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1989 Fiscal Year Final Research Report Summary

Development of Non-contact Thermal Monitor Using Fiber Optics

Research Project

Project/Area Number 63840025
Research Category

Grant-in-Aid for Developmental Scientific Research

Allocation TypeSingle-year Grants
Research Field 鉱物学(含岩石・鉱床学)
Research InstitutionUniversity of Tokyo

Principal Investigator

HAGA Nobuhiko  Univ. of Tokyo, Fac. of Science Research Assoc., 理学部, 助手 (60011748)

Co-Investigator(Kenkyū-buntansha) HORIUCHI Hiroyuki  Univ. of Tokyo, Fac. of Science Associate Prof., 理学部, 助教授 (80029892)
TOKONAMI Masayasu  Univ. of Tokyo, Fac. of Science Professor, 理学部, 教授 (80029850)
Project Period (FY) 1988 – 1989
KeywordsFiber Optics / Thermal Monitor / Gas Stream Heater / High Temperature / X-ray Diffraction / Microtexture
Research Abstract

It was the first purpose to plan and to manufacture the miniature electric resistance furnace for single crystal diffractometer and the non-contact temperature measuring system. For the miniature electric resistance furnace, the hot gas stream furnace was made instead of electric one, because of the very poor space around the specimen on the goniometer. This can blow out hot gas up to 800゚C. The temperature was controlled by changing electric voltage or gas pressure with thermally monitoring. Gas cylinder or air compressor serves as source of gas.
The temperature measuring system is characterized by the fiber optics cable connected to the detector head, and the emissivity independent for greybody target by applying the "band ratio method". This system is composed of following three principal parts. One is optical fiber assembly attached with the micro spot lens cell which has spot diameter 0.5mm and working distance 50mm. Fiber is flexible and the radius of curvature is 2". Second part is the detector head assembly, which contains the lead sulfide band filter, tuning-fork chopper and preamplifier. This enable to measure temperature during 700-1,510゚C. Detector head assembly is connected by cable to the panel controller. On front panel there are power switch, digital panel meter, gain controls, spectrum control and so on, and there is input/output connections on rear panel. The calibration source and backlighting source are equipped.
High temperature single crystal diffraction study of ferroelastic material, LaP_5O_<14>, was planned as test experiment, only room temperature experiment has been done.

  • Research Products

    (8 results)

All Other

All Publications (8 results)

  • [Publications] 堀内弘之: "Crystal Structures of mantle minerals and their implications for phase transition at high pressures" In“Dynamic Processes of Material Transport and Transformation in the Earth's Interior"Terra Scientific publishing Company. 191-217 (1990)

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] 沢本絋: "β(Mg_<0.9>Fe_<0.1>)_2Si0_4:single crystal structure,cation distribution,and property of coordination polyhedra" Phys.Chem.Minerals. (1990)

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] 芳賀信彦: "A high temperature neutron diffraction study of the anharmonicity and structural instability below the ortho-proto phase transition in evstatite,Mg_2Si_2O_6 and a lattice dynamical model" Acta Cryst.B. (1990)

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] 千葉恵里子: "Structures of methylphenylhydragone elerivatives and their nonlinear optical properties." Acta Cryst.B. (1990)

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] HORIUCHI, H.: "Crystal structure of mantle minerals and their implications for phase transition at high pressures." "Dynamic Processes of Material Transport and Transformation in the Earth's Interior".

    • Description
      「研究成果報告書概要(欧文)」より
  • [Publications] Sawamoto, H.: "BETA(Mg0.9, Fe0.1)2Si04:single crystal structure, cation distribution and property of coordination polyhedra." Phys. Chem. Minerals.

    • Description
      「研究成果報告書概要(欧文)」より
  • [Publications] HAGA, N.: "A high temperature neutron diffraction study of the anharmonicity and structural instability below the ortho-proto phase transition in enstatite, Mg_2Si_2O_6 and a lattice dynamical model." Acta Cryatallogr. B.

    • Description
      「研究成果報告書概要(欧文)」より
  • [Publications] E.Chiba: "Structures of methylphenylhydrazone derivatives and their nonlinear optical properties." Acta Cryatallogr. B.

    • Description
      「研究成果報告書概要(欧文)」より

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Published: 1993-03-26  

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