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Novel synthesis of carbon nanoparticles including ferromagnetic nanoparticles with high surface area and application to water purification technology

Research Project

Project/Area Number 24360327
Research Category

Grant-in-Aid for Scientific Research (B)

Allocation TypePartial Multi-year Fund
Section一般
Research Field Reaction engineering/Process system
Research InstitutionKyoto University

Principal Investigator

SANO Noriaki  京都大学, 工学(系)研究科(研究院), 准教授 (70295749)

Co-Investigator(Kenkyū-buntansha) TAMON Hajime  京都大学, 工学研究科, 教授 (30111933)
Project Period (FY) 2012-04-01 – 2015-03-31
Project Status Completed (Fiscal Year 2014)
Budget Amount *help
¥19,370,000 (Direct Cost: ¥14,900,000、Indirect Cost: ¥4,470,000)
Fiscal Year 2014: ¥4,810,000 (Direct Cost: ¥3,700,000、Indirect Cost: ¥1,110,000)
Fiscal Year 2013: ¥4,550,000 (Direct Cost: ¥3,500,000、Indirect Cost: ¥1,050,000)
Fiscal Year 2012: ¥10,010,000 (Direct Cost: ¥7,700,000、Indirect Cost: ¥2,310,000)
Keywords材料合成プロセス / カーボン / プラズマ / ナノ材料 / カーボンナノホーン / 強磁性体 / アーク放電
Outline of Final Research Achievements

Fe-included carbon nanohorns (Fe-CNH) were synthesized by gas-injected arc-in-water method. To open small pores on Fe-CNHs, oxidation treatment was performed on Fe-CNH under the conditions in CO2-N2, air, and ozone-dissolved water. As a result, Fe became magnetite by the treatment using N2-CO2 and ozone water, and the magnetic susceptibility of Fe-CNH increased. Furthermore, the specific surface area increased by 2.5 times by the treatment using CO2-N2. Total organic carbon in water increased when ozone react with carbon, so that the combination of ozone and Fe-CNH may not be preferable to make pure water. The activity of Fe-CNH is very high as catalyst support when biodiesel is produced.

Report

(4 results)
  • 2014 Annual Research Report   Final Research Report ( PDF )
  • 2013 Annual Research Report
  • 2012 Annual Research Report
  • Research Products

    (23 results)

All 2015 2014 2013 2012

All Journal Article (6 results) (of which Peer Reviewed: 6 results,  Acknowledgement Compliant: 3 results) Presentation (17 results) (of which Invited: 5 results)

  • [Journal Article] Simultaneous enhancement in porosity and magnetic property of Fe-dispersing single-walled carbon nanohorns by oxidation using CO22015

    • Author(s)
      Noriaki Sano, Daisuke Himara, Hajime Tamon
    • Journal Title

      Chemical Engineering Journal

      Volume: 271 Pages: 43-49

    • DOI

      10.1016/j.cej.2015.02.074

    • NAID

      120005678218

    • Related Report
      2014 Annual Research Report
    • Peer Reviewed / Acknowledgement Compliant
  • [Journal Article] Gas Flow Rate in the Gas-Injected Arc-in-Water Method as a Critical Factor to Synthesize High-Dispersion Pd–Ni Alloy Nanoparticles in Single-Walled Carbon Nanohorns2014

    • Author(s)
      Noriaki Sano, Kosuke Taniguchi and Hajime Tamon
    • Journal Title

      JOURNAL OF CHEMICAL ENGINEERING OF JAPAN

      Volume: 47 Issue: 11 Pages: 821-826

    • DOI

      10.1252/jcej.14we002

    • NAID

      130004703867

    • ISSN
      0021-9592, 1881-1299
    • Related Report
      2014 Annual Research Report
    • Peer Reviewed / Acknowledgement Compliant
  • [Journal Article] Effect of Fe/Fe2O3 loading on the catalytic activity of sulfonated single-walled carbon nanohorns for the esterification of palmitic acid2014

    • Author(s)
      Chantamanee Poonjarernsilp, Noriaki Sano, Nut Sawangpanich
    • Journal Title

      Green Chemistry

      Volume: 16 Issue: 12 Pages: 4936-4943

    • DOI

      10.1039/c4gc00262h

    • NAID

      120005661769

    • Related Report
      2014 Annual Research Report
    • Peer Reviewed / Acknowledgement Compliant
  • [Journal Article] Hydrogen Storage in Porous Single-Walled Carbon Nanohorns Dispersed with Pd−Ni Alloy Nanoparticles2014

    • Author(s)
      N. Sano, K. Taniguchi, H. Tamon
    • Journal Title

      The Journal of Physical Chemistry C

      Volume: 118 Issue: 7 Pages: 3402-3408

    • DOI

      10.1021/jp4098155

    • Related Report
      2014 Annual Research Report 2013 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Fabrication of carbon nanotube film directly grown on conductive stainless steel film and application to dielectrophoretic nanoparticle capture2014

    • Author(s)
      N. Sano, T. Nakamura, H. Tamon, T. TSuntornlohanakul, C. Poonjarernsilp, T. Charinpanitkul
    • Journal Title

      Journal of Applied Physics.

      Volume: 115 Issue: 15 Pages: 154302-154302

    • DOI

      10.1063/1.4870856

    • NAID

      120005439645

    • Related Report
      2014 Annual Research Report 2013 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Controlled Syntheses of Various Palladium Alloy Nanoparticles Dispersed in Single-Walled Carbon Nanohorns by One-Step Formation Using an Arc Discharge Method2014

    • Author(s)
      N. Sano, T. Suntornlohanakul, C. Poonjarernsilp, H. Tamon, T. Charinpanitkul
    • Journal Title

      Industrial & Engineering Chemistry Research

      Volume: 53 Issue: 12 Pages: 4732-4738

    • DOI

      10.1021/ie500146f

    • Related Report
      2014 Annual Research Report 2013 Annual Research Report
    • Peer Reviewed
  • [Presentation] SYNTHESIS OF CARBON NANOHORNS DISPERSED WITH IRON NANOPARTICLES FOR PREPARATION OF SOLID BASE CATALYST2014

    • Author(s)
      Kohei Yamada, Noriaki Sano, Hajime Tamon
    • Organizer
      International Conference on Separation Science and Technology 2014
    • Place of Presentation
      奈良公会堂
    • Year and Date
      2014-10-30 – 2014-11-01
    • Related Report
      2014 Annual Research Report
  • [Presentation] Variety of Nanotube Family Materials for Sustainable Technologies2014

    • Author(s)
      Noriaki Sano
    • Organizer
      International Conference on “Safe and Sustainable Nanotechnology”
    • Place of Presentation
      Pitsanulok (Thailand)
    • Year and Date
      2014-10-14 – 2014-10-17
    • Related Report
      2014 Annual Research Report
    • Invited
  • [Presentation] 強磁性体内包固体塩基カーボンナノ材料の合成2014

    • Author(s)
      山田 貢平・ 佐野 紀彰・ 田門 肇
    • Organizer
      化学工学会 第46回秋季大会
    • Place of Presentation
      九州大学(伊都キャンパス)
    • Year and Date
      2014-09-17 – 2014-09-19
    • Related Report
      2014 Annual Research Report
  • [Presentation] オゾン酸化処理によるFeナノ内包カーボンナノホーンの磁化特性・細孔構造の向上2014

    • Author(s)
      山田貢平,佐野紀彰,田門肇
    • Organizer
      分離技術会年会2014
    • Place of Presentation
      名古屋大学
    • Year and Date
      2014-05-30 – 2014-05-31
    • Related Report
      2014 Annual Research Report
  • [Presentation] Synthesis of Carbon Nanohorns Using Gas-Injected Arc-in-Water Method for Energy Applications2014

    • Author(s)
      Noriaki Sano
    • Organizer
      2014 International Workshop on Plasma Applications in Nanocarbon Materials and Devices
    • Place of Presentation
      福岡
    • Related Report
      2013 Annual Research Report
    • Invited
  • [Presentation] オゾン酸化を用いた高比表面積を有する強磁性ナノ粒子内包カーボンナノホーンの作製2014

    • Author(s)
      佐野 紀彰、山田 貢平、 田門 肇
    • Organizer
      化学工学会第79年会
    • Place of Presentation
      岐阜大学
    • Related Report
      2013 Annual Research Report
  • [Presentation] カーボンナノホーン・ナノチューブの合成およびその賦活効果2014

    • Author(s)
      佐野紀彰
    • Organizer
      活性炭技術研究会 活性炭講座(第9講)および第151回講演会
    • Place of Presentation
      大阪
    • Related Report
      2013 Annual Research Report
    • Invited
  • [Presentation] Single-step synthesis of carbon nanohorns including Pd-Ni alloy nanoparticles and their ability for hydrogen storage2013

    • Author(s)
      Noriaki Sano
    • Organizer
      THERMEC'2013
    • Place of Presentation
      Las Vegas
    • Related Report
      2013 Annual Research Report
    • Invited
  • [Presentation] My Researches on Carbon Nanomaterials with Thai Researchers and Students2013

    • Author(s)
      Noriaki Sano
    • Organizer
      6th Thailand-Japan International Academic Conference 2013
    • Place of Presentation
      大阪
    • Related Report
      2013 Annual Research Report
    • Invited
  • [Presentation] Synthesis of Carbon Nanotubes on Metallic Surfaces2013

    • Author(s)
      N. Sano, S. Yamamoto, T. Nakamura, H. Tamon
    • Organizer
      9th World Congress of Chemical Engineering
    • Place of Presentation
      ソウル
    • Related Report
      2013 Annual Research Report
  • [Presentation] Application of gas-injected arc-in-water method to synthesize carbon nanohorns includingferromagnetic nanoparticles2013

    • Author(s)
      Noriaki Sano, Daisuke Hirama, and Hajime Tamon
    • Organizer
      第26回プラズマ材料科学シンポジウム
    • Place of Presentation
      福岡
    • Related Report
      2013 Annual Research Report
  • [Presentation] 強磁性ナノ粒子分散カーボンナノホーンに対する二酸化炭素賦活の効果2013

    • Author(s)
      佐野紀彰、平間大介、田門肇
    • Organizer
      第27回日本吸着学会研究発表会
    • Place of Presentation
      千葉大学
    • Related Report
      2013 Annual Research Report
  • [Presentation] アーク放電を用いたFeナノ粒子分散カーボンナノホーンの合成およびCO2賦活の効果2013

    • Author(s)
      佐野紀彰、平間大介、田門肇
    • Organizer
      化学工学会第45回秋季大会
    • Place of Presentation
      岡山大学
    • Related Report
      2013 Annual Research Report
  • [Presentation] Hydrogen absorption characterist ics of single walled carbon nanohorns including Pd-Ni alloy nanoparl icles prepared by gas-injected arc-in-water method2012

    • Author(s)
      N. Sano, K. Taniguehi, H. Tamon
    • Organizer
      11th Asia-Pacific Conference on Plasma Science and Technologv
    • Place of Presentation
      京都大学(桂キャンパス)
    • Year and Date
      2012-10-03
    • Related Report
      2012 Annual Research Report
  • [Presentation] ガス導入アーク放電による強磁性ナノ粒子分散カーボンナノホーンの合成2012

    • Author(s)
      平間大介、佐野紀彰、田門肇
    • Organizer
      化学工学会第44回秋季大会
    • Place of Presentation
      東北大学(仙台)
    • Year and Date
      2012-09-20
    • Related Report
      2012 Annual Research Report
  • [Presentation] Hydrogen absorbing property of carbon nanohorns dispersed with Pd-Ni al loynanoprtic.les synthesized by gas-injected arc-in-water method2012

    • Author(s)
      N. Sano, K : Taniguchi, H. Tamon
    • Organizer
      第73回応用物理学会学術講演会
    • Place of Presentation
      愛媛大学(松山)
    • Year and Date
      2012-09-13
    • Related Report
      2012 Annual Research Report
  • [Presentation] Synthesis of carbon nanohorns dispersed with metallic nanoparticles by gas-injected arc-in-water method2012

    • Author(s)
      N. Sano, T. SunLornlohanakui, C. Poonjarerusilp, D. Hirama, K. Taniguchi, T. Norimoto, T. Jshii, H. Tamon, T. Charinuanitku
    • Organizer
      第43回フラーレン・ナノチューブ・グフフェン総合シンポジウム
    • Place of Presentation
      東北大学(仙台)
    • Year and Date
      2012-09-06
    • Related Report
      2012 Annual Research Report

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Published: 2012-04-24   Modified: 2019-07-29  

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