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2003 Fiscal Year Final Research Report Summary

Development of a new specimen thinning technique based on the quantum process.

Research Project

Project/Area Number 12355024
Research Category

Grant-in-Aid for Scientific Research (A)

Allocation TypeSingle-year Grants
Section展開研究
Research Field Physical properties of metals
Research InstitutionHOkkaido University (2003)
The University of Tokyo (2000-2002)

Principal Investigator

ICHINOSE Hideki  Hokkaido Univ., Center for Advanced Research of Energy Conversion Materials, Prof., エネルギー先端工学研究センター, 教授 (30159842)

Co-Investigator(Kenkyū-buntansha) SHIBAYAMA Tamaki  Hokkaido Univ., Center for Advanced Research of Energy Conversion Materials, Prof., 大学院・工学系研究科, 助教授 (10241564)
IKUHARA Yuichi  University of Tokyo, Graduate School of Eng., Prof., 工学部, 教授 (70192474)
須賀 唯知  東京大学, 先端科学研究センター, 教授 (40175401)
TAKAHASHI Heisichiro  Hokkaido Univ., Center for Advanced Research of Energy Conversion Materials, Prof. (80001337)
Project Period (FY) 2000 – 2003
Keywordsquantum-process thinning / damage free super thin foil / laser gun / ultra violet laser / damage free surface / thin foil for TEM observation / atomic structure analyzing system / tuned irradiation
Research Abstract

The research is aimed to develop a new specimen thinning technique employing not an accelerated ions but a tuned short wave length electro magnetic wave to cut out atomic bonding on or near the materials surface to thin the specimen layer by layer without any damages on and in the specimen. The new technique is expected to increase the quality and the credibility of indispensable atomic structure information to the nano-technology obtained by a TEM. Apparent advancement in the precise control technique of the laser power, in development of fine focus control system and in high efficiency this technique on various materials were shown. Detailed results are as follows ; (1)A quantum-process thinning system equipped by both an ion gun and a laser gun was developed to acquire the optimum optical condition and energy density of the laser, (2)Both binary elemental covalent handing material (SiC) and a pure covalent bonding material (diamond) were thinned at the fixed wavelength to compare with Si to optimize the thinning condition. (3)A guiding rule to evaluate the size of evaporating material from the surface due to the laser irradiation was obtained. (4)A prototype of the new product was designed. The research is planned to be followed by the JST project on the next stage.

  • Research Products

    (18 results)

All Other

All Publications (18 results)

  • [Publications] K.Murakami, M.Saito, E.Takuma, H.Ichinose: "ARHVTEM of the Pd/ZnO heterointerface chemical structure"J.Electron Microscopy. 52. 27-32 (2003)

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] E.Takuma, H.Ichinose: "Atomic site determination of a high-pulity SiC grain boundary"Philosophical Magazine. 82. 857-866 (2002)

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] E.Takuma, H.Ichinose, F-R.Chen: "Atomic structure observation of silicon carbide using HRTEM"J.Electron Microscopy. 51. 297-302 (2002)

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] N.Shibata, F.Oba, T.Yamamoto, T.Sakuma, Y.Ikuhara: "Grain-boundary faceting at a Σ=3, [110]/{112} grain boundary in a cubic zirconia bicrystal, Phil.Mag"Philosophical Magazine. 83. 2221-2246 (2003)

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] T.Sakuma, Y.Ikuhara, T.Yamamoto, H.Yoshida: "Twords Grain Boundary Engineering in Advanced Ceramics"Ann.Chim.Sci.Mater. 27. S345-S356 (2002)

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] Hidehiro Yoshida, Yuichi Ikuhara, Taketo Sakuma: "Grain boundary electronic structure related to the high-temperature creep resistance in polycrystalline Al_2O_3"Acta.Material. 85. 2955-2966 (2002)

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] T.Torimoto, J.P.Reyes, K.Iwasaki, H.Takahashi: "Preparation of Novel Silica-Cadmium Sulfide Composite Nanoparticles Having Adjustable Void Space by Size-Selective Photoetching"J.of American Chemical Society. 125. 316-317 (2003)

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] K.Matsuura, M.Kudoh, H.Kinoshita, H.Takahashi: "Precipitation of Si particles in a super-rapidly solidified Al-Si hypereutectic alloy"Materials Chemistry and Physics. 81. 393-395 (2003)

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] Y.Sueishi, N.Sakaguchi, T.Shibayama, H.Kinoshita, H.Takahashi: "Radiation-induced segregation and precipitation behaviors around cascadeclusters under electron irradiation"J.of Electron Microscopy. 52. 63-68 (2003)

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] K.Murakami, M.Saito, E.Takuma, H.Ichinose: "ARHVTEM of the Pd/ZnO heterointerface chemical structure"J.Electron Microscopy. 52. 27-32 (2003)

    • Description
      「研究成果報告書概要(欧文)」より
  • [Publications] E.Takuma, H.Ichinose: "Atomic site determination of a high-pulity SiC grain boundary"Philosophical Magazine. 82. 857-866 (2002)

    • Description
      「研究成果報告書概要(欧文)」より
  • [Publications] E.Takuma, H.Ichinose, F-R.Chen: "Atomic structure observation of silicon carbide using HRTEM"J.Electron Microscopy. 51. 297-302 (2002)

    • Description
      「研究成果報告書概要(欧文)」より
  • [Publications] N.Shibata, F.Oba, T.Yamamoto, T.Sakuma, Y.Ikuhara: "Grain-boundary faceting at a Σ=3, [110]/{112} grain boundary in a cubic zirconia bicrystal"Philosophical Magazine. 83. 2221-2246 (2003)

    • Description
      「研究成果報告書概要(欧文)」より
  • [Publications] T.Sakuma, Y.Ikuhara, T.Yamamoto, H.Yoshida: "Towards Grain Boundary Engineering in Advanced Ceramics"Ann.Chim.Sci.Mater. 27. S345-S356 (2002)

    • Description
      「研究成果報告書概要(欧文)」より
  • [Publications] Hidehiro Yoshida, Yuichi Ikuhara, Taketo Sakuma: "Grain boundary electronic structure related to the high-temperature creep resistance in polycrystalline Al_2O_3."Acta.Material. 85. 2955-2966 (2002)

    • Description
      「研究成果報告書概要(欧文)」より
  • [Publications] T.Torimoto, J.P.Reyes, K.Iwasaki, H.Takahashi: "Preparation of Novel Silica-Cadmium Sulfide Composite Nanoparticles Having Adjustable Void Space by Size-Selective Photoetching"J.of Americam Chemical Soc.. 125. 316-317 (2003)

    • Description
      「研究成果報告書概要(欧文)」より
  • [Publications] K.Matsuura, M.Kudoh, H.Kinoshita, H.Takahashi: "Precipitation of Si particles in a super-rapidly solidified Al-Si hypereutectic alloy"Materials Chemistry and Physics. 81. 393-395 (2003)

    • Description
      「研究成果報告書概要(欧文)」より
  • [Publications] Y.Sueishi, N.Sakaguchi, T.Shibayama, H.Kinoshita, H.Takahashi: "Radiation-induced segregation and precipitation behaviors around cascadeclusters under electron irradiation"J.of Electron Microscopy. 52. 63-68 (2003)

    • Description
      「研究成果報告書概要(欧文)」より

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Published: 2005-04-19  

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