and oxides (AlO_2, TiN, TiO_2, CrN, ZnO, etc.). However, the S-CAD has a problem that the deposition rate decreases by 1/3 to 1/5. Then, in order to increase the deposition rate, the enhanced shielded method (ES-CAD) in which the ions behind the shield were conducted and focused to the substrate by external magnetic field, was designed and the system apparatus was fabricated. After optimizing the magnetic filed configuration and magnetic flux density, the deposition rate in ES-CAD was more than 5 times as high as that in S-CAD, and was even faster than that in the non-shielded conventional method.
The improved ES-CAD (ES-CAD) in which the superconductor shield employed was then build, in order to obtain much faster deposition rate. The ions emitted from the cathode were effectively transported to the substrate by the detoured magnetic filed due to meissner effect of the superconductor. ES-CAD had higher deposition rate than ES-CAD. Furthermore, linear and torus type magnetically filtered arc deposition (FAD) systems having droplet filtering duct, were developed. As a result, it was found that the liner-FAD was not able to filter the droplets, although the torus-FAD was able to filter the droplets sufficiently.

  • Research Products

    (34 results)

All Other

All Publications (34 results)

  • [Publications] H.Takikawa: "Properties of titanium oxide film prepared by reactive cathodic vacuum arc deposition"Thin Solid Films. 348. 145-151 (1999)

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] H.Takikawa: "N_2 gas absorption in cathodic arc apparatus with an Al cathode under medium vacuum"IEEE Transactions on Plasma Science. 27・4. 1034-1038 (1999)

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] 滝川浩史: "種々の反応性真空アーク蒸着装置によるアモルファス酸化チタン膜の生成"電気学会論文誌. 119-A・10. 1243-1248 (1999)

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] H.Takikawa: "Synthesis of a-axis-oriented AlN film by a shielded reactive vacuum arc deposition method"Surface and Coatings Technology. 120/121. 383-387 (1999)

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] 宮野竜一: "TiN膜生成用シールド型真空アーク蒸着装置におけるプラズマパラメータ計測"電気学会論文誌. 119-A・12. 1397-1402 (1999)

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] 滝川浩史: "パルス電流真空アークの放電特性とドロップレット抑制効果"プラズマ応用科学. 7. 3-10 (1999)

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] H.Takikawa: "ZnO film fabrication by reactive shielded vacuum arc deposition"Transactions of the Material Research Society of Japan. 25・1. 345-348 (2000)

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] R.Miyano: "Ion energy measurement in shielded vacuum arc with graphite cathode"電気学会論文誌. 120-A・6. 724-725 (2000)

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] R.Miyano: "Preparation of metal nitride and oxide thin films using shielded reactive vacuum arc disposition"Vacuum. 59. 159-167 (2000)

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] H.Takikawa: "ZnO film formation using a steered and shielded reactive vacuum arc deposition"Thin Solid Films. 377/378. 74-80 (2000)

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] 池田光邦: "真空アークプラズマの磁気輸送とドロップレット削減効果"プラズマ応用科学. 8. 80-87 (2000)

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] H.Takikawa: "Effect of substrate bias on AlN thin film preparation in shielded reactive vacuum arc deposition"Thin Solid Films. 386. 276-280 (2001)

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] R.Miyano: "Anode mode in cathodic arc deposition apparatus with various cathodes and ambient gases"Thin Solid Films. 390・1-2. 192-196 (2001)

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] R.Miyano: "Cathode spot motion in vacuum arc of zinc cathode under oxygen gas flow"IEEE Transactions on Plasma Science. 29. 713-717 (2001)

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] 滝川浩史: "磁気フィルタ型陰極アークプラズマによるダイヤモンドライクカーボン薄膜の合成"プラズマ応用科学. 9. 49-56 (2001)

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] H.Takikawa: "Cathodic arc deposition with activated anode (CADAA) for preparation of in situ doped thin solid films"Vacuum. (印刷中). (2002)

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] R.Miyano: "Influence of gap length and pressure on medium vacuum arc with Ti cathode in various ambient gases"Thin solid films. (印刷中). (2002)

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] H. Takikawa, T. Matsui, T. Sakakibara, A. Bendavid, P. J. Martin: "Properties of titanium oxide film prepared by reactive cathodic vacuum arc deposition"Thin Solid Films. Vol.348. 145-151 (1999)

    • Description
      「研究成果報告書概要(欧文)」より
  • [Publications] H. Takikawa, N. Kawakami, T. Sakakibara: "N_2 gas absorption in cathodic arc apparatus with an Al cathode under medium vacuum"IEEE Transactions on Plasma Science. Vol. 27, No. 4. 1034-1038 (1999)

    • Description
      「研究成果報告書概要(欧文)」より
  • [Publications] H. Takikawa, T. Matsui, R. Miyano, T. Sakakibara, A. Bendavid, P. J. Martin: "Fabrication of amorphous titanium oxide films with various reactive vacuum arc deposition apparatuses"Transactions of the Institute of Electrical Engineering of Japan. 119-A. 1243-1248 (1999)

    • Description
      「研究成果報告書概要(欧文)」より
  • [Publications] H. Takikawa, N. Kawakami, T. Sakakibara: "Synthesis of a-axis-oriented AlN film by a shielded reactive vacuum arc deposition method"Surface and Coatings Technology. Vol. 120-121. 383-387 (1999)

    • Description
      「研究成果報告書概要(欧文)」より
  • [Publications] R. Miyano, H. Takikawa, K. Shinsako, T. Sakakibara: "Measurements of plasma parameters in a shielded vacuum arc deposition apparatus for TiN film fabrication"Transactions of the Institute of Electrical Engineering of Japan. 119-A. 1397-1402 (1999)

    • Description
      「研究成果報告書概要(欧文)」より
  • [Publications] H. Takikawa, K. Kimura, T. Sakakibara: "Discharge characteristics of vacuum arc with pulse current and efficiency of macrodroplet suppression"Journal of Applied Plasma Science. Vol. 7. 3-10 (1999)

    • Description
      「研究成果報告書概要(欧文)」より
  • [Publications] H. Takikawa, K. Kimura, R. Miyano, T. Sakakibara: "ZnO film fabrication by reactive shielded vacuum arc deposition"Transactions of the Material Research Society of Japan. Vol. 25,No. 1. 345-348 (2000)

    • Description
      「研究成果報告書概要(欧文)」より
  • [Publications] R. Miyano, M. Nagayama, H. Takikawa, T. Sakakibara: "Ion energy measurement in shielded vacuum arc with graphite cathode"Transactions of the Institute of Electrical Engineering of Japan. 120-A. 724-725 (2000)

    • Description
      「研究成果報告書概要(欧文)」より
  • [Publications] R. Miyano, K. Kimura, K. Izumi, H. Takikawa, T. Sakakibara: "Preparation of metal nitride and oxide thin films using shielded reactive vacuum arc deposition"Vacuum. Vol. 59, No.1. 159-167 (2000)

    • Description
      「研究成果報告書概要(欧文)」より
  • [Publications] H. Takikawa, K. Kimura, R. Miyano, T. Sakakibara: "ZnO film formation using a steered and shielded reactive vacuum arc deposition"Thin Solid Films. Vol.377-378. 74-80 (2000)

    • Description
      「研究成果報告書概要(欧文)」より
  • [Publications] M. Ikeda, K. Izumi, R. Miyano, H. Takikawa, T.Sakakibara: "Magnetic transportation of vacuum arc plasma and droplet filtering"Journal of Applied Plasma Science. Vol. 8. 80-87 (2000)

    • Description
      「研究成果報告書概要(欧文)」より
  • [Publications] H. Takikawa, K. Kimura, T. Sakakibara, A. Bendavid, P. J. Martin, A. Matsumoto, K. Tsutsumi: "Effect of substrate bias on AlN thin film preparation in shielded reactive vacuum arc deposition"Thin Solid Films. Vol. 386. 276-280 (2001)

    • Description
      「研究成果報告書概要(欧文)」より
  • [Publications] R. Miyano, T. Saito, K. Kimura, M. Ikeda, H. Takikawa, T. Sakakibara: "Anode mode in cathodic arc deposition apparatus with various cathodes and ambient gases"Thin Solid Films. Vol. 390, No.1/2. 192-196 (2001)

    • Description
      「研究成果報告書概要(欧文)」より
  • [Publications] R. Miyano, Y. Fujimura, H. Takikawa, T. Sakakibara, M. Nagao: "Cathode spot motion in vacuum arc of zinc cathode under oxygen gas flow"IEEE Transactions on Plasma Science. 29. 713-717 (2001)

    • Description
      「研究成果報告書概要(欧文)」より
  • [Publications] H. Takikawa, K. Izumi, T. Sakakibara: "Deposition of diamond-like carbon film using magnetically filtered cathodic-arc-plasma"Journal of Applied Plasma Science. Vol. 9. 49-56 (2001)

    • Description
      「研究成果報告書概要(欧文)」より
  • [Publications] H. Takikawa, K. Kimura, R. Miyano, T. Sakakibara: "Cathodic arc deposition with activated anode (CADAA) for preparation of in situ doped thin solid films"Vacuum. (in press). (2002)

    • Description
      「研究成果報告書概要(欧文)」より
  • [Publications] R. Miyano, T. Saito, H. Takikawa, T. Sakakibara: "Influence of gap length and pressure on medium vacuum arc with Ti cathode in various ambient gases"Thin solid films. (in press). (2002)

    • Description
      「研究成果報告書概要(欧文)」より

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Published: 2003-09-17  

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