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Stabilizing gamma prime phase using Suzuki segregation to enhance the creep resistance of Co-Ni-based superalloy

Research Project

Project/Area Number 19K23566
Research Category

Grant-in-Aid for Research Activity Start-up

Allocation TypeMulti-year Fund
Review Section 0401:Materials engineering, chemical engineering, and related fields
Research InstitutionTohoku University

Principal Investigator

Huakang Bian  東北大学, 金属材料研究所, 助教 (30796230)

Project Period (FY) 2019-08-30 – 2021-03-31
Project Status Completed (Fiscal Year 2020)
Budget Amount *help
¥2,730,000 (Direct Cost: ¥2,100,000、Indirect Cost: ¥630,000)
Fiscal Year 2020: ¥1,300,000 (Direct Cost: ¥1,000,000、Indirect Cost: ¥300,000)
Fiscal Year 2019: ¥1,430,000 (Direct Cost: ¥1,100,000、Indirect Cost: ¥330,000)
KeywordsSuperalloy / Ni-Co-based alloy / Suzuki segregation / gamma prime / Co-Ni-based Superalloy / Creep / Re addtition / Co-Ni-based superalloy / creep resistance / Creep resistance / Stabilizing
Outline of Research at the Start

The service life of Ni-based superalloy will be reduced by the coarsening or rafting of the γ' phase particles at high temperature,which has been successfully slowed down by the applicant using Suzuki segregation. Thus, the service life is expected to be prolonged by introducing Suzuki segregation.

Outline of Final Research Achievements

CoーNi-based superalloy was designed via Suzuki segregation strengthening which showed excellent mechanical properties at RT and high temperature. However, it shows low ductility and poor creep resistance at high temperature. The reason was attributed to the weakness of grain boundary which gives rise to intercrystalline fracture. Thus, it is necessary to enhance the strength of grain boundary. Thus, in the present research proposal, 1, 2, and 3 wt% Re was added into the developed CoーNi-based superalloy to study how Re influence the grain boundary. Beside that little B is also will be introduced to further strengthening the grain boundary. After addition of 1, 2, and 3 wt% Re, the tensile elongation increased to 14%, 23%, and 20% at RT respectively while 8%, 15%, and 18% at 700 ℃. the brittleness was obviously improved due to the enhancement of grain boundary. And the mechanism of how Suzuki segregation slowed down the coarsening of γ' phase was figured out via STEM observation.

Academic Significance and Societal Importance of the Research Achievements

鈴木効果に関する研究は長い時間で趣味になっている。特に積層欠陥エネルギー低い生体材料CCM合金における、鈴木偏析が発生しやすい。申請者ら、CCMをベースにして、γ'強化を導入、Co-Ni基超合金を開発した。さらに、鈴木偏析は高温でγ'相粗大化を抑える効果を初発見した。本提案はSTEM観察を行った、その粗大化抑えるメカニズムを解明した。さらに、このCo-Ni基超合金は延性が低い、耐クリープ性が悪い。耐クリープ性アープするため、Reを添加した。Reを添加すると、延性がよく改善された。特に、2wt% Reの添加は、最適化するとこを確認された。この研究結果により、未来もといい合金の開発を目指している。

Report

(3 results)
  • 2020 Annual Research Report   Final Research Report ( PDF )
  • 2019 Research-status Report
  • Research Products

    (7 results)

All 2021 2020 2019

All Journal Article (1 results) (of which Peer Reviewed: 1 results) Presentation (6 results)

  • [Journal Article] Hot deformation characteristics and dynamic recrystallization mechanisms of a Co?Ni-based superalloy2020

    • Author(s)
      Ouyang Lingxiao、Luo Rui、Gui Yunwei、Cao Yun、Chen Leli、Cui Yujie、Bian Huakang、Aoyagi Kenta、Yamanaka Kenta、Chiba Akihiko
    • Journal Title

      Materials Science and Engineering: A

      Volume: 788 Pages: 139638-139638

    • DOI

      10.1016/j.msea.2020.139638

    • Related Report
      2020 Annual Research Report
    • Peer Reviewed
  • [Presentation] Enhancing the ductility of C0-Ni-based superalloy at room and elevated temperatures by Re addition2021

    • Author(s)
      卞華康, 欧陽凌霄, 崔玉傑, 山中謙太, 千葉晶彦
    • Organizer
      日本金属学会2021年春期(第168回)講演大会
    • Related Report
      2020 Annual Research Report
  • [Presentation] The influence of B and Re addition on the microstructure and mechanical properties of Co-Ni-based superalloy2020

    • Author(s)
      卞華康, 欧陽凌霄, 崔玉傑, 山中謙太, 千葉晶彦
    • Organizer
      金属学会 2020年秋期(第167回)講演大会
    • Related Report
      2020 Annual Research Report
  • [Presentation] Hot deformation characteristics and dynamic recrystallization mechanisms of a Co-Ni-based superalloy2020

    • Author(s)
      卞華康, 欧陽凌霄, 貴雲, 崔玉傑, 青柳健大, 山中謙太, 千葉晶彦
    • Organizer
      第139回金研講演会
    • Related Report
      2020 Annual Research Report
  • [Presentation] A novel high entropy superalloy strengthened simultaneously by Suzuki segregation and γ' phase2019

    • Author(s)
      Huakang Bian, Kenta Yamanaka, Akihiko Chiba
    • Organizer
      2019年度日本塑性加工学会東北・北海道支部若手研究発表会
    • Related Report
      2019 Research-status Report
  • [Presentation] High Temperature Deformation characteristics and microstructure evolution of a novel high entropy superalloy2019

    • Author(s)
      Lingxiao Ouyang, Huakang Bian, Kenta Yamanaka, Akihiko Chiba
    • Organizer
      2019年度日本塑性加工学会東北・北海道支部若手研究発表会
    • Related Report
      2019 Research-status Report
  • [Presentation] The microstructure and mechanical properties of a high entropy superalloy at elevated temperatures2019

    • Author(s)
      Lingxiao Ouyang, Huakang Bian, Yujie Cui, Kenta Yamanaka, Kenta Aoyagi, Akihiko Chiba
    • Organizer
      金属学会秋期講演大会(165回)
    • Related Report
      2019 Research-status Report

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Published: 2019-09-03   Modified: 2022-01-27  

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